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WO1999065447A1 - Support for empty hard gelatine capsules, and utilization of said support with the capsules inserted - Google Patents

Support for empty hard gelatine capsules, and utilization of said support with the capsules inserted Download PDF

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Publication number
WO1999065447A1
WO1999065447A1 PCT/ES1999/000181 ES9900181W WO9965447A1 WO 1999065447 A1 WO1999065447 A1 WO 1999065447A1 ES 9900181 W ES9900181 W ES 9900181W WO 9965447 A1 WO9965447 A1 WO 9965447A1
Authority
WO
WIPO (PCT)
Prior art keywords
capsules
holes
capsule
support
filling machine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/ES1999/000181
Other languages
Spanish (es)
French (fr)
Inventor
Francisco Javier Llorca Chulia
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to JP2000554327A priority Critical patent/JP2002518099A/en
Priority to CA002335161A priority patent/CA2335161A1/en
Priority to MXPA00012855A priority patent/MXPA00012855A/en
Priority to DE69902916T priority patent/DE69902916T2/en
Priority to KR1020007014394A priority patent/KR20010052997A/en
Priority to EP99957014A priority patent/EP1092412B1/en
Priority to AT99957014T priority patent/ATE223691T1/en
Publication of WO1999065447A1 publication Critical patent/WO1999065447A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
    • A61J3/00—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms
    • A61J3/07—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms into the form of capsules or similar small containers for oral use
    • A61J3/071—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms into the form of capsules or similar small containers for oral use into the form of telescopically engaged two-piece capsules
    • A61J3/074—Filling capsules; Related operations
    • A61J3/075—Manually operated filling apparatus

Definitions

  • the sector of the technique of this patent is in pharmaceutical practice, the filling of hard gelatin capsules, of which they contain a specific amount for each of those that make up a treatment, and particularly of those made from a master formula Indication of the prior art.
  • the so-called “Capsunorm loader” is used in pharmacies, consisting of an apparatus that produces the orientation of capsules of sizes 00 to 2, for the introduction of capsules on the filling surface of an apparatus for filling capsules .
  • Said apparatus is not operative for capsule sizes 3, 4 and 5, which are the smallest and most difficult to handle, without prejudice to the difficulty of precisely handling said "loader.”
  • the indicated charger is intended to be used by a different device of the same company, ES U 278428 for "device for automatic filling of capsules”, also commercially called “Capsunorm capsule” which is formed by at least one plate equipped with holes in which to accommodate the capsules intended for filling.
  • the present invention has as its object a support surface of empty hard gelatin capsules, and use of said surface with the capsules inserted, so that it comprises the arrangement of the capsules on the surface provided with holes, as well as the use of these for the filled in a small conventional machine.
  • Figure 1 shows a plan view of the capsule bearing surface.
  • Figure 2 shows a view of said surface in correspondence of a plate of a capsule filling machine.
  • the laminar surface is shown indicated by 1, with 2 the holes made in said laminar surface, with 3 the distance between columns, with 4 the distance between rows, with 5 the base of the capsule, with 6 the lid of the capsule, with 7 the base of the capsule filling machine, with 8 each of the holes made in the surface of the capsule filling machine, with 9 the surface of the manual filling machine, with 10 the diameter of the holes of the laminar surface.
  • the laminar surface 1 disposes the holes
  • the filling machines have, according to the size of the capsules, distances between holes that are coincident with the distances between columns and rows
  • the operation is simply to overlap the set of capsules inserted in the laminar surface, detaching the laminar support by means of a pressure through a suitable card or smooth surface.
  • each capsule size has a corresponding size of sheet surface 1, and also of the base of the machine 7, so that said correspondence eliminates the need to manually introduce the capsules into the holes of the base 7.
  • the requested protection is going to be carried out on a supporting surface of empty hard gelatin capsules, in which a laminar portion of flexible material 1 is included, which is provided with holes 2, in all or in a part of said surface, said holes 2 being, in regular distribution and uniform diameter equal to that of capsules 5, 6, which supports and distribution corresponding to holes 8, of base 7, of a manual filling machine for capsules, and said holes being sizes corresponding to each of the available capsule diameters, namely size 000 to 5; and its use comprises the stages of insertion of the capsules 5, 6, arranged in the laminar surface 1, in the surface 9, and in the corresponding holes 8 of the base 7, of a capsule filling machine, such that each capsule is facing the hole to be accommodated, said capsules being lowered by manual pressure on each capsule or by pressure by a surface suitable for practicing said pressure, to be inserted into said holes 8, of the filling machine.

