RU2009112585A - Водный раствор для обработки стального листа с покрытием на основе олова, характеризующегося прекрасными стойкостью к коррозии и адгезией краски, и способ производства обработанного по поверхности стального листа - Google Patents
Водный раствор для обработки стального листа с покрытием на основе олова, характеризующегося прекрасными стойкостью к коррозии и адгезией краски, и способ производства обработанного по поверхности стального листа Download PDFInfo
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- RU2009112585A RU2009112585A RU2009112585/02A RU2009112585A RU2009112585A RU 2009112585 A RU2009112585 A RU 2009112585A RU 2009112585/02 A RU2009112585/02 A RU 2009112585/02A RU 2009112585 A RU2009112585 A RU 2009112585A RU 2009112585 A RU2009112585 A RU 2009112585A
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- steel sheet
- aqueous solution
- organic material
- silica
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- 239000007864 aqueous solution Substances 0.000 title claims abstract 15
- 238000004519 manufacturing process Methods 0.000 title claims 3
- 238000005260 corrosion Methods 0.000 title claims 2
- 230000007797 corrosion Effects 0.000 title claims 2
- 239000003973 paint Substances 0.000 title claims 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract 30
- 229910000831 Steel Inorganic materials 0.000 claims abstract 17
- 239000010959 steel Substances 0.000 claims abstract 17
- 239000000377 silicon dioxide Substances 0.000 claims abstract 15
- 239000011368 organic material Substances 0.000 claims abstract 12
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract 9
- 239000011248 coating agent Substances 0.000 claims abstract 8
- 238000000576 coating method Methods 0.000 claims abstract 8
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract 6
- 239000011651 chromium Substances 0.000 claims abstract 5
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract 4
- 150000001845 chromium compounds Chemical class 0.000 claims abstract 4
- -1 phosphoric acid compound Chemical class 0.000 claims abstract 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract 2
- 125000001931 aliphatic group Chemical group 0.000 claims abstract 2
- 229960005070 ascorbic acid Drugs 0.000 claims abstract 2
- 235000010323 ascorbic acid Nutrition 0.000 claims abstract 2
- 239000011668 ascorbic acid Substances 0.000 claims abstract 2
- 229910052799 carbon Inorganic materials 0.000 claims abstract 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims abstract 2
- JOPOVCBBYLSVDA-UHFFFAOYSA-N chromium(6+) Chemical compound [Cr+6] JOPOVCBBYLSVDA-UHFFFAOYSA-N 0.000 claims abstract 2
- 150000001261 hydroxy acids Chemical class 0.000 claims abstract 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims abstract 2
- 150000002596 lactones Chemical group 0.000 claims abstract 2
- 239000000243 solution Substances 0.000 claims abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 2
- 229910052751 metal Inorganic materials 0.000 claims 5
- 239000002184 metal Substances 0.000 claims 5
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 229910004298 SiO 2 Inorganic materials 0.000 claims 1
- 229910052788 barium Inorganic materials 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- 239000011247 coating layer Substances 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 150000002739 metals Chemical class 0.000 claims 1
- 229910052750 molybdenum Inorganic materials 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 229910052712 strontium Inorganic materials 0.000 claims 1
- 229910052718 tin Inorganic materials 0.000 claims 1
- 229910052721 tungsten Inorganic materials 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 229910052726 zirconium Inorganic materials 0.000 claims 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052681 coesite Inorganic materials 0.000 abstract 1
- 229910052906 cristobalite Inorganic materials 0.000 abstract 1
- 235000012239 silicon dioxide Nutrition 0.000 abstract 1
- 229910052682 stishovite Inorganic materials 0.000 abstract 1
- 229910052905 tridymite Inorganic materials 0.000 abstract 1
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/48—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 not containing phosphates, hexavalent chromium compounds, fluorides or complex fluorides, molybdates, tungstates, vanadates or oxalates
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/48—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 not containing phosphates, hexavalent chromium compounds, fluorides or complex fluorides, molybdates, tungstates, vanadates or oxalates
- C23C22/58—Treatment of other metallic material
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
- C23C22/08—Orthophosphates
