WO2002068140A1 - Plastic-worked member and production method thereof - Google Patents
Plastic-worked member and production method thereof Download PDFInfo
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- WO2002068140A1 WO2002068140A1 PCT/JP2002/001857 JP0201857W WO02068140A1 WO 2002068140 A1 WO2002068140 A1 WO 2002068140A1 JP 0201857 W JP0201857 W JP 0201857W WO 02068140 A1 WO02068140 A1 WO 02068140A1
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- WIPO (PCT)
- Prior art keywords
- plastic
- working
- member according
- worked
- stopper
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21J—FORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
- B21J1/00—Preparing metal stock or similar ancillary operations prior, during or post forging, e.g. heating or cooling
- B21J1/02—Preliminary treatment of metal stock without particular shaping, e.g. salvaging segregated zones, forging or pressing in the rough
- B21J1/025—Preliminary treatment of metal stock without particular shaping, e.g. salvaging segregated zones, forging or pressing in the rough affecting grain orientation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B1/00—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
- B21B1/38—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling sheets of limited length, e.g. folded sheets, superimposed sheets, pack rolling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21J—FORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
- B21J1/00—Preparing metal stock or similar ancillary operations prior, during or post forging, e.g. heating or cooling
- B21J1/02—Preliminary treatment of metal stock without particular shaping, e.g. salvaging segregated zones, forging or pressing in the rough
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21J—FORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
- B21J5/00—Methods for forging, hammering, or pressing; Special equipment or accessories therefor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D27/00—Treating the metal in the mould while it is molten or ductile ; Pressure or vacuum casting
- B22D27/04—Influencing the temperature of the metal, e.g. by heating or cooling the mould
- B22D27/045—Directionally solidified castings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B1/00—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
- B21B1/02—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling heavy work, e.g. ingots, slabs, blooms, or billets, in which the cross-sectional form is unimportant ; Rolling combined with forging or pressing
- B21B1/026—Rolling
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B3/00—Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
- B21B2003/001—Aluminium or its alloys
Definitions
- the present invention relates to a plastic-worked member obtained through plastic working of an ingot which is produced, by use of a closable mold having a mold cavity which when the mold is closed is partially defined by an end surface of a stopper and a cooling member, through forced- cooling solidification, by use of the cooling member, of molten metal fed via an molten metal inlet; as well as to a production process thereof.
- Metal ingots produced through unidirectional solidification by means of the above technique are free from internal defects, such as cast cavities, shrinkage cavities, pinholes or oxide inclusion, and thus have good quality.
- molten metal is fed into a closable mold, the same amount of molten metal can always teem, thereby eliminating the need for measuring the amount of the molten metal.
- meniscus does not assume a large curvature, there is no risk of significant variation in the size and weight of the ingots.
- the etallographic structure of the resultant ingot differs between two opposing surfaces, one being on the side of the cooling member end surface, where effects of forced-cooling are significant, and the other being on the side of the stopper end surface, where dendrite arm spacing (which denotes a distance between two adjacent secondary branches of dendrite and will hereinafter be referred to as "DAS”) is longer and grain size is larger.
- DAS dendrite arm spacing
- an object of the invention is to provide a plastic-worked member obtained through plastic working of an ingot which is produced through unidirectional solidification of molten metal, the ingot having improved mechanical characteristics on the side of the stopper end surface so as to attain overall uniform mechanical characteristics; as well as to a production process thereof.
- the plastic-worked member according to the present invention is characterized in that a cast ingot produced in a closable mold through unidirectional forced-cooling of molten metal teeming via a molten metal inlet is plastic-worked at percent working equal to or higher than a predetermined level, wherein the forced-cooling is performed by means of a cooling member, and, when the mold is closed with a stopper, an end surface of the stopper serves as a portion of the inner surface of the mold and the cooling member serves as another portion of the inner surface of the mold.
- a production method of the plastic-worked member according to the present invention is characterized by forced-cooling of molten metal teeming via a molten metal inlet into a mold cavity which, when a mold is closed, is partially defined by an end surface of a stopper and by a cooling member to thereby unidirectionally solidify a cast ingot; and plastic-working of the ingot at percent working of at least a predetermined level.
- the percent working equal to or higher than the predetermined level can be attained through single-step or multi-step plastic working of a cast ingot.
- the predetermined level of percent working can be 25% or, when necessary, 50%.
- the plastic working can be partial plastic working performed on the cast ingot or partial plastic working on at least a portion of the cast ingot including a portion on the stopper end surface side.
- the plastic-worked member can serve as an intermediate or final product.
- the plastic working is any one of forging (cold or hot) , forging-elongation swaging, rolling, extrusion, component rolling and rotary forging (rolling processing) .
- the metal is aluminum or aluminum alloy.
- DAS of the metallographic structure as observed on the stopper end surface side is 1.1 to 10.0 times that on the cooling member side.
- the grain size in terms of the metallographic structure as observed on the stopper end surface side is 1.05 to 7 times that on the cooling member side.
- the grain size as observed on the stopper end surface side is at least 1.2 times that observed on the cooling side.
- plastic working through unidirectional solidification of a metal ingot can improve the mechanical characteristics of the member tending to deteriorate on the stopper end surface side to enable increased strength of the entire member and make strength variation uniform.