Landscapes

  • Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Public Health (AREA)
  • Medical Preparation Storing Or Oral Administration Devices (AREA)
  • Basic Packing Technique (AREA)
  • Cosmetics (AREA)
  • Medicinal Preparation (AREA)
  • Paints Or Removers (AREA)
  • Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
  • Containers And Plastic Fillers For Packaging (AREA)
  • Supplying Of Containers To The Packaging Station (AREA)

Abstract

The support is comprised of a laminar surface consisting of a flexible sheet provided with a plurality of holes having a diameter which corresponds to the sizes of capsules from 000 to 5, said holes being made in the sheet and in an arrangement corresponding to the surface of a manual filling machine. The invention also relates to the use of said lamellar surface with capsules inserted into the orifices in order to position the capsules on the filling surface of the corresponding machine. Industrial application as an aid for the encapsulation using small encapsulating machines.

Description

Una superficie sustentadora de cápsulas de gelatina dura vacías, y utilización de dicha superficie con las cápsulas insertadas . A supporting surface of empty hard gelatin capsules, and use of said surface with the capsules inserted.

El sector de la técnica de esta patente es en la práctica farmacéutica, la del llenado de cápsulas de gelatina dura, de las que contienen una cantidad de específico para cada una de las que conforman un tratamiento, y particularmente de las confeccionadas a base de una fórmula magistral . Indicación del Estado de la Técnica anterior.The sector of the technique of this patent is in pharmaceutical practice, the filling of hard gelatin capsules, of which they contain a specific amount for each of those that make up a treatment, and particularly of those made from a master formula Indication of the prior art.

Existen técnicas industriales para la industria farmacéutica por las que el envasado de los productos en las cápsulas correspondientes, se lleva a cabo por procesos industriales complejos. Dichas técnicas, por necesitar grandes producciones para ser rentables, se apartan del contenido de la presente patente de invención.There are industrial techniques for the pharmaceutical industry whereby the packaging of the products in the corresponding capsules is carried out by complex industrial processes. Such techniques, because they need large productions to be profitable, depart from the content of the present invention patent.

Para pequeñas producciones, se utiliza en las farmacias el denominado "cargador de Capsunorm" , consistente en un aparato que produce la orientación de cápsulas de los tamaños 00 a 2, para la introducción de cápsulas en la superficie de llenado de un aparato de llenar cápsulas. Dicho aparato no es operativo para los tamaños 3, 4 y 5 de cápsulas, que son los mas pequeños y difíciles de manejar, sin perjuicio de la dificultad de manejo con precisión del citado "cargador" . El cargador indicado está destinado a ser utilizado por un distinto aparato de la misma compañía, ES U 278428 por "dispositivo para el llenado automático de cápsulas", también llamado comercialmente "capsulero de Capsunorm" que se halla formado por al menos una placa dotada de orificios en la que alojar las cápsulas destinadas a su llenado.For small productions, the so-called "Capsunorm loader" is used in pharmacies, consisting of an apparatus that produces the orientation of capsules of sizes 00 to 2, for the introduction of capsules on the filling surface of an apparatus for filling capsules . Said apparatus is not operative for capsule sizes 3, 4 and 5, which are the smallest and most difficult to handle, without prejudice to the difficulty of precisely handling said "loader." The indicated charger is intended to be used by a different device of the same company, ES U 278428 for "device for automatic filling of capsules", also commercially called "Capsunorm capsule" which is formed by at least one plate equipped with holes in which to accommodate the capsules intended for filling.

