[go: up one dir, main page]

WO2011136497A3 - 리튬 전이금속 인산염의 제조방법 - Google Patents

리튬 전이금속 인산염의 제조방법 Download PDF

Info

Publication number
WO2011136497A3
WO2011136497A3 PCT/KR2011/002816 KR2011002816W WO2011136497A3 WO 2011136497 A3 WO2011136497 A3 WO 2011136497A3 KR 2011002816 W KR2011002816 W KR 2011002816W WO 2011136497 A3 WO2011136497 A3 WO 2011136497A3
Authority
WO
WIPO (PCT)
Prior art keywords
transition metal
manufacturing
lithium transition
metal phosphate
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/KR2011/002816
Other languages
English (en)
French (fr)
Other versions
WO2011136497A2 (ko
WO2011136497A9 (ko
Inventor
김천중
박연정
장동규
박지호
양우영
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lotte Fine Chemical Co Ltd
Original Assignee
Samsung Fine Chemicals Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Samsung Fine Chemicals Co Ltd filed Critical Samsung Fine Chemicals Co Ltd
Priority to US13/695,342 priority Critical patent/US9537149B2/en
Priority to CA2797831A priority patent/CA2797831C/en
Priority to CN201180021860.8A priority patent/CN102869606B/zh
Priority to JP2013507869A priority patent/JP5796260B2/ja
Priority to EP11775202.2A priority patent/EP2565158B1/en
Publication of WO2011136497A2 publication Critical patent/WO2011136497A2/ko
Publication of WO2011136497A9 publication Critical patent/WO2011136497A9/ko
Publication of WO2011136497A3 publication Critical patent/WO2011136497A3/ko
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/45—Phosphates containing plural metal, or metal and ammonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Battery Electrode And Active Subsutance (AREA)

Abstract

리튬 전이금속 인산염의 제조방법이 개시된다. 개시된 리튬 전이금속 인산염의 제조방법은 리튬, 전이금속 및 인산을 포함하는 반응원료를 반응기에 주입하여 상기 반응기내에서 분자 수준으로 혼합(mixing at the molecular level)하는 단계 및 상기 반응기 내에서 상기 반응원료를 화학반응(chemical reaction)시켜 결정핵을 생성(nucleating)하는 단계를 포함한다.
PCT/KR2011/002816 2010-04-30 2011-04-20 리튬 전이금속 인산염의 제조방법 Ceased WO2011136497A2 (ko)

Priority Applications (5)

Application Number Priority Date Filing Date Title
US13/695,342 US9537149B2 (en) 2010-04-30 2011-04-20 Method for manufacturing a lithium transition metal phosphate
CA2797831A CA2797831C (en) 2010-04-30 2011-04-20 Method of manufacturing a lithium transition metal phosphate
CN201180021860.8A CN102869606B (zh) 2010-04-30 2011-04-20 锂过渡金属磷酸盐的制备方法
JP2013507869A JP5796260B2 (ja) 2010-04-30 2011-04-20 リチウム遷移金属リン酸塩の製造方法
EP11775202.2A EP2565158B1 (en) 2010-04-30 2011-04-20 Method for manufacturing a lithium transition metal phosphate

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR10-2010-0040797 2010-04-30
KR1020100040797A KR101698762B1 (ko) 2010-04-30 2010-04-30 리튬 전이금속 인산염의 제조방법

Publications (3)

Publication Number Publication Date
WO2011136497A2 WO2011136497A2 (ko) 2011-11-03
WO2011136497A9 WO2011136497A9 (ko) 2011-12-29
WO2011136497A3 true WO2011136497A3 (ko) 2012-03-01

Family

ID=44862007

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2011/002816 Ceased WO2011136497A2 (ko) 2010-04-30 2011-04-20 리튬 전이금속 인산염의 제조방법

Country Status (7)

