UA84906C2 - Способ удаления соединений, которые восстанавливают перманганат, из технологического потока карбонилирования метанола - Google Patents
Способ удаления соединений, которые восстанавливают перманганат, из технологического потока карбонилирования метанолаInfo
- Publication number
- UA84906C2 UA84906C2 UAA200609403A UAA200609403A UA84906C2 UA 84906 C2 UA84906 C2 UA 84906C2 UA A200609403 A UAA200609403 A UA A200609403A UA A200609403 A UAA200609403 A UA A200609403A UA 84906 C2 UA84906 C2 UA 84906C2
- Authority
- UA
- Ukraine
- Prior art keywords
- carbonylation process
- methanol carbonylation
- removal
- reducing compounds
- prc
- Prior art date
Links
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 title abstract 6
- 238000000034 method Methods 0.000 title abstract 3
- 230000006315 carbonylation Effects 0.000 title abstract 2
- 238000005810 carbonylation reaction Methods 0.000 title abstract 2
- 150000001875 compounds Chemical class 0.000 title abstract 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 150000001351 alkyl iodides Chemical class 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
- B01D3/324—Tray constructions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
- C07C53/08—Acetic acid
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Раскрыто улучшение способа карбонилирования метанола для получения уксусной кислоты. В частности, раскрыт способ уменьшения образования алкилйодидов и Скарбоновых кислот путем удаления соединений, восстанавливающих перманганат (СВП), из легкой фазы конденсированного потока дистиллята легких фракций, который включает (а) дистилляцию легкой фазы для получения потока дистиллята, обогащенного СВП; и (b) экстракцию третьего потока дистиллята водой в не менее чем два последовательных этапа, и сепарацию из него одного или более водных потоков, которые содержат СВП.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/708,420 US7223886B2 (en) | 2004-03-02 | 2004-03-02 | Removal of permanganate reducing compounds from methanol carbonylation process stream |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA84906C2 true UA84906C2 (ru) | 2008-12-10 |
Family
ID=34911125
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA200609403A UA84906C2 (ru) | 2004-03-02 | 2005-02-24 | Способ удаления соединений, которые восстанавливают перманганат, из технологического потока карбонилирования метанола |
Country Status (20)
| Country | Link |
|---|---|
| US (2) | US7223886B2 (ru) |
| EP (2) | EP3486228B1 (ru) |
| JP (4) | JP2007526310A (ru) |
| KR (2) | KR20060129428A (ru) |
| CN (1) | CN100522916C (ru) |
| AR (1) | AR048247A1 (ru) |
| AU (1) | AU2005219834B2 (ru) |
| BR (1) | BRPI0508438B1 (ru) |
| CA (1) | CA2556998C (ru) |
| ES (2) | ES2714170T3 (ru) |
| MY (2) | MY139400A (ru) |
| NO (1) | NO20064430L (ru) |
| NZ (1) | NZ549260A (ru) |
| PL (1) | PL209551B1 (ru) |
| RS (1) | RS20060494A (ru) |
| RU (1) | RU2372321C2 (ru) |
| TW (2) | TWI433834B (ru) |
| UA (1) | UA84906C2 (ru) |
| WO (1) | WO2005085166A1 (ru) |
| ZA (1) | ZA200607203B (ru) |
Families Citing this family (84)
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| US7208624B2 (en) * | 2004-03-02 | 2007-04-24 | Celanese International Corporation | Process for producing acetic acid |
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| US8710279B2 (en) | 2010-07-09 | 2014-04-29 | Celanese International Corporation | Hydrogenolysis of ethyl acetate in alcohol separation processes |
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| US8530696B2 (en) | 2010-09-24 | 2013-09-10 | Celanese International Corporation | Pump around reactor for production of acetic acid |
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| CN103298860B (zh) | 2010-12-30 | 2016-03-30 | 国际人造丝公司 | 乙酸产物流的纯化 |
| US8884081B2 (en) | 2011-04-26 | 2014-11-11 | Celanese International Corporation | Integrated process for producing acetic acid and alcohol |
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| TW201302684A (zh) | 2011-04-26 | 2013-01-16 | Celanese Int Corp | 由醋酸進料及再循環醋酸乙酯進料生產乙醇之製程 |
