CA2391865A1 - Une methode pour recycler des batteries rechargeables usees a polymere et lithium metallique et des materiaux apparentes - Google Patents
Une methode pour recycler des batteries rechargeables usees a polymere et lithium metallique et des materiaux apparentes Download PDFInfo
- Publication number
- CA2391865A1 CA2391865A1 CA002391865A CA2391865A CA2391865A1 CA 2391865 A1 CA2391865 A1 CA 2391865A1 CA 002391865 A CA002391865 A CA 002391865A CA 2391865 A CA2391865 A CA 2391865A CA 2391865 A1 CA2391865 A1 CA 2391865A1
- Authority
- CA
- Canada
- Prior art keywords
- mass
- acid
- comminuted
- hardened
- mother liquor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract 29
- 239000000463 material Substances 0.000 title claims abstract 13
- 229910052744 lithium Inorganic materials 0.000 title claims abstract 7
- 238000004064 recycling Methods 0.000 title claims abstract 3
- 229920000642 polymer Polymers 0.000 title 1
- 239000002253 acid Substances 0.000 claims abstract 13
- 239000012452 mother liquor Substances 0.000 claims abstract 11
- 150000003839 salts Chemical class 0.000 claims abstract 5
- 238000001816 cooling Methods 0.000 claims abstract 4
- 239000007787 solid Substances 0.000 claims abstract 4
- 150000003682 vanadium compounds Chemical class 0.000 claims abstract 4
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims abstract 3
- 235000002918 Fraxinus excelsior Nutrition 0.000 claims abstract 2
- 239000004411 aluminium Substances 0.000 claims abstract 2
- 229910052782 aluminium Inorganic materials 0.000 claims abstract 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000002956 ash Substances 0.000 claims abstract 2
- 229910001385 heavy metal Inorganic materials 0.000 claims abstract 2
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 claims abstract 2
- 229910052808 lithium carbonate Inorganic materials 0.000 claims abstract 2
- 239000005518 polymer electrolyte Substances 0.000 claims abstract 2
- 230000001376 precipitating effect Effects 0.000 claims abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 8
- 235000011149 sulphuric acid Nutrition 0.000 claims 8
- 239000000203 mixture Substances 0.000 claims 5
- 239000007789 gas Substances 0.000 claims 4
- 230000003647 oxidation Effects 0.000 claims 4
- 238000007254 oxidation reaction Methods 0.000 claims 4
- BDAGIHXWWSANSR-UHFFFAOYSA-N Formic acid Chemical compound OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 3
- 235000019253 formic acid Nutrition 0.000 claims 3
- 229910017604 nitric acid Inorganic materials 0.000 claims 3
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 claims 3
- 235000011007 phosphoric acid Nutrition 0.000 claims 3
- 239000001117 sulphuric acid Substances 0.000 claims 3
- ITMCEJHCFYSIIV-UHFFFAOYSA-N triflic acid Chemical compound OS(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-N 0.000 claims 3
- 150000007522 mineralic acids Chemical class 0.000 claims 2
- 150000007524 organic acids Chemical class 0.000 claims 2
- 235000005985 organic acids Nutrition 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 230000002378 acidificating effect Effects 0.000 claims 1
- 239000003513 alkali Substances 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 1
- 229910052788 barium Inorganic materials 0.000 claims 1
- 229910052790 beryllium Inorganic materials 0.000 claims 1
- 229910052792 caesium Inorganic materials 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 150000001768 cations Chemical class 0.000 claims 1
- 230000006378 damage Effects 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000011261 inert gas Substances 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 229910052701 rubidium Inorganic materials 0.000 claims 1
- 238000005201 scrubbing Methods 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 229910052712 strontium Inorganic materials 0.000 claims 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims 1
- KOKKJWHERHSKEB-UHFFFAOYSA-N vanadium(3+) Chemical compound [V+3] KOKKJWHERHSKEB-UHFFFAOYSA-N 0.000 claims 1
- 238000009854 hydrometallurgy Methods 0.000 abstract 1
- 238000009273 molten salt oxidation Methods 0.000 abstract 1
- 238000009853 pyrometallurgy Methods 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/054—Accumulators with insertion or intercalation of metals other than lithium, e.g. with magnesium or aluminium
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
- H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
- H01M10/0565—Polymeric materials, e.g. gel-type or solid-type
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/84—Recycling of batteries or fuel cells
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