- Figure 1 is a cross-sectional side view showing the basic structure of a casting apparatus for producing a plastic-worked member of the present invention.
- Figure 2 shows a cast ingot ( Figure 2 (a) ) , a rectangular parallelepiped sample ( Figure 2(b)), and a forged and elongated sample ( Figure 2(c)), respectively, referred to in Example 1.
- Figure 3(a) is a front view of a specimens used in a tensile test, and Figure 3(a) is a side view thereof.
- Figure 4 shows a cast ingot (Figure 4(a)), a rectangular parallelepiped sample ( Figure 4(b)), and a forged and elongated sample ( Figure 4 (c) ) , respectively, referred to in Example 2.
- Figure 5 shows a cast ingot (Figure 5(a)) and a rolled member ( Figure 5(b)), respectively, referred to in Example 3.
- Figure 6 shows a cast ingot (Figure 6(a)) and a cup- shaped forged member ( Figure 6(b)), respectively, referred to in Example 4.
- Figure 1 is a cross-sectional side view showing the basic structure of a casting apparatus 10 for producing the plastic-worked member of the present invention.
- the casting apparatus 10 illustrated in Figure 1 is used to produce metal ingots which serve as raw materials to be subjected to plastic working, such as cold forging, hot forging, closed forging, rolling, extrusion or component rolling, or to produce a variety of castings such as blanks having the shapes of final products (i.e., material for plastic working or metal ingot) .
- Raw materials for producing castings are typically steel and preferably are non-ferrous metal species, such as aluminum, zinc and magnesium, and their alloys.
- the casting apparatus 10 includes a cooling plate 100, a mold 12 and a stopper 13.
- the cooling plate 100 is formed from metal endowed with excellent refractory properties and high thermal conductivity, such as iron, copper or aluminum, or from a refractory material with high thermal conductivity, such as graphite, silicon carbide or Si 3 N 4 .
- the cooling plate 100 has a casing 14 and a spray nozzle 15 on its lower side.
- the casing 14 has a bottom covering the lower surface of the cooling plate 100.
- the spray nozzle 15 for jetting cooling water through jet holes provided at the top of the nozzle is attached to the casing 14, such that a top end of the nozzle 15 has a view of the interior of the casing 14, with the jet holes facing the lower surface of the cooling plate 100.
- the cooling plate 100, casing 14 and spray nozzle 15 are connected, via the casing 14, to an elevator-driving unit not shown, and, when the elevator-driving unit is driven, can be moved upward and downward as a unit.
- the mold 12 is integrally formed of a partition 12a having a diameter smaller than that of the cooling plate 100, a side wall 12b provided along the periphery of the lower surface of the partition 12a and an upper wall 12c provided along the periphery of the upper surface of the partition 12a.
- the mold 12 is fixedly provided in a region above the cooling plate 100, and when the cooling plate 100 moves downward, the bottom of the mold opens, whereas when the cooling plate 100 moves upward, the bottom of the mold is closed to thereby define a mold cavity 16 closed by the partition 12a, the side wall 12b and the cooling plate 100.
- Material for forming the mold 12 is determined in consideration of relevant conditions, such as the raw material of casting 1 to be produced, wettability of the mold material with respect to molten metal l 1 , temperature during use and corrosion resistance, and can be suitably selected from among heat-insulating refractory materials containing as a predominant component calcium silicate (CaSi0 3 ) , calcium oxide (CaO) , silicon dioxide
- Si0 2 aluminum oxide
- Al oxide A1 2 0 3
- magnesium oxide MgO
- refractory materials of single-component or multi-components selected from among silicon nitride, trisilicon tetranitride, boron nitride-containing trisilicon tetranitride, silicon carbide, graphite, boron nitride, titanium dioxide, zirconium oxide, aluminum nitride and a mixture thereof; and metal species such as iron and copper.
- the mold 12 preferably has air passages at appropriate positions of the mold 12 so that the air confined in the cavity 16 can be released upon teeming.
- the mold 12 has a molten metal inlet 101 at the central position of the partition 12a. While the lower section of the molten metal inlet 101 has a uniform inner diameter, the upper section thereof has a funnel shape with an upwardly increasing inner diameter. The angle of elevation of the funnel-shaped portion is 15° to 75°, preferably 30° to 60°.
- the mold 12 employed in the present embodiment is formed of silicon carbide. The position at which the molten metal inlet 101 is placed is not limited to the center of the partition 12a, but may be changed to any position depending on the shape and use of the cast ingot.
- the position of the inlet can be determined by selecting the portion which will not leave such trace (e.g., a portion which will be removed through, for example, cutting) .
- the stopper 13 has a cylindrical body, and its lower end portion has a diameter greater than the inner diameter of the lower section of the molten metal inlet 101 but smaller than the inner diameter of the opening of the funnel-shaped portion. It also has a diameter-decreasing portion 13a and a fit end 13b provided downward from the lower end of the cylindrical body. The outer diameter of the portion 13a gradually decreases downward.
- the fit end 13b also has a cylindrical shape and is formed such that it can be tightly inserted into the lower section of the molten metal inlet 101.
- the stopper 13 is movable upward and downward with its axis coinciding with the center axis of the molten metal inlet 101, and ascends or descends when urged by a driving force transmitted from a stopper-driving unit not shown.