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- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
- C23C22/36—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C2222/00—Aspects relating to chemical surface treatment of metallic material by reaction of the surface with a reactive medium
- C23C2222/10—Use of solutions containing trivalent chromium but free of hexavalent chromium
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- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Treatment Of Metals (AREA)
- Other Surface Treatments For Metallic Materials (AREA)
Abstract
1. Водный раствор для обработки стального листа с покрытием на основе Sn, содержащий (А) органический материал, (В) водорастворимое соединение хрома, (С) вододиспергируемый кремнезем и воду, в котором органический материал (А) является по меньшей мере одним из компонентов, выбранных из гидроксикислоты с соотношением гидроксильная группа/карбоксильная группа в молекуле от 3:1 до 10:1, ее лактонной формы и ее оксидного производного, причем водорастворимое соединение хрома (В) не содержит шестивалентный хром, а рН составляет от 0,7 до 6,0. ! 2. Водный раствор для обработки стального листа с покрытием на основе Sn по п.1, в котором органический материал (А) является органическим материалом с числом атомов углерода от 4 до 12. ! 3. Водный раствор для обработки стального листа с покрытием на основе Sn по п.2, в котором органический материал (А) является алифатичеcким. ! 4. Водный раствор для обработки стального листа с покрытием на основе Sn по п.3, в котором органический материал (А) является аскорбиновой кислотой или ее производным. ! 5. Водный раствор для обработки стального листа с покрытием на основе Sn по п.1, в котором вододиспергируемый кремнезем (С) содержит по меньшей мере два типа кремнезема, а именно сферический кремнезем и цепочечный кремнезем при весовом соотношении цепочечный кремнезем/сферический кремнезем (в расчете на SiO2) от 2:8 до 8:2. ! 6. Водный раствор для обработки стального листа с покрытием на основе Sn по п.1, который в качестве дополнительного компонента содержит (D) фосфорную кислоту и/или соединение фосфорной кислоты и при этом суммарное весовое соотношение Cr в обработочном растворе настоящего изобретения к PO4 в фосфорной �
Claims (9)
1. Водный раствор для обработки стального листа с покрытием на основе Sn, содержащий (А) органический материал, (В) водорастворимое соединение хрома, (С) вододиспергируемый кремнезем и воду, в котором органический материал (А) является по меньшей мере одним из компонентов, выбранных из гидроксикислоты с соотношением гидроксильная группа/карбоксильная группа в молекуле от 3:1 до 10:1, ее лактонной формы и ее оксидного производного, причем водорастворимое соединение хрома (В) не содержит шестивалентный хром, а рН составляет от 0,7 до 6,0.
2. Водный раствор для обработки стального листа с покрытием на основе Sn по п.1, в котором органический материал (А) является органическим материалом с числом атомов углерода от 4 до 12.
3. Водный раствор для обработки стального листа с покрытием на основе Sn по п.2, в котором органический материал (А) является алифатичеcким.
4. Водный раствор для обработки стального листа с покрытием на основе Sn по п.3, в котором органический материал (А) является аскорбиновой кислотой или ее производным.
5. Водный раствор для обработки стального листа с покрытием на основе Sn по п.1, в котором вододиспергируемый кремнезем (С) содержит по меньшей мере два типа кремнезема, а именно сферический кремнезем и цепочечный кремнезем при весовом соотношении цепочечный кремнезем/сферический кремнезем (в расчете на SiO2) от 2:8 до 8:2.
6. Водный раствор для обработки стального листа с покрытием на основе Sn по п.1, который в качестве дополнительного компонента содержит (D) фосфорную кислоту и/или соединение фосфорной кислоты и при этом суммарное весовое соотношение Cr в обработочном растворе настоящего изобретения к PO4 в фосфорной кислоте или соединении фосфорной кислоты (D) составляет PO4/Cr = от 1:1 до 3:1.
7. Водный раствор для обработки стального листа с покрытием на основе Sn по п.1, который в качестве дополнительного компонента (Е) содержит металлическую соль, в которой металлом является по меньшей мере один из металлов, выбранных из группы, состоящей из Mg, Ca, Ba, Sr, Co, Ni, Zr, W и Мо, и весовое соотношение металла к хрому металл/Cr составляет от 0,01:1 до 0,5:1.
8. Способ производства стального листа с покрытием на основе Sn, характеризующегося высокой стойкостью к коррозии и прекрасной адгезией краски, включающий в себя нанесение водного раствора для обработки по любому из пп.1-7 на стальной лист с образованным на нем слоем покрытия на основе Sn, содержащего от 1 до 8,8 мас.% Zn и от 91,2 до 99,0 мас.% Sn, и высушивание стального листа.
