ES2164470T3 - Proceso para producir un pigmento de tio2 usando co-oxidacion para proporcionar recubrimientos de hidroxido. - Google Patents
Proceso para producir un pigmento de tio2 usando co-oxidacion para proporcionar recubrimientos de hidroxido.Info
- Publication number
- ES2164470T3 ES2164470T3 ES98964176T ES98964176T ES2164470T3 ES 2164470 T3 ES2164470 T3 ES 2164470T3 ES 98964176 T ES98964176 T ES 98964176T ES 98964176 T ES98964176 T ES 98964176T ES 2164470 T3 ES2164470 T3 ES 2164470T3
- Authority
- ES
- Spain
- Prior art keywords
- oxide
- pigment
- tio2
- oxidation
- produce
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000049 pigment Substances 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 title 1
- 238000007254 oxidation reaction Methods 0.000 title 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract 6
- 239000002243 precursor Substances 0.000 abstract 4
- 239000000725 suspension Substances 0.000 abstract 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- -1 aluminum halide Chemical class 0.000 abstract 2
- 239000007789 gas Substances 0.000 abstract 2
- 239000011777 magnesium Substances 0.000 abstract 2
- 229910052749 magnesium Inorganic materials 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000010955 niobium Substances 0.000 abstract 2
- 229910052758 niobium Inorganic materials 0.000 abstract 2
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 abstract 2
- 239000002245 particle Substances 0.000 abstract 2
- 229910052698 phosphorus Inorganic materials 0.000 abstract 2
- 239000011574 phosphorus Substances 0.000 abstract 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 229910052796 boron Inorganic materials 0.000 abstract 1
- 229910052810 boron oxide Inorganic materials 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 abstract 1
- 229910052732 germanium Inorganic materials 0.000 abstract 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 abstract 1
- YBMRDBCBODYGJE-UHFFFAOYSA-N germanium oxide Inorganic materials O=[Ge]=O YBMRDBCBODYGJE-UHFFFAOYSA-N 0.000 abstract 1
- PVADDRMAFCOOPC-UHFFFAOYSA-N oxogermanium Chemical class [Ge]=O PVADDRMAFCOOPC-UHFFFAOYSA-N 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 239000010703 silicon Substances 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- 239000004408 titanium dioxide Substances 0.000 abstract 1
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 abstract 1
- 239000012808 vapor phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/36—Compounds of titanium
- C09C1/3607—Titanium dioxide
- C09C1/3653—Treatment with inorganic compounds
- C09C1/3661—Coating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/07—Producing by vapour phase processes, e.g. halide oxidation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
- C01P2004/82—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases
- C01P2004/84—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases one phase coated with the other
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Composite Materials (AREA)
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Abstract