Existe una divulgación previa del ES U 262629 por "dispositivo perfeccionado para el llenado de cápsulas medicamentosas", constituido por un conjunto de disposición y aplicación similar al descrito.There is a prior disclosure of ES U 262629 for "perfected device for filling medicated capsules", consisting of a set of disposition and application similar to that described.

La utilización de dicho "cargador" tiene lugar para la disposición de las cápsulas en las máquinas llenadoras de cápsulas, en las que se fijan, se alinean sobre su superficie, en la cual se dispone el polvo del específico correspondiente, y posteriormente se tapan.The use of said "loader" takes place for the arrangement of the capsules in the capsule filling machines, in which they are fixed, are aligned on their surface, in which the powder of the corresponding specific is arranged, and then covered.

Sin embargo, el uso de dicho capsulero no se extiende, como hemos dicho para las cápsulas de gelatina dura de pequeño tamaño, lo que exige que se dispongan a mano en la máquina llenadora. Ello lleva además a la circunstancia de que el capsulero se desecha en la práctica también para el uso de las cápsulas grandes, pues también son las más fáciles de manejar a mano, además de que su utilización no está exenta de cierto engorro. La presente invención tiene por objeto una superficie sustentadora de cápsulas de gelatina dura vacías, y utilización de dicha superficie con las cápsulas insertadas, de modo que comprende la disposición de las cápsulas en la superficie dotada de orificios, así como la utilización de éstas para el rellenado en una máquina convencional pequeña.However, the use of said capsule holder does not extend, as we have said for small-sized hard gelatin capsules, which requires that they be arranged by hand in the filling machine. This also leads to the circumstance that the capsule is discarded in practice also for the use of large capsules, as they are also the easiest to handle by hand, in addition to the fact that their use is not exempt from a certain nuisance. The present invention has as its object a support surface of empty hard gelatin capsules, and use of said surface with the capsules inserted, so that it comprises the arrangement of the capsules on the surface provided with holes, as well as the use of these for the filled in a small conventional machine.

Con objeto de hacer mas clara la explicación que va a seguir, se acompaña dos hojas de dibujos que en dos figuras representan la esencia de la presente invención. La figura 1 muestra una vista en planta de la superficie sustentadora de cápsulas.In order to make clearer the explanation that will follow, two sheets of drawings are attached which in two figures represent the essence of the present invention. Figure 1 shows a plan view of the capsule bearing surface.

La figura 2 muestra una vista de dicha superficie en correspondencia de una placa de una máquina llenadora de cápsulas.Figure 2 shows a view of said surface in correspondence of a plate of a capsule filling machine.

En dichas figuras se representa indicado por 1 la superficie laminar, con 2 los orificios practicados en dicha superficie laminar, con 3 la distancia entre columnas, con 4 la distancia entre filas, con 5 la base de la cápsula, con 6 la tapa de la cápsula, con 7 la base de la máquina llenadora de cápsulas, con 8 cada uno de los orificios practicados en la superficie de la máquina llenadora de cápsulas, con 9 la superficie de la máquina llenadora manual, con 10 el diámetro de los orificios de la superficie laminar.In said figures, the laminar surface is shown indicated by 1, with 2 the holes made in said laminar surface, with 3 the distance between columns, with 4 the distance between rows, with 5 the base of the capsule, with 6 the lid of the capsule, with 7 the base of the capsule filling machine, with 8 each of the holes made in the surface of the capsule filling machine, with 9 the surface of the manual filling machine, with 10 the diameter of the holes of the laminar surface.

