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RU2007103641A - METHOD FOR PRODUCING 1-ETHYL-2,3,4,5,6,7,8,9-OCTAGHYDRO-1H-CYCLOOCT- [b] -ALUMINACYCLOPENTENE - Google Patents

METHOD FOR PRODUCING 1-ETHYL-2,3,4,5,6,7,8,9-OCTAGHYDRO-1H-CYCLOOCT- [b] -ALUMINACYCLOPENTENE Download PDF

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Publication number
RU2007103641A
RU2007103641A RU2007103641/04A RU2007103641A RU2007103641A RU 2007103641 A RU2007103641 A RU 2007103641A RU 2007103641/04 A RU2007103641/04 A RU 2007103641/04A RU 2007103641 A RU2007103641 A RU 2007103641A RU 2007103641 A RU2007103641 A RU 2007103641A
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RU
Russia
Prior art keywords
ethyl
octaghydro
aluminacyclopentene
cyclooct
producing
Prior art date
Application number
RU2007103641/04A
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Russian (ru)
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RU2342395C2 (en
Inventor
Усеин Меметович Джемилев (RU)
Усеин Меметович Джемилев
конов Владимир Анатольевич Дь (RU)
Владимир Анатольевич Дьяконов
Асхат Габдрахманович Ибрагимов (RU)
Асхат Габдрахманович Ибрагимов
Регина Адиковна Зиннурова (RU)
Регина Адиковна Зиннурова
Галина Аркадьевна Джемилева (RU)
Галина Аркадьевна Джемилева
Лили Фанисовна Галимова (RU)
Лилия Фанисовна Галимова
Original Assignee
Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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Priority to RU2007103641/04A priority Critical patent/RU2342395C2/en
Publication of RU2007103641A publication Critical patent/RU2007103641A/en
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Publication of RU2342395C2 publication Critical patent/RU2342395C2/en

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Claims (1)

Способ получения 1-этил-2,3,4,5,6,7,8,9-октагидро-1Н-циклоокта[b]алюминациклопентена (1),The method of obtaining 1-ethyl-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta [b] aluminaminocyclopentene (1),
Figure 00000001
Figure 00000001
 характеризующийся тем, что циклооктин подвергают взаимодействию с триэтилалюминием Et3Al в присутствии катализатора цирконацендихлорида Cp2ZrCl2 при мольном соотношении циклооктин:Et3Al:Cp2ZrCl2=10:(10-14):(0.8-1.2) в атмосфере аргона при нормальном давлении и комнатной температуре, в гексане, в течение 8-12 ч.characterized in that cyclooctin is reacted with Et 3 Al triethylaluminium in the presence of a Cp 2 ZrCl 2 zirconacene dichloride catalyst with a cyclooctin: Et 3 Al molar ratio: Cp 2 ZrCl 2 = 10: (10-14): (0.8-1.2) in argon atmosphere at normal pressure and room temperature, in hexane, for 8-12 hours
RU2007103641/04A 2007-01-30 2007-01-30 METHOD OF OBTAINING 1-ETHYL-2,3,4,5,6,7,8,9-OCTAHYDRO-1H-CYCLOOCTA-[b]-ALUMINACYCLOPENTANE RU2342395C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2007103641/04A RU2342395C2 (en) 2007-01-30 2007-01-30 METHOD OF OBTAINING 1-ETHYL-2,3,4,5,6,7,8,9-OCTAHYDRO-1H-CYCLOOCTA-[b]-ALUMINACYCLOPENTANE

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Application Number Priority Date Filing Date Title
RU2007103641/04A RU2342395C2 (en) 2007-01-30 2007-01-30 METHOD OF OBTAINING 1-ETHYL-2,3,4,5,6,7,8,9-OCTAHYDRO-1H-CYCLOOCTA-[b]-ALUMINACYCLOPENTANE

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RU2007103641A true RU2007103641A (en) 2008-08-10
RU2342395C2 RU2342395C2 (en) 2008-12-27

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Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2420531C2 (en) 2009-05-18 2011-06-10 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing exo-tricyclo[4,2,1,0 2,5]non-3-ane-spiro-1'-(3'-ethyl-3'-aluminium)cyclopentane

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RU2283315C1 (en) * 2005-03-30 2006-09-10 Институт нефтехимии и катализа РАН Method for preparing 1-chloro-2,3,4,5-tetraalkylaluminacyclopenta-2,4-dienes

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MM4A The patent is invalid due to non-payment of fees

Effective date: 20090131