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WO2008133205A1 - シリコン結晶素材及びこれを用いたfzシリコン単結晶の製造方法 - Google Patents

シリコン結晶素材及びこれを用いたfzシリコン単結晶の製造方法 Download PDF

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Publication number
WO2008133205A1
WO2008133205A1 PCT/JP2008/057608 JP2008057608W WO2008133205A1 WO 2008133205 A1 WO2008133205 A1 WO 2008133205A1 JP 2008057608 W JP2008057608 W JP 2008057608W WO 2008133205 A1 WO2008133205 A1 WO 2008133205A1
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WO
WIPO (PCT)
Prior art keywords
crystal
silicon
section
furnace
single crystal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/057608
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English (en)
French (fr)
Inventor
Shinji Togawa
Yutaka Shiraishi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumco Techxiv Corp
Original Assignee
Sumco Techxiv Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumco Techxiv Corp filed Critical Sumco Techxiv Corp
Priority to EP08751878A priority Critical patent/EP2143833A4/en
Publication of WO2008133205A1 publication Critical patent/WO2008133205A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02Elements
    • C30B29/06Silicon
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B13/00Single-crystal growth by zone-melting; Refining by zone-melting
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C30B15/20Controlling or regulating
    • C30B15/206Controlling or regulating the thermal history of growing the ingot

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

 CZ法により製造された有転位又は多結晶のシリコン結晶素材であって、FZ法単結晶製造の原料棒として用いられ、クラックや破断が生じることなく、FZ炉内に懸垂保持するための被把持部を有する大口径の有転位又は多結晶のシリコン結晶素材を提供すること。  FZ法によるシリコン単結晶の製造に用いられるシリコン結晶素材であって、CZ法により製造された有転位又は多結晶シリコンであり種結晶部と、この種結晶部から結晶成長した漸次拡径する肩部と、円柱状の直胴部と、漸次縮径する尾部と、を有する。そして、CZ炉内で結晶成長させて炉内から取り出される前に、所定時間かけて所定温度にまで徐冷される徐冷工程を経て製造され、300°C下における残留応力が0.6MPa以下である。
PCT/JP2008/057608 2007-04-24 2008-04-18 シリコン結晶素材及びこれを用いたfzシリコン単結晶の製造方法 Ceased WO2008133205A1 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP08751878A EP2143833A4 (en) 2007-04-24 2008-04-18 SILICON CRYSTAL MATERIAL AND METHOD FOR PRODUCING AN FZ SILICON CRYSTAL WITH THEREWITH

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-113904 2007-04-24
JP2007113904A JP5318365B2 (ja) 2007-04-24 2007-04-24 シリコン結晶素材及びこれを用いたfzシリコン単結晶の製造方法

Publications (1)

Publication Number Publication Date
WO2008133205A1 true WO2008133205A1 (ja) 2008-11-06

Family

ID=39925659

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/057608 Ceased WO2008133205A1 (ja) 2007-04-24 2008-04-18 シリコン結晶素材及びこれを用いたfzシリコン単結晶の製造方法

Country Status (3)

Country Link
EP (1) EP2143833A4 (ja)
JP (1) JP5318365B2 (ja)
WO (1) WO2008133205A1 (ja)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010132470A (ja) * 2008-12-02 2010-06-17 Sumco Techxiv株式会社 Fz法シリコン単結晶の製造方法

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5846071B2 (ja) * 2012-08-01 2016-01-20 信越半導体株式会社 Fz法による半導体単結晶棒の製造方法
CN103147118B (zh) * 2013-02-25 2016-03-30 天津市环欧半导体材料技术有限公司 一种利用直拉区熔法制备太阳能级硅单晶的方法
JP6064675B2 (ja) * 2013-02-28 2017-01-25 信越半導体株式会社 半導体単結晶棒の製造方法
LV15065B (lv) * 2015-05-26 2015-11-20 Anatoly Kravtsov Silīcija beztīģeļa zonas kausēšanas paņēmiens
EP3181734A1 (en) 2015-12-16 2017-06-21 Total Marketing Services Manufacturing method of a silicon single crystal and silicon wafer production facility

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003055089A (ja) 2001-08-02 2003-02-26 Wacker Siltronic Ag フロートゾーン法により製造したシリコン単結晶及びシリコン基板
JP2005281076A (ja) 2004-03-30 2005-10-13 Shin Etsu Handotai Co Ltd シリコン単結晶の製造方法及びシリコン単結晶並びにシリコンウェーハ
JP2005306653A (ja) 2004-04-21 2005-11-04 Shin Etsu Handotai Co Ltd シリコン単結晶の製造方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3333960A1 (de) * 1983-09-20 1985-04-04 Wacker-Chemitronic Gesellschaft für Elektronik-Grundstoffe mbH, 8263 Burghausen Verfahren zur herstellung von versetzungsfreien einkristallstaeben aus silicium
JP2937115B2 (ja) * 1996-03-15 1999-08-23 住友金属工業株式会社 単結晶引き上げ方法
US6379642B1 (en) * 1997-04-09 2002-04-30 Memc Electronic Materials, Inc. Vacancy dominated, defect-free silicon
JPH1179889A (ja) * 1997-07-09 1999-03-23 Shin Etsu Handotai Co Ltd 結晶欠陥が少ないシリコン単結晶の製造方法、製造装置並びにこの方法、装置で製造されたシリコン単結晶とシリコンウエーハ
JP4867173B2 (ja) * 2005-02-07 2012-02-01 株式会社Sumco シリコン結晶の製造方法およびその製造装置

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003055089A (ja) 2001-08-02 2003-02-26 Wacker Siltronic Ag フロートゾーン法により製造したシリコン単結晶及びシリコン基板
JP2005281076A (ja) 2004-03-30 2005-10-13 Shin Etsu Handotai Co Ltd シリコン単結晶の製造方法及びシリコン単結晶並びにシリコンウェーハ
JP2005306653A (ja) 2004-04-21 2005-11-04 Shin Etsu Handotai Co Ltd シリコン単結晶の製造方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP2143833A4 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010132470A (ja) * 2008-12-02 2010-06-17 Sumco Techxiv株式会社 Fz法シリコン単結晶の製造方法

Also Published As

Publication number Publication date
JP5318365B2 (ja) 2013-10-16
JP2008266090A (ja) 2008-11-06
EP2143833A4 (en) 2010-12-22
EP2143833A1 (en) 2010-01-13

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