US2791498A - Method of improving metal powders - Google Patents
Method of improving metal powders Download PDFInfo
- Publication number
- US2791498A US2791498A US551990A US55199055A US2791498A US 2791498 A US2791498 A US 2791498A US 551990 A US551990 A US 551990A US 55199055 A US55199055 A US 55199055A US 2791498 A US2791498 A US 2791498A
- Authority
- US
- United States
- Prior art keywords
- powder
- increasing
- grain size
- metal powders
- layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000843 powder Substances 0.000 title claims description 26
- 238000000034 method Methods 0.000 title claims description 10
- 239000002184 metal Substances 0.000 title claims description 9
- 229910052751 metal Inorganic materials 0.000 title claims description 9
- 238000005097 cold rolling Methods 0.000 claims description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 8
- 238000000227 grinding Methods 0.000 description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 238000000137 annealing Methods 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 238000005482 strain hardening Methods 0.000 description 3
- 238000003466 welding Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/04—Making metallic powder or suspensions thereof using physical processes starting from solid material, e.g. by crushing, grinding or milling
Definitions
- One process when producing metal powder for powdermetallurgical purposes is as a rule a grinding operation through which the powder is given the desired grain size.
- This grinding causes a work hardening efiect, which afterwards must be removed by a heat treatment through which the compressibility of the powder will be increased.
- the heat treatment is usually carried out in reducing atmosphere, as a rule hydrogen gas, whereby the proportion of some impurities, especially oxygen and carbon, is reduced in the powder, which also aids in improving the compressibility.
- a further increasing of the compressibility would mean increased possibilities to manufacture by pressing and sintering denser details, which by means of the increased density have improved tensile strength or a possibility to obtain hitherto used densities at lower pressure, i. e. at lower cost and with less tool wearing respectively.
- Example A quantity of iron powder produced from sponge iron 2,791,498 Patented May 7, 1957 by grinding to a grain size of mesh 0.15 mm.) was divided into two lots, one of them being treated in the hitherto common way by directly annealing the powder during 1 hour at 700 C. in hydrogen atmosphere, whereas the other one was first rolled to a band according to the invention and then pulversized to the same grain size as the original powder, whereafter it was annealed during 1 hour at 700 C. in hydrogen atmosphere.
- Test pieces were pressed from the two powders at a pressure of 60.000 p. s. i. (corresponding to 4.2 kg./mm. and the density of the test pieces was measured. The following result was obtained:
- Test pieces from powder treated in the hitherto common way 6.27 g./cm.
- Test pieces from powder treated according to the invention 6.55 g./cm.
- the coldworking or compriming treatment according to this invention can also be used for quite another purpose in which case the following annealing is not necessary, namely for increasing the volume weight of the powder without substantially altering its grain size.
- Such powder could be used for 'difierent purposes, the most important of which is the manufacture of coated welding electrodes.
- Iron powder as is well known, often is incorporated in the coating of welding electrodes for the purpose of increasing the deposit rate and the yield of metal calculated on the unit length of the electrode.
- metal powder is sponge iron powder of about 100 mesh grain s1ze.
Landscapes
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Powder Metallurgy (AREA)
Description
United States Patent METHOD OF IMPROVING METAL POWDERS Nils Herman Brundin and Orjan Wiberg, Hoganas, Swe den, and Ernst Geijer, Riverton, N. 3., assignors to Aktiebolaget Hiiganiismetoder, Hoganas, Sweden, a Swedish company No Drawing. Application December 9, 1955, Serial No. 551,90
3 Claims. (Cl. 75-=-.5)
One process when producing metal powder for powdermetallurgical purposes is as a rule a grinding operation through which the powder is given the desired grain size. This grinding causes a work hardening efiect, which afterwards must be removed by a heat treatment through which the compressibility of the powder will be increased. The heat treatment is usually carried out in reducing atmosphere, as a rule hydrogen gas, whereby the proportion of some impurities, especially oxygen and carbon, is reduced in the powder, which also aids in improving the compressibility. By these methods a certain limit value of the compressibility for each quality of powder is reached. A further increasing of the compressibility would mean increased possibilities to manufacture by pressing and sintering denser details, which by means of the increased density have improved tensile strength or a possibility to obtain hitherto used densities at lower pressure, i. e. at lower cost and with less tool wearing respectively.
This invention relates to a method for such an increasing of the compressibility of metal powders. This new method is mainly characterized in that the metal powder after being ground to the desired grain size but before the following annealing is subjected to a cold working or similar compriming action without grinding, suitably to a rolling operation. The rolling is suitably carried out in such a way that a continuous band is obtained as this causes an exceedingly small deformation of the grains. The band is then again comminuted to powder of the same grain size as that powder from which the band was originally rolled. This operation can be carried out in a disintegrator and afterwards no further grinding is needed. The powder obtained in this way is then annealed in a reducing atmosphere.