Un proceso para producir un pigmento de dióxido de titanio que comprende los pasos de: a) hacer reaccionar un tetracloruro de titanio en fase vapor con haluro de aluminio y un gas que contiene oxígeno en un reactor a una temperatura dentro del intervalo de 900 C a 1600 C para proporcionar una suspensión gaseosa que comprende partículas de TiO2; b) poner en contacto la suspensión gaseosa con al menos dos precursores de óxido, donde el primer precursor de óxido es un haluro de silicio y el segundo precursor de óxido está seleccionado a partir del grupo que consiste en precursores de óxido de boro, fósforo, magnesio, niobio, germanio y una mezcla de los mismos; y c) enfriar la suspensión gaseosa para proporcionar un pigmento que comprende partículas de TiO2 quetienen un revestimiento que comprende sílice y un segundo óxido, donde el segundo óxido está seleccionado a partir del grupo que consiste en óxidos de boro, fósforo, magnesio, niobio, germanio y mezclas de los mismos.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/997,678 US5922120A (en) | 1997-12-23 | 1997-12-23 | Process for producing coated TiO2 pigment using cooxidation to provide hydrous oxide coatings |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2164470T3 true ES2164470T3 (es) | 2002-02-16 |
Family
ID=25544257
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES98964176T Expired - Lifetime ES2164470T3 (es) | 1997-12-23 | 1998-12-21 | Proceso para producir un pigmento de tio2 usando co-oxidacion para proporcionar recubrimientos de hidroxido. |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US5922120A (es) |
| EP (1) | EP1042408B1 (es) |
| JP (1) | JP3631138B2 (es) |
| AU (1) | AU750442B2 (es) |
| BR (1) | BR9814223A (es) |
| CA (1) | CA2309553C (es) |
| DE (1) | DE69802115T2 (es) |
| ES (1) | ES2164470T3 (es) |
| WO (1) | WO1999032562A1 (es) |
Families Citing this family (46)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0908494A3 (en) * | 1997-10-08 | 1999-11-10 | E.I. Dupont De Nemours And Company | Uniformly coated particulate metal oxide |
| US6040913A (en) * | 1999-01-29 | 2000-03-21 | E. I. Du Pont De Nemours And Company | Method to determine light scattering efficiency of pigments |
| US6620508B2 (en) * | 2000-01-25 | 2003-09-16 | Nippon Aerosil Co., Ltd. | Oxide powder and method for preparing the same, and product using the same |
| KR100376247B1 (ko) * | 2000-04-07 | 2003-03-15 | 삼화페인트공업주식회사 | 화염을 이용한 기상산화반응에 의한 나노사이즈이산화티타늄 초미분체 제조 방법 |
| US6548169B2 (en) * | 2000-04-25 | 2003-04-15 | Showa Denko Kabushiki Kaisha | Production process for ultrafine particulate complex oxide containing titanium oxide |
| AU2001257372B2 (en) * | 2000-04-27 | 2005-09-01 | E.I. Du Pont De Nemours And Company | Process for making durable titanium dioxide pigment in the chloride process without wet treatment |
| DE10236366A1 (de) * | 2002-08-08 | 2004-02-19 | Kronos International, Inc. | Verfahren zur Oberflächenbehandlung eines Titandioxid-Pigments |
| DE10260718A1 (de) * | 2002-12-23 | 2004-07-08 | Degussa Ag | Mit Siliziumdioxid umhülltes Titandioxid |
| US20050119398A1 (en) * | 2003-09-11 | 2005-06-02 | Lu Zhang | Plasma synthesis of metal oxide nanoparticles |
| DE102004027493A1 (de) * | 2003-12-19 | 2005-09-22 | Binnewies, Michael, Prof. Dr. | Funktionalisierung oxidischer Partikeloberflächen |
| US20050239921A1 (en) * | 2004-04-27 | 2005-10-27 | Birmingham John N | Preparation of organic additive-treated, pyrogenic silica-encapsulated titanium dioxide particles |
| US20050249659A1 (en) * | 2004-05-04 | 2005-11-10 | Flynn Harry E | Scour media for titanium dioxide production |
| US7988947B2 (en) | 2004-11-23 | 2011-08-02 | E. I. Du Pont De Nemours And Company | Mesoporous oxide of titanium |
| US20060263291A1 (en) * | 2004-11-23 | 2006-11-23 | Carmine Torardi | Mesoporous amorphous oxide of titanium |
| AU2005309411B2 (en) * | 2004-11-23 | 2011-06-02 | E.I. Dupont De Nemours And Company | Mesoporous metal oxide |
