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UA124928C2 - Спосіб каталітичного гідрування для одержання піразолів - Google Patents

Спосіб каталітичного гідрування для одержання піразолів

Info

Publication number
UA124928C2
UA124928C2 UAA201808830A UAA201808830A UA124928C2 UA 124928 C2 UA124928 C2 UA 124928C2 UA A201808830 A UAA201808830 A UA A201808830A UA A201808830 A UAA201808830 A UA A201808830A UA 124928 C2 UA124928 C2 UA 124928C2
Authority
UA
Ukraine
Prior art keywords
pyrazoles
catalytic hydrogenation
obtaining
acids
obtaining pyrazoles
Prior art date
Application number
UAA201808830A
Other languages
English (en)
Inventor
Ерік Георге Клаубер
Эрик Георге Клаубер
Міхаель Ракк
Михаэль Ракк
Себастіан Зьоргель
Себастиан Зёргель
Біргіт Гоккель
Биргит Гоккель
Роланд Гьотц
Роланд Гётц
Original Assignee
Басф Се
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Басф Се filed Critical Басф Се
Publication of UA124928C2 publication Critical patent/UA124928C2/uk

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42—Platinum
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/16—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of hydrazones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/72—Hydrazones
    • C07C251/74—Hydrazones having doubly-bound carbon atoms of hydrazone groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C251/76—Hydrazones having doubly-bound carbon atoms of hydrazone groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of a saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings linked by a chain containing hetero atoms as chain links
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D403/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00
    • C07D403/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings
    • C07D403/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings linked by a chain containing hetero atoms as chain links

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Винахід стосується каталітичного способу одержання піразолів, який включає стадію циклізації гідразонзаміщених ,,-ненасичених карбонільних сполук за допомогою їх реакції з воднем в реакційній суміші, яка містить як компоненти (а) каталізатор гідрування, (b) кислоту, вибрану з кислот Бренстеда, амонієвих солей кислот Бренстеда і кислот Льюїса, (с) протонний розчинник і (d) апротонний розчинник.
UAA201808830A 2016-02-02 2017-01-25 Спосіб каталітичного гідрування для одержання піразолів UA124928C2 (uk)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16153833 2016-02-02
PCT/EP2017/051524 WO2017133942A1 (en) 2016-02-02 2017-01-25 Catalytic hydrogenation process for preparing pyrazoles

Publications (1)

Publication Number Publication Date
UA124928C2 true UA124928C2 (uk) 2021-12-15

Family

ID=55304873

Family Applications (1)

Application Number Title Priority Date Filing Date
UAA201808830A UA124928C2 (uk) 2016-02-02 2017-01-25 Спосіб каталітичного гідрування для одержання піразолів

Country Status (21)

Country Link
US (1) US10975036B2 (uk)
EP (1) EP3411360B1 (uk)
JP (1) JP6900400B2 (uk)
KR (1) KR102651666B1 (uk)
CN (1) CN108699003B (uk)
AU (1) AU2017216082B2 (uk)
BR (1) BR112018014357B8 (uk)
CA (1) CA3010561C (uk)
CL (1) CL2018002075A1 (uk)
CO (1) CO2018008428A2 (uk)
DK (1) DK3411360T3 (uk)
ES (1) ES2795874T3 (uk)
IL (1) IL260375B (uk)
MX (1) MX384709B (uk)
PE (1) PE20181539A1 (uk)
PL (1) PL3411360T3 (uk)
PT (1) PT3411360T (uk)
RU (1) RU2733958C2 (uk)
UA (1) UA124928C2 (uk)
WO (1) WO2017133942A1 (uk)
ZA (1) ZA201805742B (uk)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2954212C (en) 2014-07-31 2023-09-19 Basf Se Process for preparing pyrazoles
CN107848922A (zh) 2015-05-08 2018-03-27 巴斯夫农业公司 柠檬烯‑4‑醇的制备方法
CN107635982A (zh) 2015-05-08 2018-01-26 巴斯夫农业公司 制备萜品油烯环氧化物的方法
JP6833718B2 (ja) 2015-05-11 2021-02-24 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ ４−アミノ−ピリダジンを製造するための方法
MX2018015765A (es) 2016-06-15 2019-08-29 Basf Agro Bv Proceso para la epoxidacion de un alqueno tretrasustituido.
ES2833202T3 (es) 2016-06-15 2021-06-14 Basf Agro Bv Procedimiento para la epoxidación de un alqueno tetrasustituido
BR112018077104A2 (pt) 2016-07-07 2019-04-02 Basf Se compostos, processo para a preparação de compostos de fórmula i, processo para a preparação de compostos de fórmula iv e uso de compostos da fórmula i
WO2018083040A1 (en) 2016-11-04 2018-05-11 Basf Se Process for purification of pyrazolpyridazines
MX2019005785A (es) 2016-11-17 2019-08-22 Basf Se Proceso para la purificacion de 1-(4-clorofenil)pirazol-3-ol.
CN110234645A (zh) 2017-01-25 2019-09-13 巴斯夫欧洲公司 制备卞型酰胺的方法
CN110431126B (zh) 2017-03-20 2022-12-02 巴斯夫欧洲公司 制备一溴三氯甲烷的方法
EP3704086B1 (en) 2017-11-02 2024-02-21 Basf Se Process for preparing 4-chlorobenzyl propargyl ether