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| US9073816B2 (en) | 2011-04-26 | 2015-07-07 | Celanese International Corporation | Reducing ethyl acetate concentration in recycle streams for ethanol production processes |
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| US8754268B2 (en) | 2011-04-26 | 2014-06-17 | Celanese International Corporation | Process for removing water from alcohol mixtures |
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| US9663437B2 (en) | 2011-09-13 | 2017-05-30 | Celanese International Corporation | Production of acetic acid with high conversion rate |
| US8809598B2 (en) | 2011-11-09 | 2014-08-19 | Celanese International Corporation | Producing ethanol using two different streams from acetic acid carbonylation process |
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| WO2013070216A1 (en) | 2011-11-09 | 2013-05-16 | Celanese International Corporation | Integrated ethanol production from methanol via carbonylation and hydrogenation by extracting halides from acetic acid |
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| US8802902B2 (en) | 2011-12-30 | 2014-08-12 | Celanese International Corporation | Pressure driven distillation for ethanol production and recovery from hydrogenation process |
| BR112013007324B1 (pt) | 2012-02-08 | 2020-10-20 | Celanese International Corporation | produção de ácido acético com alta taxa de conversão |
| US8859810B2 (en) * | 2012-08-21 | 2014-10-14 | Celanese International Corporation | Process for recovering permanganate reducing compounds from an acetic acid production process |
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| ES2807618T3 (es) | 2014-11-14 | 2021-02-23 | Celanese Int Corp | Procesos para producir ácido acético a partir de un medio de reacción que tiene bajo contenido de yoduro de etilo |
| US9302975B1 (en) | 2015-07-01 | 2016-04-05 | Celanese International Corporation | Process for flashing a reaction medium |
| WO2016122727A1 (en) | 2015-01-30 | 2016-08-04 | Celanese International Corporation | Processes for producing acetic acid |
| CN107207392B (zh) | 2015-01-30 | 2021-06-08 | 国际人造丝公司 | 生产乙酸的方法 |
| US9487464B2 (en) | 2015-01-30 | 2016-11-08 | Celanese International Corporation | Processes for producing acetic acid |
| US9561994B2 (en) | 2015-01-30 | 2017-02-07 | Celanese International Corporation | Processes for producing acetic acid |
| US9505696B2 (en) * | 2015-02-04 | 2016-11-29 | Celanese International Corporation | Process to control HI concentration in residuum stream |
| US10413840B2 (en) | 2015-02-04 | 2019-09-17 | Celanese International Coporation | Process to control HI concentration in residuum stream |
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| US9382183B1 (en) | 2015-07-01 | 2016-07-05 | Celanese International Corporation | Process for flashing a reaction medium |
| US9302974B1 (en) | 2015-07-01 | 2016-04-05 | Celanese International Corporation | Process for producing acetic acid |
| WO2017057142A1 (ja) * | 2015-09-30 | 2017-04-06 | 株式会社ダイセル | 酢酸の製造方法及び製造装置 |
| CN108137468B (zh) | 2015-10-02 | 2021-04-13 | 国际人造丝公司 | 使用水的再循环生产乙酸的方法 |
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| MX370246B (es) | 2016-10-28 | 2019-12-04 | Daicel Corp | Metodo para la produccion de acido acetico. |
| KR102255683B1 (ko) * | 2017-01-18 | 2021-05-26 | 주식회사 다이셀 | 아세트산의 제조 방법 |
| US10428004B2 (en) | 2017-01-18 | 2019-10-01 | Daicel Corporation | Method for producing acetic acid |
| BR112019012666A2 (pt) * | 2017-02-07 | 2019-11-12 | Daicel Corp | processo para produção de ácido acético, e, método para redução da formação de iodo em um processo. |
| US10710953B2 (en) | 2018-03-23 | 2020-07-14 | Lyondellbasell Acetyls, Llc | Method for purification of GAA |
| WO2019183549A1 (en) | 2018-03-23 | 2019-09-26 | Lyondellbasell Acetyls, Llc | Removal of permanganate reducing compounds from intermediate gaa process streams |
| WO2019186697A1 (ja) | 2018-03-27 | 2019-10-03 | 株式会社ダイセル | 酢酸の製造方法 |
| CN109232223A (zh) * | 2018-11-02 | 2019-01-18 | 江苏索普(集团)有限公司 | 一种合成醋酸的工艺 |