| US7601326B2 (en) * | 2004-11-23 | 2009-10-13 | E. I. Du Pont De Nemours And Company | Mesoporous oxide of zirconium |
| US7601327B2 (en) * | 2004-11-23 | 2009-10-13 | E.I. Du Pont De Nemours And Company | Mesoporous oxide of hafnium |
| US7799124B2 (en) | 2005-04-07 | 2010-09-21 | E.I. Du Pont De Nemours And Company | Process for treating inorganic particles via sintering of sinterable material |
| US20070072783A1 (en) * | 2005-09-26 | 2007-03-29 | Tronox Llc | Scour medium for titanium dioxide production |
| UA95622C2 (uk) * | 2006-01-30 | 2011-08-25 | Кронос Інтернацьональ, Інк. | ПІГМЕНТНІ ЧАСТИНКИ ДІОКСИДУ ТИТАНУ З ЛЕГОВАНОЮ ГУСТОЮ SiO2-ОБОЛОНКОЮ (ВАРІАНТИ), СПОСОБИ ЇХ ОДЕРЖАННЯ, ЗАСТОСУВАННЯ ТА МАТЕРІАЛ, ЩО ЇХ МІСТИТЬ |
| US7905953B2 (en) * | 2006-01-30 | 2011-03-15 | Kronos International Inc | Titanium dioxide pigment particles with doped, dense SiO2 skin and methods for their manufacture |
| US7763110B2 (en) * | 2006-01-30 | 2010-07-27 | Kronos International Inc | Titanium dioxide pigment particles with doped, dense SiO2 skin and methods for their manufacture |
| SA111320424B1 (ar) * | 2006-01-30 | 2014-05-11 | كرونوس انترناشونال انك | جسيمات خضاب ثاني أكسيد التيتانيوم المزوَّدة مع طبقة كثيفة ومشابة من ثاني أكسيد السيليكون SiO2 وطرق تصنيعها |
| US20070245924A1 (en) * | 2006-04-20 | 2007-10-25 | Hofmann Michael A | Reduced abrasion of titanium dioxide pigments produced from the chloride process |
| US20070248757A1 (en) * | 2006-04-20 | 2007-10-25 | Kostantinos Kourtakis | Processes for producing materials containing reduced abrasion titanium dioxide pigment |
| US7250080B1 (en) | 2006-09-06 | 2007-07-31 | Tronox Llc | Process for the manufacture of organosilicon compound-treated pigments |
| US20080053336A1 (en) * | 2006-09-06 | 2008-03-06 | Tronox Llc | Aqueous coating compositions with improved tint strength and gloss properties, comprising pigments surface-treated with certain organosilicon compounds |
| US8114377B2 (en) * | 2006-11-02 | 2012-02-14 | E.I. Du Pont De Nemours And Company | Process for producing titanium dioxide particles having reduced chlorides |
| US7238231B1 (en) | 2006-11-16 | 2007-07-03 | Tronox Llc | Process for manufacturing zirconia-treated titanium dioxide pigments |
| US8951607B2 (en) * | 2007-05-03 | 2015-02-10 | Tronox, Llc | Making co-precipitated mixed oxide-treated titanium dioxide pigments |
| US8663380B2 (en) * | 2007-11-16 | 2014-03-04 | Cristal Usa Inc. | Gas phase production of coated titania |
| US20090148605A1 (en) * | 2007-12-05 | 2009-06-11 | Akhtar M Kamal | Process for the production of coated titanium dioxide pigments |
| AU2012205850B2 (en) * | 2011-01-10 | 2016-01-07 | The Chemours Company Fc,Llc | Process for controlling particle size and additive coverage in the preparation of titanium dioxide |
| CN102352135B (zh) * | 2011-08-15 | 2013-11-13 | 无锡豪普钛业有限公司 | 包覆硅氧化物的二氧化钛颜料及包覆工艺 |
| US9573108B2 (en) | 2011-10-28 | 2017-02-21 | The Chemours Company Tt, Llc | Treated inorganic core particles having improved dispersability |
| WO2014078040A1 (en) | 2012-11-13 | 2014-05-22 | E. I. Du Pont De Nemours And Company | Process for preparing self-dispersing pigments |
| US9546450B2 (en) | 2012-11-13 | 2017-01-17 | The Chemours Company Tt, Llc | Laminates prepared from decor paper comprising self-dispersing pigments |
| CA2891157C (en) | 2012-11-13 | 2020-12-15 | E. I. Du Pont De Nemours And Company | Decor paper comprising self-dispersing pigments |
| US10094069B2 (en) | 2013-01-09 | 2018-10-09 | The Chemours Company Fc, Llc | Process for making a décor paper having improved optical performance |