- the material of the stopper 13 is selected from among heat-insulating refractory materials containing as a predominant component calcium silicate (CaSi0 3 ) , calcium oxide (CaO) , silicon dioxide (Si0 2 ) , aluminum oxide (Al 2 0 3 ) or magnesium oxide (MgO) ; or from among non-metallic materials endowed with excellent refractory/heat-insulating properties and mechanical strength, such as silicon carbide, trisilicon tetranitride and mixtures thereof. It is also possible to employ metallic materials which are non-reactive, or only slightly reactive, with the melt 1' of iron, cast steel, etc.
- reference numeral 17 denotes a lid for covering the upper region of the mold 12
- reference numeral 18 denotes an electric furnace connected with the upper wall 12c of the mold 12.
- the elevator-driving unit (not shown) is operated to move the cooling plate 100 upward to thereby form a mold cavity 16 defined by the mold partition 12a, mold side wall 12b and cooling plate 100.
- the stopper-driving unit (not shown) is operated to move the stopper 13 downward until the fit end 13b of the stopper 13 is inserted into and fitted in the lower section of the molten metal inlet 101 and the diameter-decreasing portion 13a of the stopper 13 abuts the corresponding funnel-defining wall of the molten metal inlet 101.
- the molten metal inlet 101 is closed with the stopper 13, and thus the mold cavity 16 is isolated from a reservoir 19 defined by the partition 12a and upper wall 12c of the mold 12.
- the inner walls of the mold 12 are coated with a mold-releasing agent, and in order to prevent chemical reaction with molten metal 1 ' , the stopper
- the electric furnace 18 is operated to thereby supply a predetermined amount of molten metal 1' into the aforementioned reservoir 19. Operation of the electric furnace 18 is performed not only for the purpose of maintaining a predetermined temperature of the molten metal l 1 contained in the reservoir 19, but also for the purpose of preventing heat absorption through the side wall 12b so as to attain an improved effect of unidirectional solidification which will be described hereinbelow.
- the stopper-driving unit is operated to translate the stopper 13 upward and remove the fit end 13b of the stopper 13 from the lower section of the molten metal inlet 101.
- the molten metal inlet 101 is open to establish communication between the reservoir 19 and the mold cavity 16, thereby allowing continuous teeming of molten metal 1' contained in the reservoir 19 into the mold cavity 16 through the molten metal inlet 101 so as to completely fill the cavity.
- the cooling plate 100 is preferably heated to at least 100°C in advance. Any temperature lower than 100°C is not preferable, because generation of a blow defect that is a type of casting defect cannot be prevented. The upper limit of the heating temperature is appropriately about the same as that of the molten metal 1'.
- the cooling plate 100 is preferably coated with a mold-releasing agent in advance. Coarsening the surface of the cooling plate 100 through shot blasting is also effective for preventing blow defects.
- the stopper 13 is again translated downward to close the molten metal inlet 101.
- cooling water is jetted onto the cooling plate 100 through the spray nozzle 15.
- a thermocouple has been inserted in the cooling plate 100 at the position at which molten metal arrives last so as to monitor a change in temperature of the cooling plate 100.
- solidification proceeds such that solidification interface (i.e., interface between molten metal and a solidified portion) gradually moves upward from the cooling plate 100 with unidirectionality of the movement being maintained, preferably without forming a closed region.
- solidification interface i.e., interface between molten metal and a solidified portion
- the cooling plate 100 is translated downward with respect to the mold 12 to release the cast body 1 from the mold 12 onto the cooling plate 100.
- the present embodiment provides cast bodies 1 of a variety of shapes in accordance with the configuration of the mold cavity, wherein upper and lower faces are parallel to each other, the upper face being on the side of the stopper 13, and the lower face being on the side of the cooling plate 100.
- cast bodies 1 of arbitrary shapes can be obtained.
- a combination of the upper and lower faces that are not parallel to each other or a combination of a flat surface and a curved surface may be employed.
- three-dimensionally profile cast bodies having curved surfaces may be produced. In this case, although solidification interface does not necessarily assume a horizontal flat plane, unidirectionality of solidification is maintained, preventing formation of a closed region.
- the cast ingot 1 was produced from aluminum or aluminum alloy, and DAS and grain size of the ingot was observed under a polarizing microscope (magnification: x40 to xlOO) .
- DAS was measured in accordance with the "Procedure of dendrite arm spacing measurement” described in "Light Metal, vol. 38, No. 1, p. 45 (1988)", published by the Light Metal Society, and grain size was measured in accordance with the "Metallography” described in "Light Metal , vol. 33, No. 2, p. Ill (1983)” published by the same Society.
- d2 falls within a range of (1.1 x dl) to (10 x dl), more preferably, (1.1 x dl) to (5.0 x dl) .
- DAS as measured in the vicinity of the bottom surface B is preferably 40 ⁇ m or less.
- a healthy cast ingot having, within an area of 100 mm 2 , no more than one casting defect, such as microporosity or microshrinkage, of 200 ⁇ m or more and no more than 10 microcavities of 50 to 200 ⁇ m.
- one casting defect such as microporosity or microshrinkage
- d2 ' falls within a range of (1.05 x dl ' ) to (7 x dl') / more preferably, (1.05 x dl ' ) to (5 x dl ' ) .
- grain size dl ' on the side of the bottom surface B is 100 ⁇ m or less on average.