La superficie laminar 1 dispone los orificiosThe laminar surface 1 disposes the holes

2 dispuestos de modo tal que son coincidentes con los orificios 8 de la superficie 9 de la base 7 de la llenadora. Dichos orificios 2 poseen diámetros 10 coincidentes con las cápsulas, de modo que éstas quedan sustentadas en ellos, y también distribuidas de tal modo que son coincidentes con cada correspondiente orificio de la base de la máquina llenadora. Las máquinas llenadoras poseen, de acuerdo con el tamaño de las cápsulas, unas distancias entre orificios que son coincidentes con las distancias entre columnas y filas2 arranged so that they are coincident with the holes 8 of the surface 9 of the base 7 of the filler. Said holes 2 have diameters 10 coinciding with the capsules, so that they are supported therein, and also distributed in such a way that they are coincident with each corresponding hole in the base of the filling machine. The filling machines have, according to the size of the capsules, distances between holes that are coincident with the distances between columns and rows

3 y 4 de los orificios de la superficie laminar 1. De este modo, para disponer las cápsulas en los orificios 8 de la base de la máquina llenadora, la operación es simplemente sobreposicionar el conjunto de cápsulas insertadas en la superficie laminar, desprendiendo el soporte laminar mediante una presión a través de una tarjeta o superficie lisa adecuada.3 and 4 of the holes of the laminar surface 1. Thus, to place the capsules in the holes 8 of the base of the filling machine, the operation is simply to overlap the set of capsules inserted in the laminar surface, detaching the laminar support by means of a pressure through a suitable card or smooth surface.

Evidentemente, cada tamaño de cápsula posee un tamaño correspondiente de superficie laminar 1, y también de base de la máquina 7, de modo que dicha correspondencia elimina la necesidad de introducir manualmente las cápsulas en los orificios de la base 7.Obviously, each capsule size has a corresponding size of sheet surface 1, and also of the base of the machine 7, so that said correspondence eliminates the need to manually introduce the capsules into the holes of the base 7.

Un modo de realización se deduce de la explicación dada en los dos párrafos anteriores.An embodiment is deduced from the explanation given in the previous two paragraphs.

A modo de resumen, indicamos que la protección solicitada se va a concretar en una superficie sustentadora de cápsulas de gelatina dura vacías, en la que se comprende una porción laminar de material flexible 1, que se halla dotada de orificios 2, en toda o en una parte de dicha superficie, hallándose los dichos orificios 2, en distribución regular y diámetro uniforme igual al de las cápsulas 5, 6, que sustenta y de distribución correspondiente a los orificios 8, de la base 7, de una máquina manual de llenado de cápsulas, y siendo dichos orificios de tamaños correspondientes a cada uno de los diámetros de cápsulas disponibles, a saber tamaño 000 a 5 ; y su utilización comprende las etapas de inserción de las cápsulas 5, 6, dispuestas en la superficie laminar 1, en la superficie 9, y en los orificios 8, correspondientes de la base 7, de una máquina llenadora de cápsulas, de tal modo que cada cápsula queda enfrentada al orificio que ha de alojarlas, haciéndose descender las dichas cápsulas mediante una presión manual sobre cada cápsula o mediante la presión por una superficie idónea para practicar dicha presión, para ser insertadas en los dichos orificios 8, de la máquina llenadora.As a summary, we indicate that the requested protection is going to be carried out on a supporting surface of empty hard gelatin capsules, in which a laminar portion of flexible material 1 is included, which is provided with holes 2, in all or in a part of said surface, said holes 2 being, in regular distribution and uniform diameter equal to that of capsules 5, 6, which supports and distribution corresponding to holes 8, of base 7, of a manual filling machine for capsules, and said holes being sizes corresponding to each of the available capsule diameters, namely size 000 to 5; and its use comprises the stages of insertion of the capsules 5, 6, arranged in the laminar surface 1, in the surface 9, and in the corresponding holes 8 of the base 7, of a capsule filling machine, such that each capsule is facing the hole to be accommodated, said capsules being lowered by manual pressure on each capsule or by pressure by a surface suitable for practicing said pressure, to be inserted into said holes 8, of the filling machine.