| US10807935B2 (en) | 2018-11-02 | 2020-10-20 | Celanese International Corporation | Process for continuous acetic acid production |
| US20230127564A1 (en) | 2020-04-01 | 2023-04-27 | Celanese International Corporation | Processes for removing and/or reducing permanganate reducing compounds and alkyl iodides |
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| US3769329A (en) * | 1970-03-12 | 1973-10-30 | Monsanto Co | Production of carboxylic acids and esters |
| US5144068A (en) * | 1984-05-03 | 1992-09-01 | Hoechst Celanese Corporation | Methanol carbonylation process |
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| US5001259A (en) * | 1984-05-03 | 1991-03-19 | Hoechst Celanese Corporation | Methanol carbonylation process |
| AU8790391A (en) | 1990-11-19 | 1992-05-21 | Hoechst Celanese Corporation | Removal of carbonyl impurities from a carbonylation process stream |
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| JP3833295B2 (ja) * | 1996-02-29 | 2006-10-11 | 千代田化工建設株式会社 | 酢酸の製造方法 |
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| US6339171B1 (en) * | 1996-10-18 | 2002-01-15 | Celanese International Corporation | Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream |
| US5935155A (en) | 1998-03-13 | 1999-08-10 | John Hopkins University, School Of Medicine | Visual prosthesis and method of using same |
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| US7223883B2 (en) | 2004-03-02 | 2007-05-29 | Celanese International Corporation | Removal of permanganate reducing compounds from methanol carbonylation process stream |
| US7223886B2 (en) * | 2004-03-02 | 2007-05-29 | Celanese International Corporation | Removal of permanganate reducing compounds from methanol carbonylation process stream |
-
2004
- 2004-03-02 US US10/708,420 patent/US7223886B2/en not_active Expired - Lifetime
-
2005
- 2005-02-24 RS RSP-2006/0494A patent/RS20060494A/sr unknown
- 2005-02-24 JP JP2007501855A patent/JP2007526310A/ja active Pending
- 2005-02-24 RU RU2006134649/04A patent/RU2372321C2/ru active
- 2005-02-24 ES ES05723799T patent/ES2714170T3/es not_active Expired - Lifetime
- 2005-02-24 ES ES18210232T patent/ES2859449T3/es not_active Expired - Lifetime
- 2005-02-24 BR BRPI0508438A patent/BRPI0508438B1/pt active IP Right Grant
- 2005-02-24 EP EP18210232.7A patent/EP3486228B1/en not_active Expired - Lifetime
- 2005-02-24 NZ NZ549260A patent/NZ549260A/en not_active IP Right Cessation
- 2005-02-24 ZA ZA200607203A patent/ZA200607203B/en unknown
- 2005-02-24 PL PL381109A patent/PL209551B1/pl not_active IP Right Cessation
- 2005-02-24 UA UAA200609403A patent/UA84906C2/ru unknown
- 2005-02-24 AU AU2005219834A patent/AU2005219834B2/en not_active Ceased
- 2005-02-24 KR KR1020067017672A patent/KR20060129428A/ko not_active Ceased
- 2005-02-24 CN CNB2005800069275A patent/CN100522916C/zh not_active Expired - Lifetime
- 2005-02-24 WO PCT/US2005/006092 patent/WO2005085166A1/en not_active Ceased
- 2005-02-24 EP EP05723799.2A patent/EP1720821B1/en not_active Expired - Lifetime
- 2005-02-24 KR KR1020127011247A patent/KR101233605B1/ko not_active Expired - Lifetime
- 2005-02-24 CA CA2556998A patent/CA2556998C/en not_active Expired - Fee Related
- 2005-02-28 MY MYPI20050821A patent/MY139400A/en unknown
- 2005-02-28 MY MYPI20085092A patent/MY148351A/en unknown
- 2005-03-01 AR ARP050100763A patent/AR048247A1/es not_active Application Discontinuation
- 2005-03-02 TW TW094106279A patent/TWI433834B/zh not_active IP Right Cessation
- 2005-03-02 TW TW100137114A patent/TWI549939B/zh not_active IP Right Cessation
-
2006
- 2006-09-29 NO NO20064430A patent/NO20064430L/no not_active Application Discontinuation
-
2007
- 2007-04-20 US US11/788,455 patent/US8076507B2/en active Active
-
2012
- 2012-12-03 JP JP2012264371A patent/JP2013082715A/ja active Pending
-
2015
- 2015-08-10 JP JP2015158385A patent/JP6506657B2/ja not_active Expired - Lifetime
-
2017
- 2017-08-15 JP JP2017156962A patent/JP6465934B2/ja not_active Expired - Lifetime
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