- cast ingots having a variety of shapes are produced by use of a casting apparatus having the aforementioned structure designed to attain unidirectional solidification of molten metal (i.e., a unidirectional solidification casting apparatus), and the thus-produced ingots are subjected to plastic working, which improves mechanical characteristics of each ingot, particularly those of a portion in the vicinity of the stopper, thereby eliminating variation in mechanical characteristics of the ingot and attaining uniform mechanical characteristics throughout the ingot.
- a casting apparatus having the aforementioned structure designed to attain unidirectional solidification of molten metal i.e., a unidirectional solidification casting apparatus
- plastic working refers to all possible processes that impart to a material intended shapes and properties through plastic deformation of the material.
- plastic working include, but are not limited to, forging (cold or hot) , forging-elongation swaging, rolling, extrusion, component rolling and rotary forging.
- Percent working K of plastic working is (height reduced by deformation) ⁇ (initial height) x 100 (%) for the case of swaging or similar working, and (cross-sectional area reduced by deformation) ⁇ (initial cross-sectional area) x 100 (%) for the case of extrusion or similar working.
- JIS2218 alloy melt was prepared in a separate melting apparatus (not illustrated) , and the melt was fed into a unidirectional solidification casting apparatus to cast ingots 11a (Figure 2(a)) having a length of 72 mm, a width of 72 mm and a thickness of 20 mm. Casting conditions are shown in the column "Example 1" of Table 1 below. Before casting, Al - 5 mass% Ti -1 mass% B was incorporated into the molten alloy in such an amount that the resultant alloy had a Ti content of 0.01 mass%, in an attempt to reduce the size of crystal grains. Table 2 below shows the chemical composition of the JIS2218 alloy melt that was subjected to forging.
- Each of the cast ingots 11a was subjected to ho ogenization at 505°C for eight hours. Thereafter, the cast ingot 11a was cut to obtain a rectangular parallelepiped sample lib ( Figure 2(b)) having a width of 40 mm, a length of 65 mm and a thickness of 20 mm.
- the thickness direction of the rectangular parallelepiped sample lib is identical with the solidification direction of the cast ingot 11a.
- the upper surface and lower surface, in a thickness direction, of the rectangular parallelepiped sample lib correspond to the top surface T and bottom surface B of the cast ingot 11a, respectively.
- the forged and elongated sample lie was subjected to intentional aging treatment (T6 treatment) .
- T6 treatment intentional aging treatment
- the sample lie was subjected to solid solution treatment that is the treatment including heating at 505°C for four hours and water quenching, and then subjected to tempering at 190°C for eight hours.
- tensile test pieces lid having a shape as shown in Figure 3 were prepared, through cutting, from the sample lie. The shape of each tensile test piece lid satisfies the dimensional standard (nominal diameter: 0.113 in.) specified by "E8-99, Figure 8" of the ASTM standards.
- the tensile test pieces lid were obtained from positions X, Y, and Z of the forged and elongated sample lie as shown in Figure 2(c). Positions X, Y, and Z correspond to the vicinity of the top surface T of the cast ingot 11a, the center portion of the cast ingot 11a and the vicinity of the bottom surface B of the cast ingot 11a, respectively.
- Cast ingot sample No. 1 (11a) (rectangular parallelepiped sample lib) was subjected to forging- elongation at percent working of 25%, and tensile test pieces lid (Figure 3) were obtained from positions X, Y and Z of the forged and elongated sample lie.
- the tensile test was performed at a test speed of 1 mm/min by use of an autograph produced by Shimadzu Corporation. Three evaluation items are tensile strength, 0.2% yield strength and elongation.
- Example 1 For comparison with Example 1, tensile test pieces were formed as follows. Specifically, ingots identical in shape with those of Example 1 were cast from the same alloy melt as in Example 1 through the same casting process as in Example 1. Each of the cast ingots was subjected to homogenization under the same heat treatment conditions as in Example 1, and a rectangular parallelepiped sample having the same shape as in
- Example 1 was cut from the cast ingot.
- Example 1 Forging-elongation at percent working of 10% was performed through the same process as in Example 1.
- the tensile test pieces were obtained from positions corresponding to the positions X, Y and Z shown in Figure 2(c). Similarly to the case of Example 1, the positions X and Z correspond to the top surface T and the bottom surface B of the ingot, respectively.
- the shape of each tensile test piece, tensile test method and evaluation items are the same as in Example 1.
- Table 4 shows data of tensile strength, 0.2% yield strength and elongation obtained in the tensile test. The test results show that when percent swaging is 25% or more, tensile strength, 0.2% yield strength and elongation are remarkably improved. Particularly, the properties at position X corresponding to the top surface are remarkably improved. When percent swaging is 50% or more, the properties at the top surface T and the center portion are similar to those at the bottom surface B, which generally exhibit more favorable properties as compared with the top surface or center portions.
- Example 1 forging-elongation was performed in a single step. In Example 2, however, it was performed' in a plurality of steps.
- JIS6061 alloy melt was prepared in a separate melting apparatus (not illustrated) , and the melt was fed into a unidirectional solidification casting apparatus to cast ingots 21a ( Figure 4(a)) having a length of 80 mm, a width of
- Al - 5 mass% Ti - 1 mass% B was incorporated into the molten alloy in such an amount that the resultant alloy had a Ti content of 0.01 mass%, in an attempt to reduce the size of crystal grains.
