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US20030118297A1 - Optical fiber Bragg grating coating removal detection - Google Patents

Optical fiber Bragg grating coating removal detection Download PDF

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Publication number
US20030118297A1
US20030118297A1 US10/199,966 US19996602A US2003118297A1 US 20030118297 A1 US20030118297 A1 US 20030118297A1 US 19996602 A US19996602 A US 19996602A US 2003118297 A1 US2003118297 A1 US 2003118297A1
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United States
Prior art keywords
grating
coating
wavelength
fiber
forces
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Abandoned
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US10/199,966
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English (en)
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James Dunphy
James Ryan
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Individual
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Priority to US10/199,966 priority Critical patent/US20030118297A1/en
Publication of US20030118297A1 publication Critical patent/US20030118297A1/en
Priority to US10/894,153 priority patent/US6885785B2/en
Abandoned legal-status Critical Current

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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M11/00—Testing of optical apparatus; Testing structures by optical methods not otherwise provided for
    • G01M11/08—Testing mechanical properties
    • G01M11/083—Testing mechanical properties by using an optical fiber in contact with the device under test [DUT]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C35/00—Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
    • B29C35/02—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
    • B29C35/0288—Controlling heating or curing of polymers during moulding, e.g. by measuring temperatures or properties of the polymer and regulating the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28—Shaping operations therefor
    • B29C70/54—Component parts, details or accessories; Auxiliary operations, e.g. feeding or storage of prepregs or SMC after impregnation or during ageing
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
    • C03C25/10—Coating
    • C03C25/104—Coating to obtain optical fibres
    • C03C25/106—Single coatings
    • C03C25/1061—Inorganic coatings
    • C03C25/1063—Metals
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01B—MEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
    • G01B11/00—Measuring arrangements characterised by the use of optical techniques
    • G01B11/16—Measuring arrangements characterised by the use of optical techniques for measuring the deformation in a solid, e.g. optical strain gauge
    • G01B11/18—Measuring arrangements characterised by the use of optical techniques for measuring the deformation in a solid, e.g. optical strain gauge using photoelastic elements
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01D—MEASURING NOT SPECIALLY ADAPTED FOR A SPECIFIC VARIABLE; ARRANGEMENTS FOR MEASURING TWO OR MORE VARIABLES NOT COVERED IN A SINGLE OTHER SUBCLASS; TARIFF METERING APPARATUS; MEASURING OR TESTING NOT OTHERWISE PROVIDED FOR
    • G01D5/00—Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable
    • G01D5/26—Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light
    • G01D5/32—Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light
    • G01D5/34—Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light the beams of light being detected by photocells
    • G01D5/353—Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light the beams of light being detected by photocells influencing the transmission properties of an optical fibre
    • G01D5/35306—Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light the beams of light being detected by photocells influencing the transmission properties of an optical fibre using an interferometer arrangement
    • G01D5/35309—Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light the beams of light being detected by photocells influencing the transmission properties of an optical fibre using an interferometer arrangement using multiple waves interferometer
    • G01D5/35316—Mechanical means for transferring the output of a sensing member; Means for converting the output of a sensing member to another variable where the form or nature of the sensing member does not constrain the means for converting; Transducers not specially adapted for a specific variable characterised by optical transfer means, i.e. using infrared, visible, or ultraviolet light with attenuation or whole or partial obturation of beams of light the beams of light being detected by photocells influencing the transmission properties of an optical fibre using an interferometer arrangement using multiple waves interferometer using a Bragg gratings
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M11/00—Testing of optical apparatus; Testing structures by optical methods not otherwise provided for
    • G01M11/08—Testing mechanical properties
    • G01M11/083—Testing mechanical properties by using an optical fiber in contact with the device under test [DUT]
    • G01M11/086—Details about the embedment of the optical fiber within the DUT
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00—Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/02—Optical fibres with cladding with or without a coating
    • G02B6/02057—Optical fibres with cladding with or without a coating comprising gratings
    • G02B6/02076—Refractive index modulation gratings, e.g. Bragg gratings
    • G02B6/02195—Refractive index modulation gratings, e.g. Bragg gratings characterised by means for tuning the grating
    • G02B6/022—Refractive index modulation gratings, e.g. Bragg gratings characterised by means for tuning the grating using mechanical stress, e.g. tuning by compression or elongation, special geometrical shapes such as "dog-bone" or taper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/06—Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts
    • B29K2105/08—Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts of continuous length, e.g. cords, rovings, mats, fabrics, strands or yarns
    • B29K2105/10—Cords, strands or rovings, e.g. oriented cords, strands or rovings
    • B29K2105/101—Oriented
    • B29K2105/108—Oriented arranged in parallel planes and crossing at substantial angles
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/44—Resins; Plastics; Rubber; Leather
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00—Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/02—Optical fibres with cladding with or without a coating
    • G02B6/02057—Optical fibres with cladding with or without a coating comprising gratings
    • G02B6/02076—Refractive index modulation gratings, e.g. Bragg gratings
    • G02B6/0208—Refractive index modulation gratings, e.g. Bragg gratings characterised by their structure, wavelength response
    • G02B6/021—Refractive index modulation gratings, e.g. Bragg gratings characterised by their structure, wavelength response characterised by the core or cladding or coating, e.g. materials, radial refractive index profiles, cladding shape
    • G02B6/02104—Refractive index modulation gratings, e.g. Bragg gratings characterised by their structure, wavelength response characterised by the core or cladding or coating, e.g. materials, radial refractive index profiles, cladding shape characterised by the coating external to the cladding, e.g. coating influences grating properties

