FR3056584B1 - Procede de fabrication du 1-chloro-2,2-difluoroethane - Google Patents
Procede de fabrication du 1-chloro-2,2-difluoroethane Download PDFInfo
- Publication number
- FR3056584B1 FR3056584B1 FR1659079A FR1659079A FR3056584B1 FR 3056584 B1 FR3056584 B1 FR 3056584B1 FR 1659079 A FR1659079 A FR 1659079A FR 1659079 A FR1659079 A FR 1659079A FR 3056584 B1 FR3056584 B1 FR 3056584B1
- Authority
- FR
- France
- Prior art keywords
- difluoroethane
- chloro
- stream
- manufacture
- trichloroethane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- ATEBGNALLCMSGS-UHFFFAOYSA-N 2-chloro-1,1-difluoroethane Chemical compound FC(F)CCl ATEBGNALLCMSGS-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- UBOXGVDOUJQMTN-UHFFFAOYSA-N 1,1,2-trichloroethane Chemical compound ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 abstract 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 4
- BHNZEZWIUMJCGF-UHFFFAOYSA-N 1-chloro-1,1-difluoroethane Chemical compound CC(F)(F)Cl BHNZEZWIUMJCGF-UHFFFAOYSA-N 0.000 abstract 3
- 239000012074 organic phase Substances 0.000 abstract 2
- 238000000746 purification Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
- C07C19/10—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine
- C07C19/12—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine having two carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La présente invention concerne un procédé de fabrication du 1-chloro-2,2-difluoroéthane à partir du 1,1,2-trichloroéthane comprenant au moins une étape de séparation du 1-chloro-2,2-difluoroéthane de la phase organique produite pendant le procédé ; ladite étape comprend a) une purification de la phase organique obtenue à l'étape (iii) pour former un premier courant comprenant du 1-chloro-difluoroethane et de l'acide fluorhydrique et un second courant comprenant 1,1,2-trichloroethane ; b) l'élimination de l'acide fluorhydrique dudit premier courant pour former un troisième courant comprenant du 1-chloro-difluoroethane ; c) une purification dudit troisième courant comprenant du 1-chloro-difluoroethane.
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1659079A FR3056584B1 (fr) | 2016-09-27 | 2016-09-27 | Procede de fabrication du 1-chloro-2,2-difluoroethane |
| RU2019112250A RU2019112250A (ru) | 2016-09-27 | 2017-09-25 | Способ получения 1-хлор-2,2-дифторэтана |
| EP17780836.7A EP3519378A1 (fr) | 2016-09-27 | 2017-09-25 | Procede de fabrication du 1-chloro-2,2-difluoroethane |
| PCT/FR2017/052559 WO2018060576A1 (fr) | 2016-09-27 | 2017-09-25 | Procede de fabrication du 1-chloro-2,2-difluoroethane |
| MX2019003139A MX2019003139A (es) | 2016-09-27 | 2017-09-25 | Proceso de fabricacion de 1-cloro-2,2-difluoroetano. |
| JP2019515596A JP2019529450A (ja) | 2016-09-27 | 2017-09-25 | 1−クロロ−2,2−ジフルオロエタンを製造するための方法 |
| CN201780059443.XA CN109790089A (zh) | 2016-09-27 | 2017-09-25 | 制备1-氯-2,2-二氟乙烷的方法 |
| US16/333,600 US10640439B2 (en) | 2016-09-27 | 2017-09-25 | Method for producing 1-chloro-2,2-difluoroethane |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1659079 | 2016-09-27 | ||
| FR1659079A FR3056584B1 (fr) | 2016-09-27 | 2016-09-27 | Procede de fabrication du 1-chloro-2,2-difluoroethane |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR3056584A1 FR3056584A1 (fr) | 2018-03-30 |