- Table 5 below shows the chemical composition of the JIS6061 alloy melt that was subjected to casting.
- Each of the cast ingots 21a was subjected to homogenization at 540°C for six hours. Thereafter, the cast ingot 21a was cut to obtain a rectangular parallelepiped sample 21b ( Figure 4(b)) having a width of 50 mm, a length of 80 mm and a thickness of 30 mm.
- the thickness direction of the rectangular parallelepiped sample 21b is identical with the solidification direction of the cast ingot 21a.
- the upper surface and lower surface, in a thickness direction, of the rectangular parallelepiped sample 21b correspond to the top surface T and bottom surface B of the cast ingot 21a, respectively.
- the rectangular parallelepiped sample 21b was subjected to hot or cold forging-elongation (swaging) to thereby form a forged and elongated sample 21c ( Figure 4(c)).
- Hot or cold forging-elongation was performed in two steps in a direction represented by arrows Y2 shown in Figure 4 (b) so as to reduce the width (50 mm) of the rectangular parallelepiped sample
- the 25% forging-elongation was performed as follows.
- a metallic soap film serving as a lubrication film was formed on the rectangular parallelepiped sample 21b, and then the resultant sample was subjected to 15% swaging by use of a 400-ton mechanical press. Thereafter, the resultant sample 21b was subjected to annealing at 360°C for four hours, a metallic soap film was again formed on the annealed sample, and the resultant sample was subjected to 10% swaging by use of a press, to thereby attain a total percent swaging of 25%.
- the 50% forging-elongation was performed as follows.
- the rectangular parallelepiped sample 21b was heated to 420°C in a heating furnace, and subsequently, the resultant sample was subjected to two-step swaging, 25% for each step, under the forging-elongation (swaging) conditions shown in Table 3 above, to thereby attain a total percent swaging of 50%.
- the sample underwent cooling to room temperature and re-heating to 420°C .
- the forged and elongated sample 21c was subjected to intentional aging treatment (T6 treatment) . Briefly, the sample 21c was subjected to solid solution treatment, which is the treatment including heating at 540°C for four hours, and then subjected to tempering at 170°C for eight hours.
- T6 treatment intentional aging treatment
- solid solution treatment which is the treatment including heating at 540°C for four hours, and then subjected to tempering at 170°C for eight hours.
- tensile test pieces were obtained from the sample 21c through the same method as in Example 1, and then subjected to a tensile test.
- the test apparatus, test method and evaluation items are the same as those of Example 1.
- Example 2 percent working of 25% or 50% was attained through two-step forging-elongation.
- Example 2A a rectangular parallelepiped sample having the same shape as that of the rectangular parallelepiped sample of Example 2 was cut from a cast ingot obtained under the same conditions as in Example 2, and the rectangular parallelepiped sample was subjected to forging-elongation to thereby form a forged and elongated sample.
- the rectangular parallelepiped sample was heated at 420°C, and then the sample was subjected to swaging in a single step, so as to attain (1) a percent swaging of 25% or (2) a percent swaging of 50%.
- Tensile test pieces were obtained from the resultant forged and elongated sample, and then subjected to a tensile test. The test results were compared with those of Example 2. Other conditions are the same as those of Example 2.
- Table 6 shows data of tensile strength, 0.2% yield strength and elongation obtained in the tensile test in Examples 2 and 2A.
- the test results show that mechanical characteristics of the sample that had undergone forging- elongation in a single step are similar to those of the sample that had undergone forging-elongation in two steps.
- Example 3 as plastic working, rolling was performed in a plurality of steps.
- JIS6061 alloy melt (the same material as used in Example 2) was prepared in a separate melting apparatus (not illustrated) , and the melt was fed into a unidirectional solidification casting apparatus to thereby cast ingots 31a ( Figure 5(a)) having a length of 80 mm, a width of 50 mm and a thickness of 30 mm.
- Casting conditions are shown in the column "Example 3" of Table 1 above.
- Table 5 above shows the chemical composition of the molten alloy that was subjected to casting.
- Each of the cast ingots 31a was subjected to homogenization at 550°C for six hours, and then subjected to rolling.
- the thickness direction and solidification direction of the cast ingot 31a are identical with each other.
- the upper surface and lower surface, in a thickness direction, of the cast ingot 31a correspond to the top surface T and bottom surface B of the cast ingot 31a, respectively.
- Rolling was performed by use of a two-stage rolling apparatus. Before rolling, rolls were pre-heated to 150°C, and the cast ingot 31a was pre-heated to 400°C in a heating furnace. During rolling, the cast ingot was pressed in a direction represented by arrows Y3 shown in Figure 5(a) so as to reduce the thickness (30 mm) . Rolling was performed in five steps until percent working (rolling reduction) K became 25%, such that the rolling direction was the longitudinal direction of the cast ingot. In each step, rolling reduction was 5% with respect to the thickness of the cast ingot before rolling; i.e., the reduction in thickness was 1.5 mm in each step. Rolling was performed without use of a lubricant.
- Example 2 The resultant rolled sample 31b was subjected to T6 treatment in a manner similar to that of Example 2. Subsequently, tensile test pieces were obtained from the rolled sample at positions X, Y and Z shown in Figure 5(b) along a direction parallel to the rolling direction, and were then subjected to a tensile test.