Es susceptible de aplicación industrial como ayuda para el encapsulado mediante pequeñas máquinas de encapsular . It is capable of industrial application as an aid for encapsulation by means of small encapsulating machines.

Claims

R E I V I N D I C A C I O N E S 1.- Una superficie sustentadora de cápsulas de gelatina dura vacías, caracterizada por que comprende una porción laminar de material flexible (1) , que se halla dotada de orificios (2) en toda o en una parte de dicha superficie, hallándose los dichos orificios (2) en distribución regular y diámetro uniforme igual al de las cápsulas (5, 6), que sustenta y de distribución correspondiente a los orificios (8) de la base (7) de una máquina manual de llenado de cápsulas, y siendo dichos orificios de tamaños correspondientes a cada uno de los diámetros de cápsulas disponibles, a saber tamaño 000 a 5. 2.- Utilización de superficie sustentadora de cápsulas, caracterizada por comprender las siguientes etapas : inserción de las cápsulas (5, 6) en la superficie laminar (1),CLAIMS 1.- A support surface of empty hard gelatin capsules, characterized in that it comprises a laminar portion of flexible material (1), which is provided with holes (2) in all or a part of said surface, the said ones being found holes (2) in regular distribution and uniform diameter equal to that of the capsules (5, 6), which supports and distribution corresponding to the holes (8) of the base (7) of a manual capsule filling machine, and being said holes of corresponding sizes to each of the available capsule diameters, namely size 000 to 5. 2.- Use of a capsule bearing surface, characterized by comprising the following steps: insertion of the capsules (5, 6) into the laminar surface (1), - disposición de la dicha superficie laminar (1) en la superficie (9) de orificios (8) de la base (7) de una máquina llenadora de cápsulas, de tal modo que cada cápsula queda enfrentada al orificio que ha de alojarlas, haciéndose alojar las dichas cápsulas mediante una presión manual directa sobre cada cápsula o por medio de una superficie idónea para practicar dicha presión, para ser insertadas en los dichos orificios (8) de la máquina llenadora. - arrangement of said laminar surface (1) on the surface (9) of holes (8) of the base (7) of a capsule filling machine, such that each capsule faces the hole to be housed, being made housing said capsules by direct manual pressure on each capsule or by means of a suitable surface for practicing said pressure, to be inserted into said holes (8) of the filling machine.
PCT/ES1999/000181 1998-06-18 1999-06-18 Support for empty hard gelatine capsules, and utilization of said support with the capsules inserted Ceased WO1999065447A1 (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
JP2000554327A JP2002518099A (en) 1998-06-18 1999-06-18 Support for empty hard gelatin capsules and use of said support with the capsule inserted
CA002335161A CA2335161A1 (en) 1998-06-18 1999-06-18 Support for empty hard gelatine capsules, and utilization of said support with the capsules inserted
MXPA00012855A MXPA00012855A (en) 1998-06-18 1999-06-18 Support for empty hard gelatine capsules, and utilization of said support with the capsules inserted.
DE69902916T DE69902916T2 (en) 1998-06-18 1999-06-18 RECORDING FOR EMPTY, HARD GELATINE CAPSULES AND USING THIS RECORDING WITH INSERTED CAPSULES
KR1020007014394A KR20010052997A (en) 1998-06-18 1999-06-18 Support for empty hard gelatine capsules, and utilization of said support with the capsules inserted
EP99957014A EP1092412B1 (en) 1998-06-18 1999-06-18 Support for empty hard gelatine capsules, and utilization of said support with the capsules inserted
AT99957014T ATE223691T1 (en) 1998-06-18 1999-06-18 RECEPTACLE FOR EMPTY, HARD GELATIN CAPSULES AND APPLICATION OF THIS RECEPTACLE WITH CAPSULES INSERTED