Definitions

  • This invention relates to smart structures and, more particularly, to optical corrosion detection.
  • Objects of the invention include provision of an optical sensor which detects corrosion.
  • an optical sensor comprises an optical fiber; a fiber grating embedded within the fiber having a reflection wavelength bandwidth of a reflectivity profile for reflecting incident light; a coating of a material having a predetermined thickness and being around the perimeter and along the length of the fiber grating; the coating exerting forces radially inward around and along the grating so as to cause the wavelength bandwidth of the reflectivity profile of the grating to become broader than it would be without the coating; and the forces on the grating being reduced when the coating is at least partially removed, thereby causing the wavelength bandwidth of the reflectivity profile of the grating to narrow.
  • the forces from the coating also cause a peak reflection wavelength of the grating to exhibit a wavelength shift from a value that the peak reflection wavelength would be at without the coating and wherein the wavelength shift is reduced when the coating is at least partially removed.
  • the coating comprises aluminum.
  • the invention represents an advancement in smart structure technology which allows for the detection of corrosion in structures by the discovery that a grating coated with a material, such as aluminum, causes the grating reflectivity profile to broaden and shift.
  • the amount of broadening and shifting which occurs can be adjusted by the process chosen to apply the coating to the fiber grating sensor and the material the coating is made from.
  • the invention is lightweight, inexpensive, and easy to install and has high sensitivity to corrosion.
  • the sensor is easily coupled with other smart sensor technology such as temperature and/or strain sensors which also use fiber Bragg gratings.
  • FIG. 1 is a diagram of a Bragg grating in an optical fiber which is coated with an aluminum coating, in accordance with the present invention.
  • FIG. 2 is a cross-sectional view of an optical fiber Bragg grating showing a core, a cladding, and an aluminum coating, in accordance with the present invention.
  • FIG. 3 is a graph showing the reflected optical spectrum of a Bragg grating before and after application of the coating of FIG. 1, in accordance with the present invention.
  • a light source 10 provides an optical signal 12 to a beam splitter 14 which passes a predetermined amount of light 16 into an optical fiber 18 .
  • the optical signal 16 is incident on a Bragg grating 20 which is impressed within the core of the optical fiber 18 .
  • a fiber Bragg grating as is known, is a periodic refractive index variation which reflects a narrow wavelength band of light and passes all other wavelengths, thereby exhibiting a narrow wavelength reflectivity profile, as is discussed in U.S. Pat. No. 4,725,110 to Glenn et al.
  • a portion 22 of the light 16 is reflected off the grating 20 , and the remaining wavelengths are passed through the grating 20 as indicated by the output light 24 .
  • the light 24 exits the fiber 18 and is incident on a detector 26 , which provides an electrical signal on a line 28 indicative of the intensity of the light 24 incident thereon.
  • the reflected light 22 exits the fiber 18 and is incident on the beam splitter 14 which reflects a predetermined portion of the light 22 , as indicated by a line 30 , onto a detector 32 .
  • the detector 32 provides an electrical signal on a line 34 indicative of the intensity of the light 30 incident thereon.
  • the fiber grating 20 is surrounded by a coating 40 made of, e.g., aluminum (methods for coating are discussed hereinafter).
  • a cross-sectional view of the fiber grating 20 includes a fiber core 42 , made of germania-doped silica, having a diameter of about 6 to 9 microns.
  • a cladding 44 made of pure silica having an outer diameter of about 125 microns.
  • the outer coating 40 of aluminum having an outer diameter of about 196 microns. Other materials and diameters for the core, cladding, and coating may be used if desired.
  • the wavelength broadening effect is due to small non-uniform changes in the refractive index of the fiber caused by pressure or forces (also known as “microbends”) exerted by the aluminum coating 40 on the cladding 44 and the core 42 , as indicated by lines 46 .
  • Such small non-uniformities can occur naturally as grain boundaries when the aluminum is cooled on the surface of the glass fiber.
  • non-uniformities are due to the fact that the coating 40 (FIG. 2) is not perfectly uniform around the circumference (or perimeter) of the cladding 44 , and thus, pressure 46 exerted by the coating 40 is not uniformly applied.
  • the coating 40 is not perfectly uniform in thickness along the longitudinal axis or length of the grating 20 (FIG.
  • pressure 46 exerted on the grating 20 will randomly vary along the length of the grating 20 , thereby also contributing to such non-uniformities.
  • the coating therefore causes a random pressure gradient along the longitudinal axis of the grating 20 (and also circumferentially around the grating) which causes an associated random variation in refractive index.