- the test apparatus, test method, and evaluation items are the same as those of Example 1.
- Example 3 percent working of 25% was attained after completion of five-step rolling.
- Example 3A percent working of 25% was attained through forging- elongation in a single step, and the results of Example 3 were compared with those of Example 3A.
- Example 3A a cast ingot obtained under the same conditions as those of Example 3 was heated at 400°C, and subjected to swaging in a single step, so as to attain a percent swaging of 25%.
- tensile test pieces were prepared from the resultant forged and elongated sample, and then subjected to a tensile test. Other conditions are the same as those of Example 3.
- test pieces were subjected to a tensile test.
- Other conditions are the same as those of Example 3.
- Table 7 shows data of tensile strength, 0.2% yield strength and elongation obtained in the tensile test in Examples 3 and 3A and Comparative Example 3.
- the test results show that mechanical characteristics of the sample which had undergone rolling in five steps are substantially similar to those of the sample which had undergone forging- elongation in a single step, and that, in Examples 3 and 3A, mechanical characteristics are clearly improved as compared with the case of Comparative Example 3, in which percent working is 0%.
- Example 4 hot forging was performed as plastic working. Firstly, an Al-Si-Cu-Mg-based alloy melt was prepared in a separate melting apparatus (not illustrated) , and the melt was fed into a unidirectional solidification casting apparatus, to thereby cast columnar ingots 41a
- Table 8 shows the chemical composition of the molten alloy that was subjected to casting.
- Each of the cast ingots 41a was subjected to homogenization at 490°C for eight hours. Thereafter, the cast ingot 41a was placed in a die such that the bottom surface B and top surface T of the cast ingot were the upper surface and lower surface, respectively, and the cast ingot was pressed in a vertical direction by use of a punch and then forged into a cup-shaped forged sample 41b having an outer diameter of 111 mm and an inner diameter of 100 mm as shown in Figure 6(b). The cup-shaped sample was subjected to hot forging under the conditions shown in Table 9 below.
- Samples for observation under a microscope were obtained from the cup-shaped sample 41b forged at percent working K of 50%. The samples were obtained at the following five positions: a position 1 mm inside an inner bottom surface 41p shown in Figure 6(b), a position 3 mm inside the surface 41p, the center between the surface 41p and an outer bottom surface 41q shown in Figure 6(b), a position 3 mm inside the surface 41q and a position 1 mm inside the surface 41q.
- the sample for observation under a microscope was polished and then subjected to measurement of secondary phase crystal grains by use of an image processing apparatus.
- the term "secondary phase crystal grains" used herein refers to eutectic silicon grains and primary silicon crystal grains.
- Cosmozone R500 (product of Nikon Corporation) was used as the image processing apparatus. Eutectic silicon grains and primary silicon crystal grains were observed under a microscope, and eutectic silicon grain sizes and primary silicon crystal grain sizes were measured at 800 and 200 magnifications, respectively.
- the size of a grain refers to the diameter of a circle having the same area as that of the grain; i.e., a circle- equivalent diameter (Heywood diameter) .
- the grain size was obtained by averaging the sizes of grains present in the field of view.
- eutectic silicon grains and primary silicon crystal grains the ratio of the average size of grains at each of the aforementioned positions to the average size of grains at the position 1 mm inside the surface 41p was calculated.
- Example 4 hot forging was performed at percent working of 25% or more, but in Comparative Example 4, it was performed at percent working of 0% or 10%.
- Comparative Example 4 were compared with those of Example 4. Briefly, in Comparative Example 4, cast ingots were produced under the same conditions as employed in Example 4, and each of the cast ingots was subjected to hot forging under the conditions shown in Table 9 above to thereby form a cup- shaped forged sample. The cast ingot (percent working: 0%) and the cup-shaped forged sample (percent working: 10%) were subjected to T6 treatment. Tensile test pieces were obtained from the thus-treated cast ingot and forged sample. The cast ingot was subjected to hot forging under the same conditions as employed in Example 4, except that percent working was varied.
- Example 4 the cast ingot was produced through unidirectional solidification casting.
- Comparative Example 5 a cast ingot was produced by means of a continuous casting method disclosed in, for example, JP-B SHO 54-42847, and the cast ingot was compared with that of Example 4. Briefly, in Comparative Example 5, a continuous cast bar having a diameter of 115 mm was formed from the same molten alloy as employed in Example 4. The cast bar was produced by means of a gas-pressurized hot top casting method disclosed in JP-B SHO 54-42847. The casting conditions are shown in Table 10 below. Table 10
- the thus-produced continuous cast bar (cast ingot) was subjected to homogenization, a surface portion of the cast bar was removed so as to attain a diameter of 110 mm, and the bar was cut into round slices (samples) having a thickness of 50 mm. Thereafter, each of the samples was subjected to hot forging at percent working of 50% to thereby form a cup- shaped sample as shown in Figure 6(b). After the cup-shaped sample was subjected to T6 treatment, tensile test pieces and specimens for observation under a microscope were obtained from the cup-shaped sample.
- Example 4 and Comparative Examples 4 and 5.
- the test results show that, in Comparative Example 4 in which percent working is 0% or 10%, mechanical characteristics (tensile strength,
- percent working K is 75%
- an increase in tensile strength is no longer observed, or the degree of increase in tensile strength is reduced.
