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RU2007103618A - METHOD FOR PRODUCING 1-ETHYL-1,2,3,3a, 4,5,6,7,8,9-DECAHYDROCYCLONON [b] ALUMINACYCLOPENTANE - Google Patents

METHOD FOR PRODUCING 1-ETHYL-1,2,3,3a, 4,5,6,7,8,9-DECAHYDROCYCLONON [b] ALUMINACYCLOPENTANE Download PDF

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Publication number
RU2007103618A
RU2007103618A RU2007103618/04A RU2007103618A RU2007103618A RU 2007103618 A RU2007103618 A RU 2007103618A RU 2007103618/04 A RU2007103618/04 A RU 2007103618/04A RU 2007103618 A RU2007103618 A RU 2007103618A RU 2007103618 A RU2007103618 A RU 2007103618A
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RU
Russia
Prior art keywords
ethyl
decahydrocyclonon
aluminacyclopentane
producing
nonadiene
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Application number
RU2007103618/04A
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Russian (ru)
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RU2342393C2 (en
Inventor
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
конов Владимир Анатольевич Дь (RU)
Владимир Анатольевич Дьяконов
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Регина Адиковна Зиннурова (RU)
Регина Адиковна Зиннурова
Галина Аркадьевна Джемилева (RU)
Галина Аркадьевна Джемилева
Рустам Камилевич Тимерханов (RU)
Рустам Камилевич Тимерханов
Original Assignee
Институт Нефтехимиии И Катализа Ран (Ru)
Институт Нефтехимиии И Катализа Ран
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Priority to RU2007103618/04A priority Critical patent/RU2342393C2/en
Publication of RU2007103618A publication Critical patent/RU2007103618A/en
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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Claims (1)

Способ получения 1-этил-1,2,3,3а,4,5,6,7,8,9-декагидроциклонона[b]алюминациклопентана (1),The method of obtaining 1-ethyl-1,2,3,3a, 4,5,6,7,8,9-decahydrocyclonone [b] aluminaminocyclopentane (1),
Figure 00000001
Figure 00000001
 характеризующийся тем, что 1,2-нонадиен подвергают взаимодействию с триэтилалюминием Et3Al в присутствии катализатора цирконацендихлорида Cp2ZrCl2 при мольном соотношении 1,2-нонадиен: Et3Al:Cp2ZrCl2=10:(10-14):(0.4-0.6) в атмосфере аргона при нормальном давлении и комнатной температуре, в гексане, в течение 8-12 ч.characterized in that 1,2-nonadiene is reacted with Et 3 Al triethylaluminium in the presence of a Cp 2 ZrCl 2 catalyst of zirconacene dichloride at a molar ratio of 1,2-nonadiene: Et 3 Al: Cp 2 ZrCl 2 = 10: (10-14): (0.4-0.6) in an argon atmosphere at normal pressure and room temperature, in hexane, for 8-12 hours
RU2007103618/04A 2007-01-30 2007-01-30 METHOD OF OBTAINING 1-ETHYL-1,2,3,3a,4,5,6,7,8,9-DECAHYDROCYCLONONE[b]ALUMINACYCLOPENTANE RU2342393C2 (en)

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RU2007103618/04A RU2342393C2 (en) 2007-01-30 2007-01-30 METHOD OF OBTAINING 1-ETHYL-1,2,3,3a,4,5,6,7,8,9-DECAHYDROCYCLONONE[b]ALUMINACYCLOPENTANE

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RU2007103618/04A RU2342393C2 (en) 2007-01-30 2007-01-30 METHOD OF OBTAINING 1-ETHYL-1,2,3,3a,4,5,6,7,8,9-DECAHYDROCYCLONONE[b]ALUMINACYCLOPENTANE

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RU2007103618A true RU2007103618A (en) 2008-08-10
RU2342393C2 RU2342393C2 (en) 2008-12-27

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2404187C2 (en) * 2008-11-05 2010-11-20 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран exo-PENTACYCLO[5.4.0.02,9.03,6.08,10]UNDECANE-4-SPIRO-1'-(3'-ETHYL-3'-ALUMINIUM)CYCLOPENTANE SYNTHESIS METHOD
RU2420531C2 (en) * 2009-05-18 2011-06-10 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing exo-tricyclo[4,2,1,0 2,5]non-3-ane-spiro-1'-(3'-ethyl-3'-aluminium)cyclopentane

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RU2283315C1 (en) * 2005-03-30 2006-09-10 Институт нефтехимии и катализа РАН Method for preparing 1-chloro-2,3,4,5-tetraalkylaluminacyclopenta-2,4-dienes

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Effective date: 20090131