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WO2008133110A1 - コア－シェル微粒子の製造方法及びそのコア－シェル微粒子の製造に使用される中間体の製造方法 - Google Patents

コア－シェル微粒子の製造方法及びそのコア－シェル微粒子の製造に使用される中間体の製造方法 Download PDF

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Publication number
WO2008133110A1
WO2008133110A1 PCT/JP2008/057348 JP2008057348W WO2008133110A1 WO 2008133110 A1 WO2008133110 A1 WO 2008133110A1 JP 2008057348 W JP2008057348 W JP 2008057348W WO 2008133110 A1 WO2008133110 A1 WO 2008133110A1
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WO
WIPO (PCT)
Prior art keywords
fine particle
core
shell fine
producing
monomer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/057348
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English (en)
French (fr)
Inventor
Masaki Hayashi
Masumi Takamura
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NOF Corp
Original Assignee
NOF Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NOF Corp filed Critical NOF Corp
Priority to US12/525,528 priority Critical patent/US8143327B2/en
Publication of WO2008133110A1 publication Critical patent/WO2008133110A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F4/00—Polymerisation catalysts
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/12—Polymerisation in non-solvents
    • C08F2/16—Aqueous medium
    • C08F2/20—Aqueous medium with the aid of macromolecular dispersing agents
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/12—Polymerisation in non-solvents
    • C08F2/16—Aqueous medium
    • C08F2/22—Emulsion polymerisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/38—Polymerisation using regulators, e.g. chain terminating agents, e.g. telomerisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F257/00—Macromolecular compounds obtained by polymerising monomers on to polymers of aromatic monomers as defined in group C08F12/00
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F257/00—Macromolecular compounds obtained by polymerising monomers on to polymers of aromatic monomers as defined in group C08F12/00
    • C08F257/02—Macromolecular compounds obtained by polymerising monomers on to polymers of aromatic monomers as defined in group C08F12/00 on to polymers of styrene or alkyl-substituted styrenes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F265/00—Macromolecular compounds obtained by polymerising monomers on to polymers of unsaturated monocarboxylic acids or derivatives thereof as defined in group C08F20/00
    • C08F265/04—Macromolecular compounds obtained by polymerising monomers on to polymers of unsaturated monocarboxylic acids or derivatives thereof as defined in group C08F20/00 on to polymers of esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F291/00—Macromolecular compounds obtained by polymerising monomers on to macromolecular compounds according to more than one of the groups C08F251/00 - C08F289/00
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F293/00—Macromolecular compounds obtained by polymerisation on to a macromolecule having groups capable of inducing the formation of new polymer chains bound exclusively at one or both ends of the starting macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F293/00—Macromolecular compounds obtained by polymerisation on to a macromolecule having groups capable of inducing the formation of new polymer chains bound exclusively at one or both ends of the starting macromolecule
    • C08F293/005—Macromolecular compounds obtained by polymerisation on to a macromolecule having groups capable of inducing the formation of new polymer chains bound exclusively at one or both ends of the starting macromolecule using free radical "living" or "controlled" polymerisation, e.g. using a complexing agent
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L51/00—Compositions of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
    • C08L51/003—Compositions of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers grafted on to macromolecular compounds obtained by reactions only involving unsaturated carbon-to-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2438/00—Living radical polymerisation
    • C08F2438/01—Atom Transfer Radical Polymerization [ATRP] or reverse ATRP

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Graft Or Block Polymers (AREA)
  • Polymerisation Methods In General (AREA)

Abstract

コア－シェル微粒子１０は、まず、有機系単分散シード粒子に、架橋性単量体１５～９９質量％及びＡＴＲＰ開始基を有する単量体１～８５質量％を含む単量体混合物を吸収させる。次に、該単量体混合物を重合開始剤により重合させてＡＴＲＰ重合開始基１２を含む単分散架橋微粒子１１よりなるコア層を形成する。得られたコア層に単量体をグラフト重合してシェル層１３を形成する。
PCT/JP2008/057348 2007-04-25 2008-04-15 コア－シェル微粒子の製造方法及びそのコア－シェル微粒子の製造に使用される中間体の製造方法 Ceased WO2008133110A1 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US12/525,528 US8143327B2 (en) 2007-04-25 2008-04-15 Method for producing core-shell fine particle and method for producing intermediate which is used for production of the core-shell fine particle

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-115602 2007-04-25
JP2007115602A JP5493248B2 (ja) 2007-04-25 2007-04-25 コア−シェル微粒子の製造方法及びその中間体の製造方法

Publications (1)

Publication Number Publication Date
WO2008133110A1 true WO2008133110A1 (ja) 2008-11-06

Family

ID=39925568

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/057348 Ceased WO2008133110A1 (ja) 2007-04-25 2008-04-15 コア－シェル微粒子の製造方法及びそのコア－シェル微粒子の製造に使用される中間体の製造方法

