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WO2006094979A3 - Verfahren zur herstellung von dmc-katalysatoren - Google Patents

Verfahren zur herstellung von dmc-katalysatoren Download PDF

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Publication number
WO2006094979A3
WO2006094979A3 PCT/EP2006/060517 EP2006060517W WO2006094979A3 WO 2006094979 A3 WO2006094979 A3 WO 2006094979A3 EP 2006060517 W EP2006060517 W EP 2006060517W WO 2006094979 A3 WO2006094979 A3 WO 2006094979A3
Authority
WO
WIPO (PCT)
Prior art keywords
producing
dmc catalyst
salts
cyanometallate
reacting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2006/060517
Other languages
English (en)
French (fr)
Other versions
WO2006094979A2 (de
Inventor
Edward Bohres
Michael Triller
Raimund Ruppel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to US11/908,145 priority Critical patent/US7811958B2/en
Priority to EP06708667A priority patent/EP1866084A2/de
Priority to CN2006800077933A priority patent/CN101300074B/zh
Priority to JP2008500184A priority patent/JP5329217B2/ja
Publication of WO2006094979A2 publication Critical patent/WO2006094979A2/de
Publication of WO2006094979A3 publication Critical patent/WO2006094979A3/de
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B01J27/26—Cyanides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Toxicology (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • General Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Polyethers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)

Abstract

Gegenstand der Erfindung ist ein Verfahren zur Herstellung von DMC-Katalysatoren durch Umsetzung von Cyanometallatverbindungen, vorzugsweise Cyanometallatsalzen insbesondere Alkali- oder Erdalkalisalzen, mit Metallsalzen, dadurch gekennzeichnet, dass die Umsetzung im Anwesenheit einer Brönstedt-Säure durchgeführt wird.
PCT/EP2006/060517 2005-03-10 2006-03-07 Verfahren zur herstellung von dmc-katalysatoren Ceased WO2006094979A2 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
US11/908,145 US7811958B2 (en) 2005-03-10 2006-03-07 Method for producing an DMC catalyst
EP06708667A EP1866084A2 (de) 2005-03-10 2006-03-07 Verfahren zur herstellung von dmc-katalysatoren
CN2006800077933A CN101300074B (zh) 2005-03-10 2006-03-07 生产dmc催化剂的方法
JP2008500184A JP5329217B2 (ja) 2005-03-10 2006-03-07 複金属シアン化物錯体（ｄｍｃ）触媒の製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102005011581.0 2005-03-10
DE102005011581A DE102005011581A1 (de) 2005-03-10 2005-03-10 Verfahren zur Herstellung von DMC-Katalysatoren

Publications (2)

Publication Number Publication Date
WO2006094979A2 WO2006094979A2 (de) 2006-09-14
WO2006094979A3 true WO2006094979A3 (de) 2007-07-12

Family

ID=36477234

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/060517 Ceased WO2006094979A2 (de) 2005-03-10 2006-03-07 Verfahren zur herstellung von dmc-katalysatoren

Country Status (7)

Country Link
US (1) US7811958B2 (de)
EP (1) EP1866084A2 (de)
JP (1) JP5329217B2 (de)
KR (1) KR20070116249A (de)
CN (1) CN101300074B (de)
DE (1) DE102005011581A1 (de)
WO (1) WO2006094979A2 (de)