Country Link
US (1) US9537149B2 (ko)
EP (1) EP2565158B1 (ko)
JP (1) JP5796260B2 (ko)
KR (1) KR101698762B1 (ko)
CN (1) CN102869606B (ko)
CA (1) CA2797831C (ko)
WO (1) WO2011136497A2 (ko)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20140021843A (ko) * 2012-08-10 2014-02-21 삼성정밀화학 주식회사 나노사이즈 철인산염 입자의 제조 방법
CN105000541B (zh) * 2015-07-31 2017-12-19 浙江大学宁波理工学院 一种纳米羟基磷灰石的制备方法
CN105344125A (zh) * 2015-12-08 2016-02-24 山西长林环保机械设备有限公司 一种卧式双进口增压旋转填料床
CN116374986B (zh) * 2023-04-14 2024-08-02 河南佰利新能源材料有限公司 一种磷酸铁锂正极材料及其制备方法和应用
KR20250092855A (ko) * 2023-12-15 2025-06-24 포스코홀딩스 주식회사 인산리튬의 제조 방법
WO2025137961A1 (zh) * 2023-12-27 2025-07-03 北京当升材料科技股份有限公司 磷酸铁锂正极材料及其制备方法、锂离子电池

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH07130357A (ja) * 1993-11-02 1995-05-19 Mitsubishi Cable Ind Ltd リチウム電池用正極材及びその製造方法
KR20040094762A (ko) * 2002-03-06 2004-11-10 발렌스 테크놀로지 (네바다), 인크. 알칼리/전이금속 인산염 및 관련 전극 활물질
KR20040096773A (ko) * 2003-05-09 2004-11-17 산요덴키가부시키가이샤 리튬 2차 전지용 양극 및 리튬 2차 전지
KR20070112278A (ko) * 2005-03-18 2007-11-22 쉬드-케미아크티엔게젤샤프트 리튬 금속 인산염을 습식 화학법으로 제조하기 위한 순환식방법

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1373083A (zh) 2001-03-07 2002-10-09 鞍山钢铁学院 一种尺寸可控的纳米粉体制备方法
CN1166448C (zh) * 2001-07-27 2004-09-15 鞍山钢铁学院 液相纳米粉体及纳米粒子聚集结构材料的制备方法
JP2003062440A (ja) * 2001-08-27 2003-03-04 Nakamura Sogo Kenkyusho:Kk 複数物質を含有する液状物の超混合方法
JP2004095386A (ja) * 2002-08-30 2004-03-25 Sumitomo Osaka Cement Co Ltd リチウムイオン電池用正極材料の製造方法およびリチウムイオン電池
CN100335415C (zh) 2003-02-28 2007-09-05 新加坡纳米材料科技有限公司 一种制备各种晶态钙钛矿类化合物粉体的方法
CN100355495C (zh) * 2004-12-16 2007-12-19 财团法人工业技术研究院 使用旋转填充床反应器的纳米流体制备法
WO2006096906A1 (en) * 2005-03-18 2006-09-21 Nanomaterials Technology Pte Ltd Inhalable drug
SG128490A1 (en) * 2005-06-07 2007-01-30 Nanomaterials Tech Pte Ltd Process for forming dispersant-coated carbon particles
JP5344452B2 (ja) * 2005-09-21 2013-11-20 関東電化工業株式会社 正極活物質及びその製造方法並びに正極活物質を含む正極を有する非水電解質電池
US7985388B2 (en) * 2006-10-02 2011-07-26 Nanomaterials Technology Pte Ltd Process for making nano-sized and micro-sized precipitate particles
DE102006055218A1 (de) 2006-11-21 2008-05-29 Bayer Technology Services Gmbh Kontinuierliches Verfahren zur Synthese von nanoskaligen metallhaltigen Nanopartikel und Nanopartikeldispersion
JP5479106B2 (ja) * 2006-12-22 2014-04-23 ユミコア ソシエテ アノニム 結晶性ナノＬｉＦｅＭＰＯ４の合成
US20090117020A1 (en) * 2007-11-05 2009-05-07 Board Of Regents, The University Of Texas System Rapid microwave-solvothermal synthesis and surface modification of nanostructured phospho-olivine cathodes for lithium ion batteries
DE102007058674A1 (de) 2007-12-06 2009-07-02 Süd-Chemie AG Nanopartikuläre Zusammensetzung und Verfahren zu deren Herstellung
KR101128860B1 (ko) * 2009-08-11 2012-03-23 삼성정밀화학 주식회사 리튬티타네이트 나노입자의 제조방법
CN101693531A (zh) 2009-10-16 2010-04-14 清华大学 一种纳米磷酸铁的制备方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH07130357A (ja) * 1993-11-02 1995-05-19 Mitsubishi Cable Ind Ltd リチウム電池用正極材及びその製造方法
KR20040094762A (ko) * 2002-03-06 2004-11-10 발렌스 테크놀로지 (네바다), 인크. 알칼리/전이금속 인산염 및 관련 전극 활물질
KR20040096773A (ko) * 2003-05-09 2004-11-17 산요덴키가부시키가이샤 리튬 2차 전지용 양극 및 리튬 2차 전지
KR20070112278A (ko) * 2005-03-18 2007-11-22 쉬드-케미아크티엔게젤샤프트 리튬 금속 인산염을 습식 화학법으로 제조하기 위한 순환식방법