- elongation tends to be improved even at percent working of 75%. Particularly, at the top surface, further improvement of elongation is observed.
- Tables 12 and 13 below show the results of measurement of the size of secondary phase crystal grains in Example 4 and Comparative Example 5, respectively.
- Table 12 regarding the size of secondary phase crystal grains of the cup-shaped forged sample 41b obtained in Example 4, the size of eutectic silicon grains tends to increase in a downward direction from the inner bottom surface 41p toward the outer bottom surface 41q, and the ratio of the average size of the eutectic silicon grains at "the position 1 mm inside the outer bottom surface 41q" to that of the grains at "the position 1 mm inside the inner bottom surface 41p" is 2.67.
- the number of primary silicon crystal grains present in the field of view of 0.307 mm 2 increases in a downward direction from the inner bottom surface 1p toward the outer bottom surface 41q, and the average size of the crystal grains increases in the same downward direction.
- the ratio of the average size of the crystal grains at "the position 1 mm inside the outer bottom surface 41q" to that of the grains at "the position 1 mm inside the inner bottom surface 41p" is
- the size of eutectic silicon grains is substantially the same from position to position, and the size of primary crystal grains is also substantially the same from position to position.
- the number of the primary silicon crystal grains present in the field of view of 0.307 mm 2 is substantially the same throughout the aforementioned positions.
- Example 4 and Comparative Example 5 having the aforementioned secondary phase crystal grains was subjected to evaluation of wear resistance at two positions, namely, "the position 1 mm inside the inner bottom surface” and “the position 1 mm inside the outer bottom surface.”
- Test apparatus wear test apparatus TRI-S500 (product of Takachiho Seiki Co., Ltd.)
- Lubricant oil Clean SF-GF2 (product of Castle Oil Co., Ltd.) .. (Temperature: 80°C). . . . .
- Evaluation items were the "amount of loss by wear” and "hardness.” Wear resistance test pieces were obtained from the cup-shaped sample, from which the tensile test pieces were obtained, at the aforementioned two positions. Each of the test pieces was formed into a columnar pin for a wear resistance test, such that the axial direction of the pin was identical with the thickness direction of the bottom portion of the cup-shaped sample. The pin was subjected to T6 treatment serving as heat treatment.
- Hardness test pieces were obtained from positions adjacent to the positions from which the wear resistance test pieces were obtained, and subjected to hardness measurement by use of a Rockwell hardness meter.
- Rockwell B scale HRB was used as a hardness scale.
- Table 14 below shows the results of the wear resistance evaluation test in Example 4 and Comparative Example 5. As shown in Table 14 below, in Comparative Example 5, there is slight difference in the amount of loss by wear of the sample between the positions at the inner bottom surface and the outer bottom surface.
- the test results show that the amount of loss by wear of the sample of Example 4 at "the position 1 mm inside the inner bottom surface” is equal to that of the sample of Comparative Example 5 at the corresponding position, but the amount of loss by wear of the sample of Example 4 at "the position 1 mm inside the outer bottom surface” is remarkably low, and is about 50% that at "the position 1 mm inside the inner bottom surface.” That is to say, the outer bottom surface of the sample of Example 4 exhibits improved wear resistance. Meanwhile, the hardness (HRB) of the test pieces obtained from the sample of Example 4 is substantially equal to that of the test pieces obtained from the sample of
- the plastic-worked sample produced from the cast ingot obtained through unidirectional solidification casting was subjected to measurement of the size of secondary phase crystal grains (eutectic silicon grain size and primary silicon crystal grain size) .
- the ratio of the grain size on the stopper side of the plastic-worked sample to that on the cooling member side of the sample is 1.2 or more.
- Recent lightweight, highly rigid internal combustion engine pistons produced from an aluminum alloy must have high thermal conductivity and wear resistance. Specifically, a piston head portion and a ring groove portion must have wear resistance, low thermal expansion property and thermal shock resistance. Meanwhile, a piston skirt portion and a pin boss portion, which are greatly deformed through plastic working, must have high deformability and mechanical workability as well as high fatigue strength during use.
- the cast ingot 1 (11a, 21a, 31a, 41a) obtained through unidirectional solidification casting is subjected to plastic working to thereby form a plastic-worked member, poor mechanical characteristics of the top surface of the cast ingot can be considerably improved, the strength of the entire member produced from the cast ingot obtained through unidirectional solidification casting can be increased, and variation in strength can be reduced.
- the cast ingot 1 obtained through unidirectional solidification casting having excellent internal quality and low variation in size and weight, has been used as a valuable product.
- the strength of the plastic-worked member produced from the ingot is increased and variation in the strength is reduced, the member can be used as a structural member requiring strength.
- forging-elongation, rolling or hot forging is performed as plastic working.
- any other plastic working for imparting intended shape and properties to a material utilizing material plastic deformation such as cold forging, component rolling, rotary forging (rolling processing) or extrusion.
- the aforementioned plastic-worked member produced by subjecting the cast ingot to plastic working may be a final product, or an intermediate product which requires further processing so as to yield a final product.
- the pressing direction of the cast ingot in the course of plastic working is the width direction or the thickness direction of the ingot.
- the cast ingot is pressed in an arbitrary direction, effects similar to those described above can be obtained.