9. Способ производства по п.8, в котором вес покрытия после сушки (в расчете на металлический хром) составляет от 3 до 100 мг/м2 на одной поверхности стального листа с покрытием на основе Sn.
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| JP2006242221 | 2006-09-07 | ||
| JP2006-242221 | 2006-09-07 |
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| US (1) | US8097306B2 (ru) |
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| CN (1) | CN101512045B (ru) |
| BR (1) | BRPI0716246B1 (ru) |
| CA (1) | CA2662611C (ru) |
| MX (1) | MX2009002399A (ru) |
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| CN103205741B (zh) * | 2012-01-13 | 2016-01-20 | 苏州汉扬精密电子有限公司 | 镁合金钝化液及镁合金表面处理方法 |
| DE102012102082B3 (de) * | 2012-03-13 | 2013-03-21 | Thyssenkrupp Rasselstein Gmbh | Verfahren zur Behandlung eines mit einer Metallbeschichtung versehenen Stahlbands oder -blechs mit einem Nachbehandlungsmittel sowie ein mit einer Metallbeschichtung versehenes Stahlband oder -blech. |
| JP2013249528A (ja) * | 2012-06-04 | 2013-12-12 | Dipsol Chemicals Co Ltd | アルミ変性コロイダルシリカを含有した３価クロム化成処理液 |
| JP6206112B2 (ja) * | 2013-11-19 | 2017-10-04 | 新日鐵住金株式会社 | Ｓｎ系めっき鋼板及び水系処理液 |
| DE112014005596B4 (de) | 2013-12-09 | 2020-08-27 | Angus Chemical Company | Farbzusammensetzung und verfahren zur herstellung einer wasserbasierten farbzusammensetzung |
| JP6265050B2 (ja) * | 2014-05-28 | 2018-01-24 | 新日鐵住金株式会社 | 優れた耐食性と塗料密着性を有する溶融Ｓｎ−Ｚｎめっき鋼板とその製造方法 |
| ES2790576T3 (es) * | 2014-09-24 | 2020-10-28 | Canon Kk | Medio de impresión |
| JP6601283B2 (ja) * | 2016-03-10 | 2019-11-06 | 日本製鉄株式会社 | 燃料タンク |
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-
2007
- 2007-09-06 JP JP2008533222A patent/JP5230428B2/ja active Active
- 2007-09-06 KR KR1020097004622A patent/KR101120230B1/ko not_active Expired - Fee Related
- 2007-09-06 CN CN2007800332698A patent/CN101512045B/zh not_active Expired - Fee Related
- 2007-09-06 WO PCT/JP2007/067772 patent/WO2008029953A1/ja not_active Ceased
- 2007-09-06 BR BRPI0716246-4A patent/BRPI0716246B1/pt not_active IP Right Cessation
- 2007-09-06 CA CA2662611A patent/CA2662611C/en not_active Expired - Fee Related
- 2007-09-06 MX MX2009002399A patent/MX2009002399A/es active IP Right Grant
- 2007-09-06 US US12/310,605 patent/US8097306B2/en not_active Expired - Fee Related
- 2007-09-06 RU RU2009112585/02A patent/RU2417276C2/ru not_active IP Right Cessation
- 2007-09-06 EP EP07807179.2A patent/EP2060660B1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| EP2060660B1 (en) | 2015-02-25 |
| CA2662611C (en) | 2013-02-19 |
| CN101512045B (zh) | 2011-08-17 |
| BRPI0716246A2 (pt) | 2013-09-03 |
| JP5230428B2 (ja) | 2013-07-10 |
| KR101120230B1 (ko) | 2012-03-16 |
| JPWO2008029953A1 (ja) | 2010-01-21 |
| WO2008029953A1 (fr) | 2008-03-13 |
| US20100239773A1 (en) | 2010-09-23 |
| EP2060660A1 (en) | 2009-05-20 |
| US8097306B2 (en) | 2012-01-17 |
| BRPI0716246B1 (pt) | 2018-03-06 |
| EP2060660A4 (en) | 2012-02-01 |
| MX2009002399A (es) | 2009-03-20 |
| KR20090048495A (ko) | 2009-05-13 |
| CA2662611A1 (en) | 2008-03-13 |
| RU2417276C2 (ru) | 2011-04-27 |
| CN101512045A (zh) | 2009-08-19 |
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