Also Published As

Publication number Publication date
KR101698762B1 (ko) 2017-01-23
US20130045153A1 (en) 2013-02-21
WO2011136497A2 (ko) 2011-11-03
CA2797831C (en) 2018-06-12
JP5796260B2 (ja) 2015-10-21
CA2797831A1 (en) 2011-11-03
EP2565158A4 (en) 2016-04-13
CN102869606B (zh) 2016-03-02
KR20110121272A (ko) 2011-11-07
US9537149B2 (en) 2017-01-03
CN102869606A (zh) 2013-01-09
EP2565158B1 (en) 2019-07-31
EP2565158A2 (en) 2013-03-06
WO2011136497A9 (ko) 2011-12-29
JP2013530112A (ja) 2013-07-25

Similar Documents

Publication Publication Date Title
WO2009024424A3 (de) PULVERFÖRMIGE NiaM1bM2c(O)x(OH)y VERBINDUNGEN, VERFAHREN ZU DEREN HERSTELLUNG SOWIE DEREN VERWENDUNG IN BATTERIEN
WO2011019171A3 (ko) 리튬티타네이트 나노입자의 제조방법
WO2011136497A3 (ko) 리튬 전이금속 인산염의 제조방법
WO2013148975A3 (en) Emm-19: zeolitic imidazolate framework material, methods for making same, and uses thereof
WO2011049811A3 (en) Point-of-use silylamine generation
WO2009128973A3 (en) Methods for the production of silver nanowires
WO2011019871A3 (en) Biochars, methods of using biochars, methods of making biochars, and reactors
WO2011073798A3 (en) Method of producing a sulfide solid electrolyte material, sulfide solid electrolyte material, and lithium battery
WO2013002486A3 (ko) 고상 반응에 의한 리튬 망간 산화물의 제조 방법
WO2009022676A1 (ja) 五フッ化リン及び六フッ化リン酸塩の製造方法
WO2011003034A3 (en) Biological methods for preparing adipic acid
WO2009010263A3 (de) Prozess zur herstellung von bariumsulfat
NZ601352A (en) Organically chelated mineral compositions and methods thereof
WO2008090826A1 (ja) 間葉系細胞の製造方法、歯の製造方法及び歯形成用間葉系細胞
WO2013055135A3 (ko) 입상화 탄소 메조 기공 구조체의 제조 방법
WO2012039923A3 (en) Data model dualization
HK1199262A1 (en) Methods and systems for forming boronic acids and intermediates thereof
EP2626330A4 (en) MANGANIC OXIDE, METHOD FOR THE PRODUCTION THEREOF, AND METHOD FOR THE PRODUCTION OF A LITHIUM MANANGER COMPOUND OXIDE THEREWITH
WO2008096723A1 (ja) 六フッ化リン酸塩の製造方法
WO2008155965A1 (ja) 七フッ化ヨウ素の製造法
AU2008242996A8 (en) Polyquaternium-1 synthesis methods
WO2010060630A3 (de) Verfahren und vorrichtung zur herstellung von reinstsilzium
WO2014004386A3 (en) Low-cost method for making lithium transition metal olivines with high energy density
PL2464715T3 (pl) Sposób wytwarzania biodiesla na drodze kwasowej transestryfikacji oraz zastosowanie kwasu sulfonowego jako katalizatora przy wytwarzaniu biodiesla
WO2011104386A3 (de) Verfahren zur herstellung von ammoniak

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 201180021860.8

Country of ref document: CN

121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 11775202

Country of ref document: EP

Kind code of ref document: A2

ENP Entry into the national phase

Ref document number: 2797831

Country of ref document: CA

WWE Wipo information: entry into national phase

Ref document number: 2011775202

Country of ref document: EP

ENP Entry into the national phase

Ref document number: 2013507869

Country of ref document: JP

Kind code of ref document: A

NENP Non-entry into the national phase

Ref country code: DE

WWE Wipo information: entry into national phase

Ref document number: 13695342

Country of ref document: US