- the entirety of the cast ingot is subjected to plastic working, but the ingot may be partially subjected to plastic working.
- the entirety of a profile cast ingot produced through unidirectional solidification casting is not necessarily subjected to plastic working, and the profile cast ingot may be partially subjected to plastic working at percent working of 25% or more.
- at least a portion of the cast ingot facing a stopper is preferably subjected to plastic working at percent working of 25% or more, and the percent working of other portions of the ingot may be less than 25%.
- the cast ingot may be subjected to swaging, to thereby subject a portion of the ingot facing a stopper to forging-elongation at percent working of 25% or more.
- the cast ingot i.e., material for plastic working
- the cast ingot can be formed into a material having a shape similar to that of a forging die.
- mechanical characteristics of a portion of the material can be improved.
- a cast ingot fed into a forging die can be made to have a smallest possible volume.
- plastic-worked member particularly the plastic-worked member which has undergone plastic working at percent working of 25% or more and has no variation in mechanical characteristics, is typically employed to manufacture the below-described parts, which should not be construed as limiting the invention parts.
- Examples of automobile parts for suspension and brake systems in which the plastic-worked member is employed include an upper arm, a lower arm, a torsion rod and an ABS pump housing.
- Examples of engine-related automobile parts in which the plastic-worked member is employed include a connecting rod, a GDI body and an internal combustion engine piston.
- Examples of motorcycle parts in which the plastic-worked member is employed include a cushion arm, a bracket and a fork bottom bridge.
- Examples of bicycle parts in which the plastic-worked member is employed include a gear crank.
- the entirety of a cast ingot is subjected to plastic working at percent working of 25% or more, or the cast ingot is partially subjected to plastic working such as forging or forging-elongation at percent working of 25% or more.
- a plastic-worked member is obtained by subjecting to plastic working a cast ingot produced through oriented crystal growth starting at a portion of melt in the vicinity of the cooling member toward an opposite portion of melt in the vicinity of the stopper. Therefore, mechanical characteristics associated with the portion facing the stopper, which have conventionally been unsatisfactory, can be significantly improved, and thus, the strength of plastic- worked member produced via oriented crystal growth can be improved throughout the member with reduced variation in strength.
- Plastic-worked members produced through oriented crystal growth have heretofore been employed as products of high value in use, due to their excellent internal quality and small variation in size and weight. According to the present invention, strength is improved in the entirety of such a plastic-worked member and variation in strength is reduced, and thus, application of the member has been extended to a structural member requiring strength.
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- Engineering & Computer Science (AREA)
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Abstract
Description
Claims
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2002567487A JP2004519331A (en) | 2001-02-28 | 2002-02-28 | Plastically processed member and method of manufacturing the same |
| EP02705057A EP1274527A4 (en) | 2001-02-28 | 2002-02-28 | Plastic-worked member and production method thereof |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001055977 | 2001-02-28 | ||
| JP2001-055977 | 2001-02-28 | ||
| US27650101P | 2001-03-19 | 2001-03-19 | |
| US60/276,501 | 2001-03-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO2002068140A1 true WO2002068140A1 (en) | 2002-09-06 |
Family
ID=26610382
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/JP2002/001857 Ceased WO2002068140A1 (en) | 2001-02-28 | 2002-02-28 | Plastic-worked member and production method thereof |
Country Status (3)
| Country | Link |
|---|---|
| EP (1) | EP1274527A4 (en) |
| JP (1) | JP2004519331A (en) |
| WO (1) | WO2002068140A1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104338749A (en) * | 2014-10-10 | 2015-02-11 | 成都迅德科技有限公司 | Plate material forming device |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04254559A (en) * | 1991-02-06 | 1992-09-09 | Furukawa Electric Co Ltd:The | Manufacturing method of ultra-fine wire |
| JPH09174198A (en) * | 1995-12-27 | 1997-07-08 | Showa Denko Kk | Metallic cast billet for plastic working |
| JPH11336726A (en) * | 1998-05-22 | 1999-12-07 | Mitsubishi Heavy Ind Ltd | Bolt, nut and connector |
-
2002
- 2002-02-28 WO PCT/JP2002/001857 patent/WO2002068140A1/en not_active Ceased
- 2002-02-28 EP EP02705057A patent/EP1274527A4/en not_active Withdrawn
- 2002-02-28 JP JP2002567487A patent/JP2004519331A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04254559A (en) * | 1991-02-06 | 1992-09-09 | Furukawa Electric Co Ltd:The | Manufacturing method of ultra-fine wire |
| JPH09174198A (en) * | 1995-12-27 | 1997-07-08 | Showa Denko Kk | Metallic cast billet for plastic working |
| JPH11336726A (en) * | 1998-05-22 | 1999-12-07 | Mitsubishi Heavy Ind Ltd | Bolt, nut and connector |
Non-Patent Citations (1)
| Title |
|---|
| See also references of EP1274527A4 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104338749A (en) * | 2014-10-10 | 2015-02-11 | 成都迅德科技有限公司 | Plate material forming device |
| CN104338749B (en) * | 2014-10-10 | 2016-03-30 | 成都迅德科技有限公司 | Panel forming apparatus |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2004519331A (en) | 2004-07-02 |
| EP1274527A1 (en) | 2003-01-15 |
| EP1274527A4 (en) | 2006-12-20 |
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