Country Status (4)

Country Link
US (1) US8143327B2 (ja)
JP (1) JP5493248B2 (ja)
TW (1) TWI428352B (ja)
WO (1) WO2008133110A1 (ja)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009298989A (ja) * 2008-06-17 2009-12-24 Kao Corp グラフトポリマーの製造方法
JP2017105906A (ja) * 2015-12-08 2017-06-15 株式会社日本触媒 有機ナノ微粒子及び複合粒子

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8877250B2 (en) 2005-12-20 2014-11-04 Bridgestone Corporation Hollow nano-particles and method thereof
WO2010078320A2 (en) * 2008-12-31 2010-07-08 Bridgestone Corporation Core-first nanoparticle formation process, nanoparticle, and composition
US9062144B2 (en) 2009-04-03 2015-06-23 Bridgestone Corporation Hairy polymeric nanoparticles with first and second shell block polymer arms
US9428604B1 (en) 2011-12-30 2016-08-30 Bridgestone Corporation Nanoparticle fillers and methods of mixing into elastomers
US10106699B2 (en) * 2013-02-20 2018-10-23 Wisconsin Alumni Research Foundation Inimer-containing random copolymers and crosslinked copolymer films for dense polymer brush growth
JP6206963B2 (ja) * 2013-03-12 2017-10-04 国立大学法人 千葉大学 有機−無機ハイブリッド粒子の製造方法及び無機中空粒子の製造方法
US9097979B2 (en) 2013-03-13 2015-08-04 Wisconsin Alumni Research Foundation Block copolymer-based mask structures for the growth of nanopatterned polymer brushes
JP6209922B2 (ja) * 2013-09-27 2017-10-11 ダイキン工業株式会社 （メタ）アクリレート系グラフトポリマー及びその製造方法
JP6404592B2 (ja) * 2014-05-07 2018-10-10 旭化成株式会社 遮熱材料
TWI548651B (zh) * 2015-02-10 2016-09-11 長興材料工業股份有限公司 核殼型聚合物粒子及其製造方法
JP6254239B2 (ja) * 2016-02-29 2017-12-27 大日精化工業株式会社 ポリマーの製造方法
WO2017174422A1 (en) 2016-04-06 2017-10-12 Ge Healthcare Bioprocess R&D Ab Chromatography matrix
JP6721495B2 (ja) * 2016-12-05 2020-07-15 大日精化工業株式会社 架橋アクリル微粒子及びその製造方法
JP6245719B1 (ja) 2017-03-24 2017-12-13 大日精化工業株式会社 ポリマーの製造方法
US11999808B2 (en) * 2018-02-27 2024-06-04 Waters Technologies Corporation Polymer particles with a gradient composition and methods of production thereof
US11180665B2 (en) 2020-02-21 2021-11-23 Swimc Llc Stain-blocking polymers, primers, kits, and methods
CN114874095B (zh) * 2021-02-05 2023-07-14 万华化学(四川)有限公司 一种乙酸芳樟酯的制备方法

Citations (2)

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JP2002363205A (ja) * 2001-04-04 2002-12-18 Sekisui Chem Co Ltd 微粒子及び導電性微粒子
JP2004018556A (ja) * 2002-06-12 2004-01-22 Nisshinbo Ind Inc リビング開始種を有するポリマー粒子及びその製造方法

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US5292814A (en) * 1987-04-29 1994-03-08 Ernst Bayer Process for the preparation of monodispersed polymer beads
AU777829B2 (en) * 1999-04-09 2004-11-04 Life Technologies As Process for the preparation of monodisperse polymer particles
SE0202016D0 (sv) * 2002-06-27 2002-06-27 Amersham Biosciences Ab Polymeric Support Having Novel Pore Structures
US7709542B2 (en) * 2007-03-23 2010-05-04 Agency For Science, Technology And Research Proton-exchange composite containing nanoparticles having outer oligomeric ionomer, and methods of forming

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002363205A (ja) * 2001-04-04 2002-12-18 Sekisui Chem Co Ltd 微粒子及び導電性微粒子
JP2004018556A (ja) * 2002-06-12 2004-01-22 Nisshinbo Ind Inc リビング開始種を有するポリマー粒子及びその製造方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009298989A (ja) * 2008-06-17 2009-12-24 Kao Corp グラフトポリマーの製造方法
JP2017105906A (ja) * 2015-12-08 2017-06-15 株式会社日本触媒 有機ナノ微粒子及び複合粒子

Also Published As

Publication number Publication date
TWI428352B (zh) 2014-03-01
US8143327B2 (en) 2012-03-27
JP5493248B2 (ja) 2014-05-14
TW200902562A (en) 2009-01-16
JP2008274006A (ja) 2008-11-13
US20100036055A1 (en) 2010-02-11

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