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WO2013057319A3 - Procédés de préparation et de mise en forme de catalyseurs métalliques actifs supportés et précurseurs correspondants - Google Patents

Procédés de préparation et de mise en forme de catalyseurs métalliques actifs supportés et précurseurs correspondants Download PDF

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Publication number
WO2013057319A3
WO2013057319A3 PCT/EP2012/070897 EP2012070897W WO2013057319A3 WO 2013057319 A3 WO2013057319 A3 WO 2013057319A3 EP 2012070897 W EP2012070897 W EP 2012070897W WO 2013057319 A3 WO2013057319 A3 WO 2013057319A3
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WIPO (PCT)
Prior art keywords
active metal
precursors
preparation
methods
metal catalysts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
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PCT/EP2012/070897
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English (en)
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WO2013057319A2 (fr
Inventor
Richard HYMAN
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
INGEN GTL Ltd
Original Assignee
INGEN GTL Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from GB201118228A external-priority patent/GB201118228D0/en
Priority to EP12783914.0A priority Critical patent/EP2768612A2/fr
Priority to GB1408450.3A priority patent/GB2513488A/en
Priority to US14/351,920 priority patent/US9908110B2/en
Priority to EA201400487A priority patent/EA027722B1/ru
Priority to CA2851988A priority patent/CA2851988C/fr
Priority to BR112014009541-8A priority patent/BR112014009541B1/pt
Priority to CN201280051673.9A priority patent/CN103889577B/zh
Priority to JP2014536285A priority patent/JP6180421B2/ja
Priority to AU2012324802A priority patent/AU2012324802B2/en
Application filed by INGEN GTL Ltd filed Critical INGEN GTL Ltd
Publication of WO2013057319A2 publication Critical patent/WO2013057319A2/fr
Publication of WO2013057319A3 publication Critical patent/WO2013057319A3/fr
Anticipated expiration legal-status Critical
Priority to ZA2014/03535A priority patent/ZA201403535B/en
Priority to AU2017201067A priority patent/AU2017201067B2/en
Ceased legal-status Critical Current

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    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
    • C10G2/331—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals
    • C10G2/332—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals of the iron-group
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
    • C10G2/331—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals
    • C10G2/333—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals of the platinum-group
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
    • C10G2/334—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing molecular sieve catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/38—Base treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B01J2523/10—Constitutive chemical elements of heterogeneous catalysts of Group I (IA or IB) of the Periodic Table
    • B01J2523/13—Potassium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B01J2523/10—Constitutive chemical elements of heterogeneous catalysts of Group I (IA or IB) of the Periodic Table
    • B01J2523/17—Copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B01J2523/30—Constitutive chemical elements of heterogeneous catalysts of Group III (IIIA or IIIB) of the Periodic Table
    • B01J2523/31—Aluminium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B01J2523/30—Constitutive chemical elements of heterogeneous catalysts of Group III (IIIA or IIIB) of the Periodic Table
    • B01J2523/37—Lanthanides
    • B01J2523/3712—Cerium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B01J2523/40—Constitutive chemical elements of heterogeneous catalysts of Group IV (IVA or IVB) of the Periodic Table
    • B01J2523/41—Silicon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B01J2523/80—Constitutive chemical elements of heterogeneous catalysts of Group VIII of the Periodic Table
    • B01J2523/84—Metals of the iron group
    • B01J2523/842—Iron

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

L'invention porte sur un procédé de préparation d'un catalyseur supporté, lequel procédé comprend les étapes consistant à : (i) utiliser un support de catalyseur poreux comprenant une ossature ayant une structure poreuse interne comprenant un ou plusieurs pores, laquelle structure poreuse interne comprend un réactif précipitant; (ii) mettre en contact le support de catalyseur avec une solution ou une suspension colloïdale comprenant un métal catalytiquement actif de façon à ce que, au contact avec le réactif précipitant, des particules comprenant le métal catalytiquement actif soient précipitées à l'intérieur de la structure poreuse interne de l'ossature du support de catalyseur. L'invention porte également sur des catalyseurs supportés formés selon le procédé ci-dessus et sur l'utilisation des catalyseurs en catalyse de réactions chimiques, par exemple dans la synthèse de Fischer-Tropsch d'hydrocarbures.
PCT/EP2012/070897 2011-10-21 2012-10-22 Procédés de préparation et de mise en forme de catalyseurs métalliques actifs supportés et précurseurs correspondants Ceased WO2013057319A2 (fr)

Priority Applications (11)

Application Number Priority Date Filing Date Title
GB1408450.3A GB2513488A (en) 2011-10-21 2012-10-22 Methods of preparation and forming supported active metal catalysts and precursors
CN201280051673.9A CN103889577B (zh) 2011-10-21 2012-10-22 制备和形成负载活性金属的催化剂和前体的方法
US14/351,920 US9908110B2 (en) 2011-10-21 2012-10-22 Methods of preparation and forming supported active metal catalysts and precursors
EA201400487A EA027722B1 (ru) 2011-10-21 2012-10-22 Способы получения и формирования нанесенных активных металлических катализаторов и предшественников
CA2851988A CA2851988C (fr) 2011-10-21 2012-10-22 Procedes de preparation et de mise en forme de catalyseurs metalliques actifs supportes et precurseurs correspondants
BR112014009541-8A BR112014009541B1 (pt) 2011-10-21 2012-10-22 Métodos de preparação e formação de catalisadores e precursores suportados de metal ativo
JP2014536285A JP6180421B2 (ja) 2011-10-21 2012-10-22 担持活性金属触媒および前駆体を製造および形成する方法
EP12783914.0A EP2768612A2 (fr) 2011-10-21 2012-10-22 Procédés de préparation et de mise en forme de catalyseurs métalliques actifs supportés et précurseurs correspondants
AU2012324802A AU2012324802B2 (en) 2011-10-21 2012-10-22 Methods of preparation and forming supported active metal catalysts and precursors
ZA2014/03535A ZA201403535B (en) 2011-10-21 2014-05-15 Methods of preparation and forming supported active metal catalysts and precursons
AU2017201067A AU2017201067B2 (en) 2011-10-21 2017-02-16 Methods of preparation and forming supported active metal catalysts and precursors

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
GB201118228A GB201118228D0 (en) 2011-10-21 2011-10-21 Methods of preparation and forming supported active metal catalysts and precursors
GB1118228.4 2011-10-21
GBPCT/GB2012/000803 2012-10-19
GB2012000803 2012-10-19

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WO2013057319A2 WO2013057319A2 (fr) 2013-04-25
WO2013057319A3 true WO2013057319A3 (fr) 2013-06-06

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JP (1) JP6180421B2 (fr)
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AU (2) AU2012324802B2 (fr)
BR (1) BR112014009541B1 (fr)
CA (1) CA2851988C (fr)
EA (1) EA027722B1 (fr)
GB (1) GB2513488A (fr)
WO (1) WO2013057319A2 (fr)
ZA (2) ZA201403535B (fr)

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