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WO2011128137A3 - Réacteur immergé - Google Patents

Réacteur immergé Download PDF

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Publication number
WO2011128137A3
WO2011128137A3 PCT/EP2011/052334 EP2011052334W WO2011128137A3 WO 2011128137 A3 WO2011128137 A3 WO 2011128137A3 EP 2011052334 W EP2011052334 W EP 2011052334W WO 2011128137 A3 WO2011128137 A3 WO 2011128137A3
Authority
WO
WIPO (PCT)
Prior art keywords
chlorine dioxide
mixing tube
reaction
water
feed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2011/052334
Other languages
German (de)
English (en)
Other versions
WO2011128137A2 (fr
Inventor
Johannes Duve
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik Operations GmbH
Original Assignee
Infracor GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Infracor GmbH filed Critical Infracor GmbH
Priority to BR112012026300A priority Critical patent/BR112012026300A2/pt
Priority to SG2012075453A priority patent/SG184548A1/en
Priority to US13/641,576 priority patent/US9206063B2/en
Priority to ES11704969T priority patent/ES2870586T3/es
Priority to EP11704969.2A priority patent/EP2558192B1/fr
Priority to PL11704969T priority patent/PL2558192T3/pl
Priority to DK11704969.2T priority patent/DK2558192T3/da
Priority to JP2013504180A priority patent/JP5850913B2/ja
Priority to CA2795979A priority patent/CA2795979A1/fr
Publication of WO2011128137A2 publication Critical patent/WO2011128137A2/fr
Publication of WO2011128137A3 publication Critical patent/WO2011128137A3/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/72—Treatment of water, waste water, or sewage by oxidation
    • C02F1/76—Treatment of water, waste water, or sewage by oxidation with halogens or compounds of halogens
    • C02F1/763—Devices for the addition of such compounds in gaseous form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20—Mixing gases with liquids
    • B01F23/23—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/232—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles
    • B01F23/2323—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles by circulating the flow in guiding constructions or conduits
    • B01F23/23231—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles by circulating the flow in guiding constructions or conduits being at least partially immersed in the liquid, e.g. in a closed circuit
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20—Mixing gases with liquids
    • B01F23/23—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/237—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media
    • B01F23/2376—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media characterised by the gas being introduced
    • B01F23/23763—Chlorine or chlorine containing gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/45—Mixing liquids with liquids; Emulsifying using flow mixing
    • B01F23/454—Mixing liquids with liquids; Emulsifying using flow mixing by injecting a mixture of liquid and gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30—Injector mixers
    • B01F25/31—Injector mixers in conduits or tubes through which the main component flows
    • B01F25/312—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof
    • B01F25/3124—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof characterised by the place of introduction of the main flow
    • B01F25/31243—Eductor or eductor-type venturi, i.e. the main flow being injected through the venturi with high speed in the form of a jet
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002—Nozzle-type elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B11/00—Oxides or oxyacids of halogens; Salts thereof
    • C01B11/02—Oxides of chlorine
    • C01B11/022—Chlorine dioxide (ClO2)
    • C01B11/023—Preparation from chlorites or chlorates
    • C01B11/024—Preparation from chlorites or chlorates from chlorites
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/72—Treatment of water, waste water, or sewage by oxidation
    • C02F1/76—Treatment of water, waste water, or sewage by oxidation with halogens or compounds of halogens
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • C02F1/685—Devices for dosing the additives
    • C02F1/686—Devices for dosing liquid additives
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/02—Non-contaminated water, e.g. for industrial water supply
    • C02F2103/023—Water in cooling circuits

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Inorganic Chemistry (AREA)
  • Treatment Of Water By Oxidation Or Reduction (AREA)

Abstract

L'invention concerne un dispositif (1) destiné à l'addition de dioxyde de chlore dans de l'eau et comportant une première conduite (5a) pour le transport d'un premier composant réactionnel, une deuxième conduite (5b) pour le transport d'un deuxième composant réactionnel, un tube mélangeur (2) pour mélanger et mettre en réaction les deux composants réactionnels afin d'obtenir du dioxyde de chlore, les deux conduites (5a,5b) débouchant à une des extrémités de ce mélangeur et une chambre d'aspiration (4) étant disposée à l'autre extrémité, chambre dans laquelle de l'eau additionnelle à enrichir en dioxyde de chlore peut être injectée par l'intermédiaire d'une buse (12), le dispositif comportant également une conduite d'évacuation d'eau usée (13) sortant de la chambre d'aspiration (4) et évacuant le liquide en aval. L'invention vise à perfectionner un tel dispositif de manière à ce qu'il soit de conception simple et robuste et à ce qu'il permette l'exécution sans danger de différentes synthèses de dioxyde de chlore à base de deux composants réactionnels. À cet effet, le tube mélangeur (2) est doté d'une d'entrée additionnelle (10) pour la pénétration d'eau additionnelle exempte de composants réactionnels et devant être enrichie en dioxyde de chlore.
PCT/EP2011/052334 2010-04-16 2011-02-17 Réacteur immergé Ceased WO2011128137A2 (fr)