  • the microbends disrupt the smooth sinusoidal periodic refractive index variation which creates the narrow reflectivity profile of the typical narrow-band Bragg grating.
  • Such pressure gradient and the associated refractive index change can also reduce the reflection efficiency (i.e., the peak reflectivity) of the grating 20 from a reflectivity R 1 for an uncoated grating to a lower reflectivity R 2 for a coated grating due to the broadening of the wavelength reflectivity profile.
  • the reflection efficiency i.e., the peak reflectivity
  • the wavelength shift ⁇ s is caused by a change in the overall force exerted on the grating from that which exists in an uncoated grating.
  • the greater the overall force exerted on the grating by the coating the larger the wavelength shift ⁇ s will be.
  • the amount of coating removal needed before the grating will exhibit a change in the grating reflectivity profile depends on the initial force applied to the grating by the coating, the stiffness of coating material, and the thickness of the coating remaining, and can be easily determined by those skilled in the art.
  • the wavelength shift ⁇ s is due to an overall average force exerted by the coating on the grating and the bandwidth increase is caused by the aforementioned microbends (or non-uniform forces applied to the grating).
  • the process used for coating the grating and the type of coating material used determines the amount of wavelength shift ⁇ s and the amount of narrowing of the reflectivity profile which occurs.
  • the fiber is coated with aluminum when the fiber is at the melting temperature of aluminum, e.g., by dipping the fiber into molten aluminum at temperature of about 650° C. then removing the fiber to facilitate cooling and adhesion of the coating to the surface of the fiber, the large difference in thermal expansion coefficients between fiber and aluminum cause a large overall force to be exerted on the fiber during cooling.
  • This technique is known as “freeze coating.”
  • the average wavelength shift ⁇ s may be of the order of ⁇ 4.9 nm due to the compressive strain effect of the aluminum along the length and around the circumference of the optical fiber after cooling occurs.
  • the increase in the reflection bandwidth of the grating e.g., the full-width-half-max. value
  • the increase in the reflection bandwidth of the grating may be about a factor of 3 or less, e.g., an effective increase from about 0.17 nm to 0.55 nm or less.
  • the cooling temperature gradient for the fiber is not as large and, thus, the overall average force exerted on the fiber is not as large as the previously discussed dipping technique. Accordingly, the wavelength shift ⁇ s is smaller. Also, when using such a process, the coating tends to be quite smooth and uniform. As such, the non-uniform forces or microbends are less and, thus, the change in reflection bandwidth is less, than the aforementioned dipping technique.
  • the source 10 may be a broadband light source and the detector 32 may be an optical spectrometer which provides an electrical signal 34 indicative of the wavelength reflectivity profile, i.e., the reflected wavelengths and the associated intensities thereof.
  • the source 10 may be a variable source as used in an active wavelength scan/interrogation technique, such as that described in copending U.S. patent application Ser. No. 08/129,217, entitled “Diagnostic System for Fiber Grating Sensors.”
  • any other means of analyzing the optical output signals 30 or 24 may be used to detect the changes in the optical output signals due to corrosion.
  • the sensing technique is not critical to the present invention.
  • an optional fiber grating 60 which is matched to the reflectivity profile of the grating 20 without a coating, may be placed between the detector 32 and the beamsplitter 14 , in the path of the light 30 and the grating 20 coated with the technique discussed hereinbefore that minimizes wavelength shift. In that case, when the grating 20 is coated (and the reflectivity profile is broad), the reflected light 22 and 30 will also be broadband.
  • the grating 60 has a narrower reflectivity profile than the incident light 30 , a portion of the light 30 will pass through the grating 60 and be seen at the detector 32 . Conversely, when the coating is removed from the grating 20 , the reflectivity profiles of the two gratings 20 , 60 match and no (or minimal) light is passed to the detector 32 .
  • the two gratings 20 , 60 may be matched and coated, with only the grating 20 being exposed to corrosion. In that case, light will be minimized when no corrosion exists and, when the coating on the grating 20 corrodes, the light seen by the detector will be maximized due to the higher reflectivity of the uncoated fiber.
  • a material other than aluminum may be used as the coating around the grating, provided such coating either corrodes, evaporates, thins, or in some other way is removed partially of completely from coating the grating so as to reduce the forces exerted on the grating. Therefore, the invention may be used to detect the partial or complete removal of any coating surrounding a grating, provided a predetermined criteria of changes in overall average force and non-uniformity of forces on the grating are satisfied, as discussed hereinbefore.
  • a portion of the grating length may be coated.

