UA88426C2 - Способ производства первичных диаминов - Google Patents
Способ производства первичных диаминовInfo
- Publication number
- UA88426C2 UA88426C2 UAA200814818A UAA200814818A UA88426C2 UA 88426 C2 UA88426 C2 UA 88426C2 UA A200814818 A UAA200814818 A UA A200814818A UA A200814818 A UAA200814818 A UA A200814818A UA 88426 C2 UA88426 C2 UA 88426C2
- Authority
- UA
- Ukraine
- Prior art keywords
- manufacture
- distillation
- diamine
- primary diamines
- hydrogenation
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 150000004985 diamines Chemical class 0.000 title abstract 2
- 238000004821 distillation Methods 0.000 abstract 3
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 abstract 2
- 238000005984 hydrogenation reaction Methods 0.000 abstract 2
- BTGRAWJCKBQKAO-UHFFFAOYSA-N adiponitrile Chemical compound N#CCCCCC#N BTGRAWJCKBQKAO-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- RTWNYYOXLSILQN-UHFFFAOYSA-N methanediamine Chemical compound NCN RTWNYYOXLSILQN-UHFFFAOYSA-N 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J25/00—Catalysts of the Raney type
- B01J25/02—Raney nickel
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
- C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
- C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
- C07C211/09—Diamines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
- C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
- C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
- C07C211/09—Diamines
- C07C211/12—1,6-Diaminohexanes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Данное изобретение касается способа производства первичных диаминов путем гидрогенизации динитрильного соединения при наличии катализатора.Детальнее, представлен способ производства гексаметилендиамина путем гидрогенизации адипонитрила. Способ включает восстановление диамина, образованного с помощью дистилляции в нескольких дистилляционных колоннах, установленных последовательно, и включает удаление тяжелых примесей из второй дистилляции.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0605464A FR2902425B1 (fr) | 2006-06-20 | 2006-06-20 | Procede de fabrication de diamines primaires |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA88426C2 true UA88426C2 (ru) | 2009-10-12 |
Family
ID=37898526
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA200814818A UA88426C2 (ru) | 2006-06-20 | 2007-06-15 | Способ производства первичных диаминов |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US7939691B2 (ru) |
| EP (1) | EP2035365B1 (ru) |
| JP (1) | JP5466942B2 (ru) |
| KR (2) | KR101137279B1 (ru) |
| CN (1) | CN101500980B (ru) |
| BR (1) | BRPI0712621B1 (ru) |
| ES (1) | ES2421196T3 (ru) |
| FR (1) | FR2902425B1 (ru) |
| IN (1) | IN2008CH07021A (ru) |
| RU (1) | RU2430912C2 (ru) |
| TW (1) | TW200806607A (ru) |
| UA (1) | UA88426C2 (ru) |
| WO (1) | WO2007147960A2 (ru) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015038675A1 (en) * | 2013-09-13 | 2015-03-19 | Invista Technologies S.À R.L. | Hydrogenation process for making diamine from dinitrile |
| CN105658618A (zh) * | 2013-09-13 | 2016-06-08 | 因温斯特技术公司 | 催化剂制备和氢化方法 |
| CN104974046B (zh) * | 2014-04-03 | 2017-11-17 | 凯赛(金乡)生物材料有限公司 | 一种戊二胺的纯化方法 |
| CN103936595B (zh) * | 2014-04-30 | 2015-12-02 | 中国天辰工程有限公司 | 一种粗己二胺的精制方法 |
| CN106810455B (zh) * | 2016-12-27 | 2018-04-13 | 河南神马尼龙化工有限责任公司 | 一种高品质精己二胺的生产方法 |
| WO2025119889A1 (en) | 2023-12-07 | 2025-06-12 | Basf Se | Process for manufacturing an aliphatic diamine |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB731819A (en) * | 1951-04-11 | 1955-06-15 | Du Pont | Improvements in or relating to the production of hexamethylene diamine and salts thereof |
| US3017331A (en) * | 1959-04-15 | 1962-01-16 | Chemstrand Corp | Method for the purification of hexamethylenediamine |
| DE19500222A1 (de) * | 1995-01-05 | 1996-07-11 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin |