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ES009801285A ES2159219B1 (en) 1998-06-18 1998-06-18 A SUSTAINING SURFACE OF EMPTY GELATINE CAPSULES, AND USE OF SUCH SURFACE WITH THE INSERTED CAPSULES.
ESP9801285 1998-06-18

Publications (1)

Publication Number Publication Date
WO1999065447A1 true WO1999065447A1 (en) 1999-12-23

Family

ID=8304208

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/ES1999/000181 Ceased WO1999065447A1 (en) 1998-06-18 1999-06-18 Support for empty hard gelatine capsules, and utilization of said support with the capsules inserted

Country Status (10)

Country Link
EP (1) EP1092412B1 (en)
JP (1) JP2002518099A (en)
KR (1) KR20010052997A (en)
CN (1) CN1191807C (en)
AT (1) ATE223691T1 (en)
CA (1) CA2335161A1 (en)
DE (1) DE69902916T2 (en)
ES (1) ES2159219B1 (en)
MX (1) MXPA00012855A (en)
WO (1) WO1999065447A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2163981B1 (en) 1999-06-16 2003-04-01 Chulia Francisco J Llorca MACHINERY TO ORDER GELATINE CAPSULES FOR DISPOSITION IN BLISTERS.
CN104013532B (en) * 2013-03-01 2016-08-03 何志全 Domestic capsule clamp

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2574727A (en) * 1948-02-09 1951-11-13 George A Burkett Pharmaceutical capsule sizing device with volumetric capacity varying means
US2680548A (en) * 1952-09-12 1954-06-08 Karos Sam Capsule filling device
US2720351A (en) * 1952-04-04 1955-10-11 Fleischer Henry Device for filling gelating capsules
US3552095A (en) * 1968-04-18 1971-01-05 Lilly Co Eli Manual capsule filling apparatus
US5319749A (en) * 1988-12-22 1994-06-07 U.S. Philips Corporation Circuit arrangement for geometric image transformation including a memory storing an assignment between addresses in input and output images

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2746675C2 (en) * 1977-10-18 1979-10-04 Hermann Heye, 3063 Obernkirchen Glass forming machine with several stations
DE3018232C2 (en) * 1980-05-13 1982-04-08 Fa. Hermann Heye, 3063 Obernkirchen Dispensing station of a glass forming machine
DE69014551T2 (en) * 1989-10-27 1995-05-04 Vhc Ltd Distribution mechanism for glassware.
CA2078380C (en) * 1991-09-17 1998-05-19 Victor Tijerina-Ramos Machine for the production of glassware articles by the press and blow process

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2574727A (en) * 1948-02-09 1951-11-13 George A Burkett Pharmaceutical capsule sizing device with volumetric capacity varying means
US2720351A (en) * 1952-04-04 1955-10-11 Fleischer Henry Device for filling gelating capsules
US2680548A (en) * 1952-09-12 1954-06-08 Karos Sam Capsule filling device
US3552095A (en) * 1968-04-18 1971-01-05 Lilly Co Eli Manual capsule filling apparatus
US5319749A (en) * 1988-12-22 1994-06-07 U.S. Philips Corporation Circuit arrangement for geometric image transformation including a memory storing an assignment between addresses in input and output images

Also Published As

Publication number Publication date
MXPA00012855A (en) 2002-05-08
KR20010052997A (en) 2001-06-25
ES2159219A1 (en) 2001-09-16
DE69902916T2 (en) 2003-05-15
ES2159219B1 (en) 2002-04-01
CN1306411A (en) 2001-08-01
DE69902916D1 (en) 2002-10-17
CA2335161A1 (en) 1999-12-23
ATE223691T1 (en) 2002-09-15
JP2002518099A (en) 2002-06-25
EP1092412B1 (en) 2002-09-11
CN1191807C (en) 2005-03-09
EP1092412A1 (en) 2001-04-18

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