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DE102005057895A1 (de) * 2005-12-02 2007-06-06 Basf Ag Verfahren zur Herstellung von Multimetallcyanidverbindungen
WO2010072769A1 (de) 2008-12-23 2010-07-01 Basf Se Verfahren zur herstellung von polyether-blockcopolymeren
HUE044164T2 (hu) * 2009-10-19 2019-10-28 Basf Se Kettõs fém-cianid katalizátorok kondicionálása
WO2011160296A1 (en) * 2010-06-23 2011-12-29 Basf Se Modified double metal cyanide catalyst
BR112013015393A2 (pt) 2010-12-20 2016-09-20 Bayer Ip Gmbh método para a preparação de poliéter polióis
KR101404702B1 (ko) 2011-03-08 2014-06-17 에스케이이노베이션 주식회사 에테르 결합 단위체를 함유한 이산화탄소/에폭사이드 공중합체의 제조 방법
WO2013062682A1 (en) 2011-10-28 2013-05-02 Dow Global Technologies Llc Compositions of hydrocarbon oils and oil soluble pags produced by dmc catalysis
US9562134B2 (en) 2013-03-12 2017-02-07 Covestro Llc Catalyst for the production of polyols having lower amounts of high molecular weight tail
GB201515350D0 (en) 2015-08-28 2015-10-14 Econic Technologies Ltd Method for preparing polyols
GB201703324D0 (en) 2017-03-01 2017-04-12 Econic Tech Ltd Method for preparing polyether carbonates
GB201717441D0 (en) 2017-10-24 2017-12-06 Econic Tech Ltd A polymerisation process
GB201717459D0 (en) 2017-10-24 2017-12-06 Econic Tech Limited Methods for forming polycarbonate ether polyols and high molecular weight polyether carbonates
JP2021522382A (ja) 2018-04-25 2021-08-30 ヘンケル・アクチェンゲゼルシャフト・ウント・コムパニー・コマンディットゲゼルシャフト・アウフ・アクチェンＨｅｎｋｅｌ ＡＧ ＆ Ｃｏ． ＫＧａＡ ヒドロキシル官能化ポリエーテルポリシロキサンブロックコポリマーの調製用プロセス
CN112368317B (zh) 2018-06-19 2024-04-02 汉高股份有限及两合公司 高活性双金属氰化物化合物
GB201814526D0 (en) 2018-09-06 2018-10-24 Econic Tech Ltd Methods for forming polycarbonate ether polyols and high molecular weight polyether carbonates
CN110964191B (zh) * 2018-09-29 2021-02-02 杭州普力材料科技有限公司 一种混合酸改性的锌钴双金属氰化物催化剂及其制备方法
CN111286014B (zh) * 2018-09-29 2022-04-12 杭州普力材料科技有限公司 一种用于二氧化碳和环氧化物共聚的双金属氰化物催化剂及其制备方法
WO2020084033A1 (de) 2018-10-26 2020-04-30 Basf Se Hydrophob assoziierende copolymere für die tertiäre erdölförderung umfassend monomere mit propylenoxy-einheiten
WO2020084046A1 (de) 2018-10-26 2020-04-30 Basf Se Verfahren zur herstellung von propylenoxy-haltigen hydrophob assoziierenden monomeren mittels dmc-katalyse
ES2985743T3 (es) 2018-12-06 2024-11-07 Henkel Ag & Co Kgaa Preparación de copolímeros en cepillo de polisiloxano-polialquilenglicol
ES2977551T3 (es) 2018-12-06 2024-08-26 Henkel Ag & Co Kgaa Composición curable que comprende copolímeros de polisiloxano polialquilenglicol en cepillo
GB201906210D0 (en) 2019-05-02 2019-06-19 Econic Tech Limited A polyol block copolymer, compositions and processes therefor
GB201906214D0 (en) 2019-05-02 2019-06-19 Econic Tech Ltd A polyol block copolymer, compositions and processes therefor
GB202003002D0 (en) 2020-03-02 2020-04-15 Crane Ltd Method of preparation of a polyol block copolymer
GB202003003D0 (en) 2020-03-02 2020-04-15 Econic Tech Ltd A polyol block copolymer
CN111349224B (zh) * 2020-03-30 2021-06-01 杭州普力材料科技有限公司 一种液相法管道化连续化生产聚碳酸酯-聚醚多元醇的方法
CN111393629B (zh) * 2020-03-30 2021-06-01 杭州普力材料科技有限公司 一种预加热液相法管道化连续化生产聚碳酸丙烯酯的方法
CN111484610B (zh) * 2020-03-30 2021-11-09 杭州普力材料科技有限公司 一种聚碳酸酯-聚醚二元醇的制备方法
CN111378106B (zh) * 2020-03-30 2021-06-01 杭州普力材料科技有限公司 一种预加热液相法管道化连续化生产聚碳酸酯-聚醚多元醇的方法
EP3932973B1 (de) 2020-07-01 2025-09-03 Henkel AG & Co. KGaA Bifunktionalisierte polysiloxanbürstencopolymere
GB202017531D0 (en) 2020-11-05 2020-12-23 Econic Tech Limited (poly)ol block copolymer
CN118103137A (zh) 2021-08-11 2024-05-28 伊科尼克技术有限公司 使用大环双金属催化剂与双金属氰化物催化剂的混合物通过环氧化物和co2共聚制备表面活性剂的方法
GB202115335D0 (en) 2021-10-25 2021-12-08 Econic Tech Ltd Surface-active agent
GB2626546A (en) 2023-01-25 2024-07-31 Econic Tech Ltd Surface-active agent
GB2626989A (en) 2023-02-10 2024-08-14 Econic Tech Ltd Surface-active agent
GB2629367A (en) 2023-04-25 2024-10-30 Econic Tech Ltd Surface-active agent
WO2024223596A1 (en) 2023-04-25 2024-10-31 Unilever Ip Holdings B.V. Compositions
EP4480992A1 (de) 2023-06-19 2024-12-25 Henkel AG & Co. KGaA Gradientencopolymere aus polyether und polysiloxan