Example A quantity of iron powder produced from sponge iron 2,791,498 Patented May 7, 1957 by grinding to a grain size of mesh 0.15 mm.) was divided into two lots, one of them being treated in the hitherto common way by directly annealing the powder during 1 hour at 700 C. in hydrogen atmosphere, whereas the other one was first rolled to a band according to the invention and then pulversized to the same grain size as the original powder, whereafter it was annealed during 1 hour at 700 C. in hydrogen atmosphere. Test pieces were pressed from the two powders at a pressure of 60.000 p. s. i. (corresponding to 4.2 kg./mm. and the density of the test pieces was measured. The following result was obtained:
Test pieces from powder treated in the hitherto common way, 6.27 g./cm.
Test pieces from powder treated according to the invention, 6.55 g./cm.
The coldworking or compriming treatment according to this invention can also be used for quite another purpose in which case the following annealing is not necessary, namely for increasing the volume weight of the powder without substantially altering its grain size. Such powder could be used for 'difierent purposes, the most important of which is the manufacture of coated welding electrodes. Iron powder, as is well known, often is incorporated in the coating of welding electrodes for the purpose of increasing the deposit rate and the yield of metal calculated on the unit length of the electrode. By increasing the volume weight of the iron powder used for this purpose it is possible to increase the iron content of the coating to a certain degree Without necessitating increasing the thickness of the coating and thereby the outer diameter of the welding rod.
We claim:
1. A method of increasing the volume weight of metal powder without substantially increasing its grain size which comprises cold rolling the powder in a layer of sufiicient thickness and under suflicient pressure to form a continuous layer and comminuting said layer to a powder.
2. A method as defined in claim 1 in which the metal powder is sponge iron powder of about 100 mesh grain s1ze.
3. A method as defined in claim 1 in which the layer is comminuted to a powder of the same grain size as the original powder.
References Cited in the file of this patent UNITED STATES PATENTS 2,306,665 Schwarzkoph Dec. 29, 1942
Claims (1)
1. A METHOD OF INCREASING THE VOLUME WEIGHT OF METAL POWDER WITHOUT SUBSTANTIALLY INCREASING ITS GRAIN SIZE WHICH COMPRISES COLD ROLLING THE POWDER IN A LAYER OF SUFFICIENT THICKNESS AND UNDER SUFFICIENT PRESSURE TO FORM A CONTINUOUS LAYER AND COMMINUTING SAID LAYER TO A POWDER.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US551990A US2791498A (en) | 1955-12-09 | 1955-12-09 | Method of improving metal powders |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US551990A US2791498A (en) | 1955-12-09 | 1955-12-09 | Method of improving metal powders |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US2791498A true US2791498A (en) | 1957-05-07 |
Family
ID=24203497
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US551990A Expired - Lifetime US2791498A (en) | 1955-12-09 | 1955-12-09 | Method of improving metal powders |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US2791498A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3141761A (en) * | 1962-02-23 | 1964-07-21 | Walter U Schmitt G M B H Fa Dr | Pulverized silver alloys for use in producing dental amalgams |
| US3498782A (en) * | 1966-02-18 | 1970-03-03 | Amax Specialty Metals Inc | Compactible fused and atomized metal powder |
| US20080038573A1 (en) * | 2004-03-15 | 2008-02-14 | Katsuyoshi Kondoh | Alloy Powder Raw Material and its Manufacturing Method |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2306665A (en) * | 1941-03-19 | 1942-12-29 | American Electro Metal Corp | Method of preparing ferritic iron powder for manufacturing shaped iron bodies |
-
1955
- 1955-12-09 US US551990A patent/US2791498A/en not_active Expired - Lifetime
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2306665A (en) * | 1941-03-19 | 1942-12-29 | American Electro Metal Corp | Method of preparing ferritic iron powder for manufacturing shaped iron bodies |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3141761A (en) * | 1962-02-23 | 1964-07-21 | Walter U Schmitt G M B H Fa Dr | Pulverized silver alloys for use in producing dental amalgams |
| US3498782A (en) * | 1966-02-18 | 1970-03-03 | Amax Specialty Metals Inc | Compactible fused and atomized metal powder |
| US20080038573A1 (en) * | 2004-03-15 | 2008-02-14 | Katsuyoshi Kondoh | Alloy Powder Raw Material and its Manufacturing Method |
| US7909948B2 (en) * | 2004-03-15 | 2011-03-22 | Gohsyu Co., Ltd. | Alloy powder raw material and its manufacturing method |
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