Family Cites Families (18)

* Cited by examiner, † Cited by third party
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JP2007326784A (ja) * 2006-06-06 2007-12-20 Sagami Chem Res Center １−置換−５−フルオロアルキルピラゾール−４−カルボン酸エステルの製造方法
US20110189167A1 (en) 2007-04-20 2011-08-04 Flynn Daniel L Methods and Compositions for the Treatment of Myeloproliferative Diseases and other Proliferative Diseases
CA2684950A1 (en) * 2007-04-20 2008-10-30 Deciphera Pharmaceuticals, Llc Kinase inhibitors useful for the treatment of myleoproliferative diseases and other proliferative diseases
UA103006C2 (uk) 2007-08-27 2013-09-10 Басф Се Піразольні сполуки для боротьби з безхребетними шкідниками
WO2009068652A1 (en) 2007-11-30 2009-06-04 Smithkline Beecham Corporation 2, 6-disubstituted pyridines and 2, 4-disubstituted pyrimidines as soluble guanylate cyclase activators
ES2525807T3 (es) * 2008-05-05 2014-12-30 Basf Se Procedimiento de preparación de compuestos de pirazol sustituidos en las posiciones 1, 3, 4
BRPI0919085B1 (pt) 2008-09-24 2021-05-11 Basf Se métodos não terapêuticos para controlar pragas invertebradas e para proteger material de propagação de plantas e/ou plantas que se desenvolvem dos mesmos, compostos de pirazol ou um sal ou um n-óxido dos mesmos, e, composição agrícola
KR101364869B1 (ko) * 2008-09-24 2014-02-21 바스프 에스이 무척추　해충을　방제하기　위한　피라졸　화합물
EP2236505A1 (de) 2009-04-03 2010-10-06 Bayer CropScience AG Acylierte Aminopyridine und - pyridazine als Insektizide
AR076984A1 (es) 2009-06-08 2011-07-20 Merck Serono Sa Derivados de pirazol oxadiazol
JP6170037B2 (ja) 2011-04-12 2017-07-26 サーメディカル・インコーポレイテッド アブレーション器具
PT2699563T (pt) 2011-04-21 2016-07-14 Basf Se Novos compostos pesticidas de pirazol
JO3407B1 (ar) * 2012-05-31 2019-10-20 Eisai R&D Man Co Ltd مركبات رباعي هيدرو بيرازولو بيريميدين
EP2671873A1 (en) 2012-06-06 2013-12-11 Solvay Sa Method for the cyclization of hydrazinoacrylic acid derivatives
ES2800288T3 (es) 2012-06-20 2020-12-29 Basf Se Mezclas plaguicidas que comprenden un compuesto de pirazol
ES2834959T3 (es) 2012-12-06 2021-06-21 Celgene Quanticel Res Inc Inhibidores de histona desmetilasa
CA2954212C (en) 2014-07-31 2023-09-19 Basf Se Process for preparing pyrazoles
JP6833718B2 (ja) 2015-05-11 2021-02-24 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ ４−アミノ−ピリダジンを製造するための方法

Also Published As

Publication number Publication date
BR112018014357B8 (pt) 2022-09-06
MX2018009453A (es) 2018-09-21
JP2019504883A (ja) 2019-02-21
MX384709B (es) 2025-03-14
BR112018014357A2 (pt) 2018-12-18
CL2018002075A1 (es) 2018-09-14
US10975036B2 (en) 2021-04-13
JP6900400B2 (ja) 2021-07-07
CN108699003B (zh) 2023-02-03
EP3411360B1 (en) 2020-03-11
BR112018014357B1 (pt) 2022-08-16
CA3010561A1 (en) 2017-08-10
WO2017133942A1 (en) 2017-08-10
AU2017216082B2 (en) 2020-12-03
DK3411360T3 (da) 2020-06-08
KR102651666B1 (ko) 2024-03-26
ES2795874T3 (es) 2020-11-25
AU2017216082A1 (en) 2018-07-26
CO2018008428A2 (es) 2018-08-21
CA3010561C (en) 2024-04-16
PT3411360T (pt) 2020-06-01
RU2733958C2 (ru) 2020-10-08
ZA201805742B (en) 2019-11-27
CN108699003A (zh) 2018-10-23
IL260375B (en) 2021-03-25
US20190055200A1 (en) 2019-02-21
KR20180104743A (ko) 2018-09-21
PE20181539A1 (es) 2018-09-26
PL3411360T3 (pl) 2020-08-24
EP3411360A1 (en) 2018-12-12
RU2018130339A3 (uk) 2020-03-19
RU2018130339A (ru) 2020-03-04

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