| FR3056584B1 true FR3056584B1 (fr) | 2020-05-08 |
Family
ID=57485719
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR1659079A Expired - Fee Related FR3056584B1 (fr) | 2016-09-27 | 2016-09-27 | Procede de fabrication du 1-chloro-2,2-difluoroethane |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10640439B2 (fr) |
| EP (1) | EP3519378A1 (fr) |
| JP (1) | JP2019529450A (fr) |
| CN (1) | CN109790089A (fr) |
| FR (1) | FR3056584B1 (fr) |
| MX (1) | MX2019003139A (fr) |
| RU (1) | RU2019112250A (fr) |
| WO (1) | WO2018060576A1 (fr) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101666691B1 (ko) | 2008-11-20 | 2016-10-17 | 얼라인 테크널러지, 인크. | 매개변수를 가지는 부착물을 포함하는 교정 시스템 및 방법 |
| JP6673395B2 (ja) * | 2018-05-07 | 2020-03-25 | ダイキン工業株式会社 | 1,2−ジフルオロエチレン及び/又は1,1,2−トリフルオロエタンの製造方法 |
| JP6908060B2 (ja) * | 2019-01-16 | 2021-07-21 | ダイキン工業株式会社 | 1−クロロ−1,2−ジフルオロエタンを含む共沸又は共沸様組成物 |
| CN119490383A (zh) | 2019-04-10 | 2025-02-21 | 大金工业株式会社 | 含有1-氯-2,2-二氟乙烷和氟化氢的共沸或类共沸组合物 |
| WO2025242610A1 (fr) | 2024-05-21 | 2025-11-27 | Specialty Operations France | Procédé de fabrication de 1-chloro-2,2-difluoroéthane par fluoration de 1,1,2-trichloroéthane et/ou de 1,2-dichloroéthylène en phase gazeuse |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1008575A1 (fr) * | 1998-12-08 | 2000-06-14 | Elf Atochem North America, Inc. | Préparation de 1-chloro-2,2-difluoroethane ("142") |
| ES2674149T3 (es) * | 2011-10-12 | 2018-06-27 | Bayer Intellectual Property Gmbh | Fluoración catalítica en fase gaseosa de 1,1,2-tricloroetano y/o 1,2-dicloroeteno para producir 1-cloro-2,2-difluoroetano |
| FR3014099B1 (fr) * | 2013-12-04 | 2017-01-13 | Arkema France | Procede de fabrication du 1-chloro-2,2,-difluoroethane |
| CN104692998B (zh) * | 2015-02-11 | 2018-06-26 | 巨化集团技术中心 | 1,1-二氟-2-氯乙烷的制备方法 |
| CN104692997B (zh) * | 2015-02-11 | 2017-12-22 | 巨化集团技术中心 | 一种1,1‑二氟‑2‑氯乙烷的制备方法 |
-
2016
- 2016-09-27 FR FR1659079A patent/FR3056584B1/fr not_active Expired - Fee Related
-
2017
- 2017-09-25 JP JP2019515596A patent/JP2019529450A/ja active Pending
- 2017-09-25 CN CN201780059443.XA patent/CN109790089A/zh active Pending
- 2017-09-25 WO PCT/FR2017/052559 patent/WO2018060576A1/fr not_active Ceased
- 2017-09-25 MX MX2019003139A patent/MX2019003139A/es unknown
- 2017-09-25 EP EP17780836.7A patent/EP3519378A1/fr not_active Withdrawn
- 2017-09-25 US US16/333,600 patent/US10640439B2/en not_active Expired - Fee Related
- 2017-09-25 RU RU2019112250A patent/RU2019112250A/ru not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| JP2019529450A (ja) | 2019-10-17 |
| WO2018060576A1 (fr) | 2018-04-05 |
| EP3519378A1 (fr) | 2019-08-07 |
| CN109790089A (zh) | 2019-05-21 |
| FR3056584A1 (fr) | 2018-03-30 |
| US10640439B2 (en) | 2020-05-05 |
| RU2019112250A (ru) | 2020-10-29 |
| MX2019003139A (es) | 2019-06-17 |
| US20200002253A1 (en) | 2020-01-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PLFP | Fee payment |
Year of fee payment: 2 |
|
| PLSC | Publication of the preliminary search report |
Effective date: 20180330 |
|
| PLFP | Fee payment |
Year of fee payment: 3 |
|
| PLFP | Fee payment |
Year of fee payment: 4 |
|
| ST | Notification of lapse |
Effective date: 20210506 |