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Publication number Priority date Publication date Assignee Title
GB1008319A (en) * 1962-07-03 1965-10-27 Kali Chemie Veb Process for the production of directly precipitated milori blue
US4472560A (en) * 1982-03-31 1984-09-18 Shell Oil Company Process for the polymerization of epoxides
US4477589A (en) * 1982-03-31 1984-10-16 Shell Oil Company Catalysts for the polymerization of epoxides and process for the preparation of such catalysts
US6063897A (en) * 1998-05-05 2000-05-16 Arco Chemical Technology, L.P. Acid-treated double metal cyanide complex catalysts
WO2001003831A1 (en) * 1999-07-09 2001-01-18 The Dow Chemical Company Incipient wetness method for making metal-containing cyanide catalysts
US20020032121A1 (en) * 1999-06-02 2002-03-14 Georg Heinrich Grosch Multimetal cyanide compounds, their preparation and their use
WO2003080240A2 (en) * 2002-03-21 2003-10-02 Dow Global Technologies, Inc. Method for preparing metal cyanide catalysts using zero valent metals

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WO2003080239A2 (en) 2002-03-19 2003-10-02 Dow Global Technologies, Inc. Method for preparing metal cyanide catalysts using insoluble metal salts
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Patent Citations (7)

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GB1008319A (en) * 1962-07-03 1965-10-27 Kali Chemie Veb Process for the production of directly precipitated milori blue
US4472560A (en) * 1982-03-31 1984-09-18 Shell Oil Company Process for the polymerization of epoxides
US4477589A (en) * 1982-03-31 1984-10-16 Shell Oil Company Catalysts for the polymerization of epoxides and process for the preparation of such catalysts
US6063897A (en) * 1998-05-05 2000-05-16 Arco Chemical Technology, L.P. Acid-treated double metal cyanide complex catalysts
US20020032121A1 (en) * 1999-06-02 2002-03-14 Georg Heinrich Grosch Multimetal cyanide compounds, their preparation and their use
WO2001003831A1 (en) * 1999-07-09 2001-01-18 The Dow Chemical Company Incipient wetness method for making metal-containing cyanide catalysts
WO2003080240A2 (en) * 2002-03-21 2003-10-02 Dow Global Technologies, Inc. Method for preparing metal cyanide catalysts using zero valent metals

Also Published As

Publication number Publication date
US20080167502A1 (en) 2008-07-10
JP5329217B2 (ja) 2013-10-30
US7811958B2 (en) 2010-10-12
WO2006094979A2 (de) 2006-09-14
DE102005011581A1 (de) 2006-09-14
KR20070116249A (ko) 2007-12-07
JP2008533227A (ja) 2008-08-21
CN101300074A (zh) 2008-11-05
EP1866084A2 (de) 2007-12-19
CN101300074B (zh) 2010-11-10

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