| JP6240219B2 (ja) | 2013-01-09 | 2017-11-29 | ザ ケマーズ カンパニー ティーティー リミテッド ライアビリティ カンパニー | 処理済無機粒子を含む、光学性能を改善した装飾紙 |
| US9315615B2 (en) | 2013-03-15 | 2016-04-19 | Tronox Llc | Titanium dioxide pigment and manufacturing method |
| US9353266B2 (en) | 2013-03-15 | 2016-05-31 | Tronox Llc | Process for manufacturing titanium dioxide pigments using ultrasonication |
| US10125219B2 (en) | 2014-10-30 | 2018-11-13 | Tronox Llc | Titanium dioxide pigment and manufacturing method |
| US9745405B2 (en) | 2015-04-20 | 2017-08-29 | Tronox Llc | Polymer, polymer modified titanium dioxide pigment, and method of forming a pigmented paint formulation |
| TW202307111A (zh) | 2021-08-10 | 2023-02-16 | 美商科慕Fc有限責任公司 | 用於修改聚合物結晶度之經處理之無機粒子 |
| CN114920614B (zh) * | 2022-04-28 | 2023-04-18 | 西安近代化学研究所 | 一种高燃烧效率的包覆二氧化钛的硼燃料及溶胶凝胶法制备方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL241242A (es) * | 1958-07-15 | |||
| NL130649C (es) * | 1965-10-01 | |||
| US3856929A (en) * | 1972-08-25 | 1974-12-24 | Du Pont | PRODUCTION OF ANATASE TiO{11 {11 BY THE CHLORIDE PROCESS |
| US4214913A (en) * | 1979-03-05 | 1980-07-29 | E. I. Du Pont De Nemours And Company | Process for producing rutile TiO2 |
| GB9216933D0 (en) * | 1992-08-10 | 1992-09-23 | Tioxide Group Services Ltd | Oxidation of titanium tetrachloride |
| US5562764A (en) * | 1994-06-28 | 1996-10-08 | E. I. Du Pont De Nemours And Company | Process for preparing improved TIO2 by silicon halide addition |
| US5698177A (en) * | 1994-08-31 | 1997-12-16 | University Of Cincinnati | Process for producing ceramic powders, especially titanium dioxide useful as a photocatalyst |
| TW370552B (en) * | 1994-11-09 | 1999-09-21 | Du Pont | Process for making rutile titanium dioxide pigment comprising coated titanium dioxide particles |
| WO1996036441A1 (en) * | 1995-05-17 | 1996-11-21 | Kemira Pigments, Inc. | COATING OF TiO2 PIGMENT BY GAS-PHASE AND SURFACE REACTIONS |
| US5730795A (en) * | 1996-09-24 | 1998-03-24 | E. I. Du Pont De Nemours And Company | Process for manufacturing titanium dioxide pigment having a hydrous oxide coating using a media mill |
| US5728205A (en) * | 1996-12-11 | 1998-03-17 | E. I. Du Pont De Nemours And Company | Process for the addition of boron in a TiO2 manufacturing process |
-
1997
- 1997-12-23 US US08/997,678 patent/US5922120A/en not_active Expired - Lifetime
-
1998
- 1998-12-21 DE DE69802115T patent/DE69802115T2/de not_active Expired - Lifetime
- 1998-12-21 BR BR9814223-2A patent/BR9814223A/pt not_active Application Discontinuation
- 1998-12-21 CA CA002309553A patent/CA2309553C/en not_active Expired - Lifetime
- 1998-12-21 EP EP98964176A patent/EP1042408B1/en not_active Expired - Lifetime
- 1998-12-21 ES ES98964176T patent/ES2164470T3/es not_active Expired - Lifetime
- 1998-12-21 JP JP2000525490A patent/JP3631138B2/ja not_active Expired - Lifetime
- 1998-12-21 WO PCT/US1998/027156 patent/WO1999032562A1/en not_active Ceased
- 1998-12-21 AU AU19355/99A patent/AU750442B2/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| JP2001527114A (ja) | 2001-12-25 |
| AU750442B2 (en) | 2002-07-18 |
| BR9814223A (pt) | 2000-10-03 |
| EP1042408A1 (en) | 2000-10-11 |
| CA2309553C (en) | 2007-12-18 |
| DE69802115T2 (de) | 2002-06-06 |
| US5922120A (en) | 1999-07-13 |
| JP3631138B2 (ja) | 2005-03-23 |
| EP1042408B1 (en) | 2001-10-17 |
| DE69802115D1 (de) | 2001-11-22 |
| AU1935599A (en) | 1999-07-12 |
| CA2309553A1 (en) | 1999-07-01 |
| WO1999032562A1 (en) | 1999-07-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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