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MX2019013011A - Purificacion de 1,4-bis(4-fenoxibenzoil)benceno mediante filtracion por centrifugacion. - Google Patents

Purificacion de 1,4-bis(4-fenoxibenzoil)benceno mediante filtracion por centrifugacion.

Info

Publication number
MX2019013011A
MX2019013011A MX2019013011A MX2019013011A MX2019013011A MX 2019013011 A MX2019013011 A MX 2019013011A MX 2019013011 A MX2019013011 A MX 2019013011A MX 2019013011 A MX2019013011 A MX 2019013011A MX 2019013011 A MX2019013011 A MX 2019013011A
Authority
MX
Mexico
Prior art keywords
phenoxybenzoylbenzene
bis
centrifugal filtration
lewis acid
purification
Prior art date
Application number
MX2019013011A
Other languages
English (en)
Inventor
Le Guillaume
Jouanneau Julien
Amstutz Jérome
Original Assignee
Arkema France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France filed Critical Arkema France
Publication of MX2019013011A publication Critical patent/MX2019013011A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
    • C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
    • C08G65/4012—Other compound (II) containing a ketone group, e.g. X-Ar-C(=O)-Ar-X for polyetherketones
    • C08G65/4018—(I) or (II) containing halogens other than as leaving group (X)
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
    • C07C45/46—Friedel-Crafts reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/36—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/79—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/76—Ketones containing a keto group bound to a six-membered aromatic ring
    • C07C49/84—Ketones containing a keto group bound to a six-membered aromatic ring containing ether groups, groups, groups, or groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/148—Purification; Separation; Use of additives by treatment giving rise to a chemical modification of at least one compound
    • C07C7/14875—Purification; Separation; Use of additives by treatment giving rise to a chemical modification of at least one compound with organic compounds
    • C07C7/14891—Purification; Separation; Use of additives by treatment giving rise to a chemical modification of at least one compound with organic compounds alcohols
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
    • C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
    • C08G65/4012—Other compound (II) containing a ketone group, e.g. X-Ar-C(=O)-Ar-X for polyetherketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/16—Systems containing only non-condensed rings with a six-membered ring the ring being unsaturated
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G2650/28—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type
    • C08G2650/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type containing oxygen in addition to the ether group
    • C08G2650/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type containing oxygen in addition to the ether group containing ketone groups, e.g. polyarylethylketones, PEEK or PEK
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G2650/62—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the nature of monomer used

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Water Supply & Treatment (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Polyethers (AREA)

Abstract

La invención se refiere a un método para manufacturar el 1,4-bis(4-fenoxibenzoil)benceno, que comprende: - hacer reaccionar el cloruro de tereftaloilo con difenil éter en un solvente de reacción y en la presencia de un ácido de Lewis, con el fin de obtener una mezcla de producto que comprende un complejo de 1,4-bis(4-fenoxibenzoil)benceno-ácido de Lewis; - poner la mezcla de producto en contacto con un solvente prótico, con el fin de obtener una primera fase que contiene el ácido de Lewis y una segunda fase que contiene el 1,4-bis(4-fenoxibenzoil)b enceno; - someter al menos la segunda fase a un paso de separación sólido/líquido mediante filtración por centrifugación, con el fin de recuperar 1,4-bis(4-fenoxibenzoil) benceno sólido.
MX2019013011A 2017-05-18 2018-05-17 Purificacion de 1,4-bis(4-fenoxibenzoil)benceno mediante filtracion por centrifugacion. MX2019013011A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP17305583.1A EP3404013B1 (en) 2017-05-18 2017-05-18 Purification of 1,4-bis (4-phenoxybenzoyl)benzene by centrifugal filtration
PCT/EP2018/063014 WO2018211046A1 (en) 2017-05-18 2018-05-17 Purification of 1,4-bis (4-phenoxybenzoylbenzene) by centrifugal filtration

Publications (1)

Publication Number Publication Date
MX2019013011A true MX2019013011A (es) 2020-02-05

Family

ID=58800757

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019013011A MX2019013011A (es) 2017-05-18 2018-05-17 Purificacion de 1,4-bis(4-fenoxibenzoil)benceno mediante filtracion por centrifugacion.