Priority Applications (9)

Application Number Priority Date Filing Date Title
BR112012026300A BR112012026300A2 (pt) 2010-04-16 2011-02-17 aparelho para alimentar dióxido de cloro à água, aparelho para adicionar gás cloro à água e banho de água
SG2012075453A SG184548A1 (en) 2010-04-16 2011-02-17 Immersion reactor
US13/641,576 US9206063B2 (en) 2010-04-16 2011-02-17 Immersion reactor
ES11704969T ES2870586T3 (es) 2010-04-16 2011-02-17 Reactor de inmersión para la adición de cloro gaseoso o dióxido de cloro en agua
EP11704969.2A EP2558192B1 (fr) 2010-04-16 2011-02-17 Réacteur immergé pour l'ajout de chlore gazeux ou de dioxyde de chlore dans l'eau
PL11704969T PL2558192T3 (pl) 2010-04-16 2011-02-17 Reaktor zanurzeniowy do dodawania gazu chlorowego lub dwutlenku chloru do wody
DK11704969.2T DK2558192T3 (da) 2010-04-16 2011-02-17 Nedsænkningsreaktor til tilsætning af chlorgas eller chlordioxid i vand
JP2013504180A JP5850913B2 (ja) 2010-04-16 2011-02-17 浸漬型反応器
CA2795979A CA2795979A1 (fr) 2010-04-16 2011-02-17 Reacteur immerge

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102010027840A DE102010027840A1 (de) 2010-04-16 2010-04-16 Tauchreaktor
DE102010027840.8 2010-04-16

Publications (2)

Publication Number Publication Date
WO2011128137A2 WO2011128137A2 (fr) 2011-10-20
WO2011128137A3 true WO2011128137A3 (fr) 2011-12-15

Family

ID=44584131

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2011/052334 Ceased WO2011128137A2 (fr) 2010-04-16 2011-02-17 Réacteur immergé

Country Status (12)

Country Link
US (1) US9206063B2 (fr)
EP (1) EP2558192B1 (fr)
JP (1) JP5850913B2 (fr)
BR (1) BR112012026300A2 (fr)
CA (1) CA2795979A1 (fr)
DE (2) DE202010017479U1 (fr)
DK (1) DK2558192T3 (fr)
ES (1) ES2870586T3 (fr)
PL (1) PL2558192T3 (fr)
PT (1) PT2558192T (fr)
SG (2) SG184548A1 (fr)
WO (1) WO2011128137A2 (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL2581340T3 (pl) 2011-10-14 2017-08-31 Evonik Degussa Gmbh Ulepszony sposób traktowania wody ditlenkiem chloru
CN110291047A (zh) 2017-02-27 2019-09-27 埃科莱布美国股份有限公司 现场生产二氧化氯的方法
US11130677B2 (en) 2017-03-24 2021-09-28 Ecolab Usa Inc. Low risk chlorine dioxide onsite generation system
AR111541A1 (es) 2017-08-17 2019-07-24 Ecolab Usa Inc Sistema de generación in situ de dióxido de cloro de bajo riesgo
US11970393B2 (en) 2018-07-05 2024-04-30 Ecolab Usa Inc. Decomposition mediation in chlorine dioxide generation systems through sound detection and control
DE102022110015B3 (de) 2022-04-26 2023-08-03 Matthias Weber Vorrichtung und Verfahren zur Herstellung von Chlordioxid

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0024851A1 (fr) * 1979-08-13 1981-03-11 Rio Linda Chemical Company, Incorporated Procédé pour la préparation de dioxyde de chlore
WO2002014216A1 (fr) * 2000-08-11 2002-02-21 Sabre Oxidation Technologies, Inc. Generateur de dioxyde de chlorure
WO2003000586A1 (fr) * 2001-06-25 2003-01-03 Akzo Nobel N.V. Procede de production de dioxyde de chlore
US20050244328A1 (en) * 2002-05-03 2005-11-03 Schmitz Wilfried J Reactor for production of chlorine dioxide, methods of production of same, and related systems and methods of using the reactor
JP2008094662A (ja) * 2006-10-12 2008-04-24 Takimoto Giken Kogyo Kk 配管接続型の二酸化塩素水生成装置
US20080219087A1 (en) * 2005-05-20 2008-09-11 Tronox Llc Fluid Mixing Apparatus and Method
DE102008042424A1 (de) * 2007-12-19 2009-06-25 Infracor Gmbh Verfahren zur Behandlung von Wasser mit Chlordioxid
DE102008049734A1 (de) * 2008-09-30 2010-04-01 Weidner Wassertechnik Gmbh Verfahren und System zur Herstellung einer Chlordioxidlösung

