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FR3046163B1 - Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene. - Google Patents

Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene. Download PDF

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Publication number
FR3046163B1
FR3046163B1 FR1563167A FR1563167A FR3046163B1 FR 3046163 B1 FR3046163 B1 FR 3046163B1 FR 1563167 A FR1563167 A FR 1563167A FR 1563167 A FR1563167 A FR 1563167A FR 3046163 B1 FR3046163 B1 FR 3046163B1
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composition
tetrafluoro
propene
purification
production
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FR1563167A
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FR3046163A1 (fr
Inventor
Abdelatif BABA-AHMED
Dominique Deur-Bert
Bertrand Collier
Laurent Wendlinger
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Arkema France SA
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Arkema France SA
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Priority to FR1563167A priority Critical patent/FR3046163B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to MX2018007596A priority patent/MX2018007596A/es
Priority to EP16809820.0A priority patent/EP3394013A1/fr
Priority to CN201680071234.2A priority patent/CN108368007A/zh
Priority to JP2018532126A priority patent/JP6892862B2/ja
Priority to US16/063,304 priority patent/US10494320B2/en
Priority to PCT/EP2016/080948 priority patent/WO2017108522A1/fr
Publication of FR3046163A1 publication Critical patent/FR3046163A1/fr
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Publication of FR3046163B1 publication Critical patent/FR3046163B1/fr
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • C07C19/03—Chloromethanes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C211/03—Monoamines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C211/09—Diamines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/20—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic unsaturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/20—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic unsaturated carbon skeleton
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/33—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings
    • C07C211/34—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings of a saturated carbon skeleton
    • C07C211/35—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings of a saturated carbon skeleton containing only non-condensed rings
    • C—CHEMISTRY; METALLURGY
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    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/02—Monohydroxylic acyclic alcohols
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    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
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    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/14—Unsaturated ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/04—Saturated compounds containing keto groups bound to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/04—Formic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/04—Formic acid esters
    • C07C69/06—Formic acid esters of monohydroxylic compounds
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    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/12—Acetic acid esters
    • C07C69/14—Acetic acid esters of monohydroxylic compounds
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    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2205/00—Aspects relating to compounds used in compression type refrigeration systems
    • C09K2205/10—Components
    • C09K2205/12—Hydrocarbons
    • C09K2205/126—Unsaturated fluorinated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
    • C09K5/02—Materials undergoing a change of physical state when used
    • C09K5/04—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa
    • C09K5/041—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa for compression-type refrigeration systems
    • C09K5/044—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa for compression-type refrigeration systems comprising halogenated compounds
    • C09K5/045—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa for compression-type refrigeration systems comprising halogenated compounds containing only fluorine as halogen

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

La présente invention concerne un procédé de production et de purification du 2,3,3,3-tétrafluoro -1-propène (1234yf) à partir d'une première composition première composition comprenant du 2,3,3,3-tétrafluoro-1-propène et chlorométhane (40), ledit procédé comprenant les étapes de: (a) mise en contact de ladite première composition avec au moins un agent d'extraction organique pour former une seconde composition ; (b) distillation extractive de ladite seconde composition pour former (i) une troisième composition comprenant ledit agent d'extraction organique et le chlorométhane (40); et (ii) un courant comprenant le 2,3,3,3-tétrafluoro -1-propène (1234yf) ; (c) récupération et séparation de ladite troisième composition, de préférence par distillation, pour former un courant comprenant ledit agent d'extraction organique et un courant comprenant le chlorométhane (40).
FR1563167A 2015-12-23 2015-12-23 Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene. Active FR3046163B1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR1563167A FR3046163B1 (fr) 2015-12-23 2015-12-23 Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene.
EP16809820.0A EP3394013A1 (fr) 2015-12-23 2016-12-14 Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene
CN201680071234.2A CN108368007A (zh) 2015-12-23 2016-12-14 生产和纯化2,3,3,3-四氟-1-丙烯的方法
JP2018532126A JP6892862B2 (ja) 2015-12-23 2016-12-14 ２，３，３，３−テトラフルオロ−１−プロペンを製造及び精製するための方法
MX2018007596A MX2018007596A (es) 2015-12-23 2016-12-14 Proceso de produccion y de purificacion del 2,3,3,3-tetrafluoro-1- propeno.
US16/063,304 US10494320B2 (en) 2015-12-23 2016-12-14 Method for producing and purifying 2,3,3,3-tetrafluoro-1-propene
PCT/EP2016/080948 WO2017108522A1 (fr) 2015-12-23 2016-12-14 Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1563167A FR3046163B1 (fr) 2015-12-23 2015-12-23 Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene.
FR1563167 2015-12-23

Publications (2)

Publication Number Publication Date
FR3046163A1 FR3046163A1 (fr) 2017-06-30
FR3046163B1 true FR3046163B1 (fr) 2019-12-13

Family

ID=55806495

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1563167A Active FR3046163B1 (fr) 2015-12-23 2015-12-23 Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene.

Country Status (7)

Country Link
US (1) US10494320B2 (fr)
EP (1) EP3394013A1 (fr)
JP (1) JP6892862B2 (fr)
CN (1) CN108368007A (fr)
FR (1) FR3046163B1 (fr)
MX (1) MX2018007596A (fr)
WO (1) WO2017108522A1 (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2019220454A1 (fr) 2018-05-16 2019-11-21 Srf Limited Procédé de purification d'une charge oléfinique comprenant 1234 yf

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2447037T3 (es) * 2006-09-05 2014-03-11 E.I. Du Pont De Nemours And Company Procedimiento de fabricación de 2,3,3,3-tetrafluoropropeno
RU2474569C2 (ru) * 2008-02-21 2013-02-10 Е.И.Дюпон Де Немур Энд Компани Способ отделения 1,3,3,3-тетрафторпропена от фтороводорода азеотропной дистилляцией
WO2012011609A1 (fr) * 2010-07-23 2012-01-26 Daikin Industries, Ltd. Procédé de purification du 2,3,3,3-tétrafluoropropène
CN103998405B (zh) * 2011-12-14 2016-06-08 阿克马法国公司 2,3,3,3-四氟丙烯的制备方法
JP5201284B1 (ja) * 2012-03-14 2013-06-05 旭硝子株式会社 ２，３，３，３−テトラフルオロプロペンの製造方法
JP6168068B2 (ja) * 2012-12-27 2017-07-26 旭硝子株式会社 テトラフルオロプロペンの精製方法
WO2015053339A1 (fr) * 2013-10-09 2015-04-16 旭硝子株式会社 Procédé de purification de 2,3,3,3-tétrafluoropropène

Also Published As

Publication number Publication date
WO2017108522A1 (fr) 2017-06-29
JP6892862B2 (ja) 2021-06-23
FR3046163A1 (fr) 2017-06-30
CN108368007A (zh) 2018-08-03
MX2018007596A (es) 2018-09-21
US10494320B2 (en) 2019-12-03
US20180370881A1 (en) 2018-12-27
EP3394013A1 (fr) 2018-10-31
JP2018538316A (ja) 2018-12-27

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