L'invention concerne un procédé pyrométallurgique et hydrométallurgique de récupération et de recyclage de composés au lithium et au vanadium à partir d'un matériau comprenant des piles au lithium rechargeables, en particulier du type à gel au lithium et électrolyte polymère solide. On fournit une masse de matériau considéré qui subit les opérations suivantes: durcissement par refroidissement à une température inférieure à la température ambiante, comminution de la masse ainsi traitée, digestion avec un acide des cendres de cette masse résultant d'une incinération, ou des sels solidifiés résultant d'une oxydation en bain de sels fondus, ou bien comminution de la masse proprement dite. Le procédé donne une liqueur mère qui permet l'extraction des composés au vanadium, la séparation des métaux lourds et de l'aluminium, et la précipitation de carbonate de lithium à partir de la solution restante.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA2730336A CA2730336A1 (fr) | 2000-09-13 | 2001-09-13 | Procede de recyclage de piles rechargeables a polymere/lithium et materiaux connexes |
| CA2391865A CA2391865C (fr) | 2000-09-13 | 2001-09-13 | Une methode pour recycler des batteries rechargeables usees a polymere et lithium metallique et des materiaux apparentes |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA2,319,285 | 2000-09-13 | ||
| CA 2319285 CA2319285A1 (fr) | 2000-09-13 | 2000-09-13 | Methode de neutralisation et de recyclage de batteries rechargeables de polymere de metal lithium epuisees |
| CA2391865A CA2391865C (fr) | 2000-09-13 | 2001-09-13 | Une methode pour recycler des batteries rechargeables usees a polymere et lithium metallique et des materiaux apparentes |
| PCT/CA2001/001300 WO2002023651A1 (fr) | 2000-09-13 | 2001-09-13 | Procede de recyclage de piles rechargeables a polymere/lithium et materiaux connexes |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2730336A Division CA2730336A1 (fr) | 2000-09-13 | 2001-09-13 | Procede de recyclage de piles rechargeables a polymere/lithium et materiaux connexes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2391865A1 true CA2391865A1 (fr) | 2002-03-21 |
| CA2391865C CA2391865C (fr) | 2011-04-19 |
Family
ID=25682076
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2391865A Expired - Lifetime CA2391865C (fr) | 2000-09-13 | 2001-09-13 | Une methode pour recycler des batteries rechargeables usees a polymere et lithium metallique et des materiaux apparentes |
| CA2730336A Abandoned CA2730336A1 (fr) | 2000-09-13 | 2001-09-13 | Procede de recyclage de piles rechargeables a polymere/lithium et materiaux connexes |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2730336A Abandoned CA2730336A1 (fr) | 2000-09-13 | 2001-09-13 | Procede de recyclage de piles rechargeables a polymere/lithium et materiaux connexes |
Country Status (1)
| Country | Link |
|---|---|
| CA (2) | CA2391865C (fr) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010102377A1 (fr) * | 2009-03-13 | 2010-09-16 | Stevens Wayne C | Recyclage de batterie |
| CN115725858A (zh) * | 2022-12-02 | 2023-03-03 | 湖北金泉新材料有限公司 | 一种从黏土型锂矿中提取锂的方法 |
| WO2023045331A1 (fr) * | 2021-09-27 | 2023-03-30 | 湖南邦普循环科技有限公司 | Procédé de récupération sélective de métal précieux dans une batterie au lithium-ion usagée |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10435768B1 (en) | 2018-11-26 | 2019-10-08 | Pgm Recovery Systems, Inc. | Method of recovering materials bound to a metallic substrate using cryogenic cooling |
| US12037658B2 (en) | 2018-11-26 | 2024-07-16 | Pgm Recovery Systems, Inc. | Method of recovering materials bound to a metallic substrate using cryogenic cooling and an aqueous solution |
| CN113764762A (zh) * | 2021-08-16 | 2021-12-07 | 华中科技大学 | 用废旧锂离子电池合成高性能锂离子电池正极材料的方法 |
| CN113896214B (zh) * | 2021-11-29 | 2023-03-21 | 福州大学 | 一种硫酸锂溶液吸附碳化制备高纯碳酸锂的方法 |
-
2001
- 2001-09-13 CA CA2391865A patent/CA2391865C/fr not_active Expired - Lifetime
- 2001-09-13 CA CA2730336A patent/CA2730336A1/fr not_active Abandoned
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010102377A1 (fr) * | 2009-03-13 | 2010-09-16 | Stevens Wayne C | Recyclage de batterie |
| WO2023045331A1 (fr) * | 2021-09-27 | 2023-03-30 | 湖南邦普循环科技有限公司 | Procédé de récupération sélective de métal précieux dans une batterie au lithium-ion usagée |
| GB2622169A (en) * | 2021-09-27 | 2024-03-06 | Hunan Brunp Recycling Tech Co Ltd | Method for selectively recovering valuable metal in waste lithium battery |
| CN115725858A (zh) * | 2022-12-02 | 2023-03-03 | 湖北金泉新材料有限公司 | 一种从黏土型锂矿中提取锂的方法 |
| CN115725858B (zh) * | 2022-12-02 | 2023-12-15 | 湖北金泉新材料有限公司 | 一种从黏土型锂矿中提取锂的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CA2391865C (fr) | 2011-04-19 |
| CA2730336A1 (fr) | 2002-03-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKEX | Expiry |
Effective date: 20210913 |
|
| MKEX | Expiry |
Effective date: 20210913 |