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NL110391C (fr) 1953-04-14
US3862279A (en) 1973-06-26 1975-01-21 Sr Walter Andersen Subsurface aerator and mixer
US4250144A (en) * 1979-06-14 1981-02-10 Fischer & Porter Company Chlorine dioxide generating system
EP0119686A1 (fr) 1983-01-26 1984-09-26 Calgon Corporation Dispositif et procédé de préparation de bioxyde de chlore
US4472256A (en) 1983-07-13 1984-09-18 Hilbig Herbert H Electrolytic pool chlorinator
CA1230464A (fr) 1984-02-22 1987-12-22 W. Howard Rapson Generateur de dioxyde de chlore a faible debit pour le traitement des eaux usees
US4582586A (en) 1985-08-02 1986-04-15 Robert Maddock Chlorine gas injection system for swimming pool
US5204081A (en) * 1991-05-03 1993-04-20 Rio Linda Chemical Co., Ltd. Process for the generation of chlorine dioxide
US6051135A (en) 1996-02-23 2000-04-18 Water Technologies Limited Apparatus for making aqueous chlorine dioxide and apparatus for treating water with aqueous chlorine dioxide
JPH1110164A (ja) 1997-06-25 1999-01-19 Lucky San:Kk 殺菌剤の製法と水の殺菌方法及びそれらに用いられる装置
RU2163882C2 (ru) 1998-06-09 2001-03-10 Акцо Нобель Н.В. Способ получения двуокиси хлора
JP4042025B2 (ja) 2000-11-24 2008-02-06 ダイソー株式会社 二酸化塩素水の製造方法および製造装置
JP2003260468A (ja) 2002-03-11 2003-09-16 Nishihara Environment Technology Inc 消毒装置
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DE102008055016A1 (de) 2008-12-19 2010-07-01 Infracor Gmbh Verfahren zur Behandlung von Wasser und wässrigen Systemen in Rohrleitungen mit Chlordioxid
DE102010027908A1 (de) 2010-04-19 2011-10-20 Infracor Gmbh Rohrreaktor

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0024851A1 (fr) * 1979-08-13 1981-03-11 Rio Linda Chemical Company, Incorporated Procédé pour la préparation de dioxyde de chlore
WO2002014216A1 (fr) * 2000-08-11 2002-02-21 Sabre Oxidation Technologies, Inc. Generateur de dioxyde de chlorure
WO2003000586A1 (fr) * 2001-06-25 2003-01-03 Akzo Nobel N.V. Procede de production de dioxyde de chlore
US20050244328A1 (en) * 2002-05-03 2005-11-03 Schmitz Wilfried J Reactor for production of chlorine dioxide, methods of production of same, and related systems and methods of using the reactor
US20080219087A1 (en) * 2005-05-20 2008-09-11 Tronox Llc Fluid Mixing Apparatus and Method
JP2008094662A (ja) * 2006-10-12 2008-04-24 Takimoto Giken Kogyo Kk 配管接続型の二酸化塩素水生成装置
DE102008042424A1 (de) * 2007-12-19 2009-06-25 Infracor Gmbh Verfahren zur Behandlung von Wasser mit Chlordioxid
DE102008049734A1 (de) * 2008-09-30 2010-04-01 Weidner Wassertechnik Gmbh Verfahren und System zur Herstellung einer Chlordioxidlösung

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Also Published As

Publication number Publication date
ES2870586T3 (es) 2021-10-27
PL2558192T3 (pl) 2021-10-04
CA2795979A1 (fr) 2011-10-20
US20130106003A1 (en) 2013-05-02
WO2011128137A2 (fr) 2011-10-20
DE102010027840A1 (de) 2011-10-20
DE202010017479U1 (de) 2012-02-16
US9206063B2 (en) 2015-12-08
EP2558192B1 (fr) 2021-04-07
BR112012026300A2 (pt) 2016-07-12
EP2558192A2 (fr) 2013-02-20
SG184548A1 (en) 2012-11-29
JP2013527028A (ja) 2013-06-27
SG10201700650TA (en) 2017-03-30
PT2558192T (pt) 2021-05-25
DK2558192T3 (da) 2021-07-05
JP5850913B2 (ja) 2016-02-03

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