| DE19548289A1 (de) * | 1995-12-22 | 1997-06-26 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin |
| DE19636766A1 (de) * | 1996-09-10 | 1998-03-12 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
| DE19704612A1 (de) * | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Gewinnung von Hexamethylendiamin aus Hexamethylendiamin enthaltenden Mischungen |
| US5900511A (en) * | 1997-03-28 | 1999-05-04 | E. I. De Pont De Nemours And Company | Process for continuous hydrogenation of adiponitrile |
| DE19812427A1 (de) * | 1998-03-20 | 1999-09-23 | Basf Ag | Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat |
| FR2778661B1 (fr) * | 1998-05-15 | 2000-06-16 | Rhone Poulenc Fibres | Procede de preparation d'aminonitrile et de diamine |
| DE19832529A1 (de) * | 1998-07-20 | 2000-01-27 | Basf Ag | Verbessertes Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
| DE19839338A1 (de) * | 1998-08-28 | 2000-03-02 | Basf Ag | Verbessertes Verfahren zur gleizeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
| DE19839346A1 (de) * | 1998-08-28 | 2000-03-02 | Basf Ag | Verbessertes Verfahren zur Herstellung von Hexamethylendiamin |
| DE10047703A1 (de) * | 2000-09-25 | 2002-04-11 | Basf Ag | Verfahren zur Regenerierung von Katalysatoren |
| FR2826364B1 (fr) * | 2001-06-22 | 2005-01-14 | Rhodia Polyamide Intermediates | Procede d'hemihydrogenation de dinitriles en aminonitriles |
| JP4545738B2 (ja) * | 2003-01-31 | 2010-09-15 | ディーエスエム アイピー アセッツ ビー.ブイ. | ニトリルの接触水素化方法 |
| US6887352B2 (en) * | 2003-03-07 | 2005-05-03 | Invista North America S.A.R.L. | Distillative method for separating hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
| FR2856682B1 (fr) * | 2003-06-27 | 2005-08-26 | Rhodia Polyamide Intermediates | Procede de purification de diamines |
| US7208632B2 (en) * | 2004-09-10 | 2007-04-24 | Invista North America S.A R.L. | Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
| US7468119B2 (en) * | 2004-09-10 | 2008-12-23 | Invista North America S.A.R.L. | Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
-
2006
- 2006-06-20 FR FR0605464A patent/FR2902425B1/fr active Active
-
2007
- 2007-06-15 TW TW096122003A patent/TW200806607A/zh unknown
- 2007-06-15 JP JP2009515909A patent/JP5466942B2/ja not_active Expired - Fee Related
- 2007-06-15 RU RU2009101506/04A patent/RU2430912C2/ru not_active IP Right Cessation
- 2007-06-15 US US12/308,688 patent/US7939691B2/en active Active
- 2007-06-15 WO PCT/FR2007/000998 patent/WO2007147960A2/fr not_active Ceased
- 2007-06-15 EP EP07788893.1A patent/EP2035365B1/fr not_active Revoked
- 2007-06-15 KR KR1020087030927A patent/KR101137279B1/ko not_active Expired - Fee Related
- 2007-06-15 UA UAA200814818A patent/UA88426C2/ru unknown
- 2007-06-15 ES ES07788893T patent/ES2421196T3/es active Active
- 2007-06-15 CN CN2007800228529A patent/CN101500980B/zh active Active
- 2007-06-15 BR BRPI0712621A patent/BRPI0712621B1/pt active IP Right Grant
- 2007-06-15 KR KR1020117031547A patent/KR20120006093A/ko not_active Withdrawn
-
2008
- 2008-12-19 IN IN7021CH2008 patent/IN2008CH07021A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO2007147960A3 (fr) | 2008-02-28 |
| JP5466942B2 (ja) | 2014-04-09 |
| EP2035365B1 (fr) | 2013-04-10 |
| US20100036169A1 (en) | 2010-02-11 |
| KR20120006093A (ko) | 2012-01-17 |
| KR101137279B1 (ko) | 2012-04-20 |
| BRPI0712621B1 (pt) | 2017-04-18 |
| ES2421196T3 (es) | 2013-08-29 |
| CN101500980B (zh) | 2013-03-20 |
| JP2009541277A (ja) | 2009-11-26 |
| BRPI0712621A2 (pt) | 2012-10-16 |
| CN101500980A (zh) | 2009-08-05 |
| IN2008CH07021A (ru) | 2009-03-27 |
| FR2902425A1 (fr) | 2007-12-21 |
| RU2009101506A (ru) | 2010-07-27 |
| US7939691B2 (en) | 2011-05-10 |
| FR2902425B1 (fr) | 2008-07-18 |
| TW200806607A (en) | 2008-02-01 |
| EP2035365A2 (fr) | 2009-03-18 |
| WO2007147960A2 (fr) | 2007-12-27 |
| KR20090017618A (ko) | 2009-02-18 |
| RU2430912C2 (ru) | 2011-10-10 |
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