Country Status (10)

Country Link
US (2) US20210155571A1 (es)
EP (2) EP3404013B1 (es)
JP (1) JP2020520364A (es)
KR (1) KR102406451B1 (es)
CN (1) CN110650939B (es)
BR (1) BR112019023018A2 (es)
CA (1) CA3061560A1 (es)
MX (1) MX2019013011A (es)
RU (1) RU2019141827A (es)
WO (1) WO2018211046A1 (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3404012B1 (en) 2017-05-18 2020-09-09 Arkema France Ripening of 1,4-bis (4-phenoxybenzoyl)benzene
EP3404008B1 (en) 2017-05-16 2020-08-12 Arkema France Method for manufacturing 1,4-bis (4-phenoxybenzoyl)benzene at an elevated temperature
EP3404010B1 (en) 2017-05-16 2020-08-12 Arkema France Method for manufacturing 1,4-bis (4-phenoxybenzoyl)benzene using substantially non-hydrolyzed terephthaloyl chloride
US10793500B2 (en) 2017-05-16 2020-10-06 Arkema France Dissociation of 1,4-bis (4-phenoxybenzoyl)benzene—Lewis acid complex in a protic solvent
EP3404011B1 (en) 2017-05-18 2020-08-26 Arkema France Dissociation of a 1,4-bis(4-phenoxybenzoyl)benzene-lewis acid-complex in an aqueous solution
EP3431522B1 (en) * 2017-07-18 2020-11-18 Arkema France Purification of polyetherketoneketone by centrifugal filtration
EP3438085A1 (en) * 2017-08-04 2019-02-06 Arkema France Process for producing polyether ketone ketone
EP3650433B1 (en) 2018-11-09 2024-04-24 Arkema France Method for manufacturing 1,4-bis (4-phenoxybenzoylbenzene) at an elevated temperature
KR20220028244A (ko) 2020-08-28 2022-03-08 한화솔루션 주식회사 1,4-비스(4-페녹시벤조일)벤젠을 제조하는 방법 및 이에 의해 제조된 1,4-비스(4-페녹시벤조일)벤젠
JP2023151638A (ja) * 2022-03-31 2023-10-16 旭化成株式会社 ポリアリーレンエーテルケトン樹脂及びその製造方法、並びに芳香族ジケトン化合物
CN119371297B (zh) * 2024-12-30 2025-04-11 山东凯盛新材料股份有限公司 1,4-双（4-苯氧基苯甲酰基）苯的合成工艺
CN120025539B (zh) * 2025-04-21 2025-07-18 江苏苏博特新材料股份有限公司 一种高韧性聚醚酮酮聚合物及其制备方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU445643A1 (ru) 1973-01-08 1974-10-05 Институт Высокомолекулярных Соединений Ан Ссср Способ получени 1,4-бис(4-феноксибензоил)бензола
US4816556A (en) 1985-02-22 1989-03-28 E. I. Du Pont De Nemours And Company Ordered polyetherketones
US4716211A (en) 1985-03-11 1987-12-29 Amoco Corporation Slurry process for producing high molecular weight crystalline polyaryletherketones
EP0268112B1 (en) 1986-11-20 1994-03-16 Asahi Kasei Kogyo Kabushiki Kaisha A novel aromatic polyether and a process for producing a polyether
US4826947A (en) * 1987-07-09 1989-05-02 Raychem Corporation Preparation of poly(arylene ether ketones)
US4794155A (en) * 1987-08-26 1988-12-27 The Dow Chemical Company Process for forming arylether polymers
US4835319A (en) * 1987-11-09 1989-05-30 E. I. Du Pont De Nemours And Company Process for the manufacture of 1,4-bis(4-phenoxybenzoyl)benzene with a zeolite catalyst
US4827041A (en) * 1988-03-10 1989-05-02 E. I. Du Pont De Nemours And Company Process for the manufacture of 1,4-bis(4-phenoxybenzoyl)benzene with a perfluorosulfonyl resin catalyst
US4918237A (en) * 1989-03-13 1990-04-17 E. I. Du Pont De Nemours And Company Process for the manufacture of 1,4-bis(4-phenoxybenzoyl)benzene with certain metal-containing catalysts
GB9403944D0 (en) 1994-03-02 1994-04-20 Victrex Manufacturing Ltd Aromatic polymers

Also Published As

Publication number Publication date
US20180334538A1 (en) 2018-11-22
CN110650939B (zh) 2023-07-14
KR20200009038A (ko) 2020-01-29
US10344125B2 (en) 2019-07-09
KR102406451B1 (ko) 2022-06-07
WO2018211046A1 (en) 2018-11-22
CA3061560A1 (en) 2018-11-22
US20210155571A1 (en) 2021-05-27
BR112019023018A2 (pt) 2020-05-19
RU2019141827A (ru) 2021-06-18
CN110650939A (zh) 2020-01-03
EP3404013A1 (en) 2018-11-21
JP2020520364A (ja) 2020-07-09
EP3625204A1 (en) 2020-03-25
EP3404013B1 (en) 2021-10-27

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