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  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Health & Medical Sciences (AREA)
  • Mechanical Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Composite Materials (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Thermal Sciences (AREA)
  • Optics & Photonics (AREA)
  • Optical Fibers, Optical Fiber Cores, And Optical Fiber Bundles (AREA)
  • Optical Transform (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Length Measuring Devices By Optical Means (AREA)
  • Measuring Temperature Or Quantity Of Heat (AREA)
US10/199,966 1994-11-29 2002-07-19 Optical fiber Bragg grating coating removal detection Abandoned US20030118297A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US10/199,966 US20030118297A1 (en) 1994-11-29 2002-07-19 Optical fiber Bragg grating coating removal detection
US10/894,153 US6885785B2 (en) 1994-11-29 2004-07-19 Optical fiber bragg grating coating removal detection

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US34605994A 1994-11-29 1994-11-29
US10/199,966 US20030118297A1 (en) 1994-11-29 2002-07-19 Optical fiber Bragg grating coating removal detection

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US (2) US20030118297A1 (fr)
EP (1) EP0795117B1 (fr)
JP (1) JP3410101B2 (fr)
KR (1) KR100322430B1 (fr)
CN (1) CN1090317C (fr)
DE (1) DE69507635T2 (fr)
DK (1) DK0795117T3 (fr)
GR (1) GR3029748T3 (fr)
WO (1) WO1996017223A1 (fr)

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US20020178756A1 (en) * 2001-04-24 2002-12-05 Davis Monica K. Method for manufacturing optical gratings
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US9192307B2 (en) 2002-10-07 2015-11-24 Vascular Imaging Corporation Systems and methods for minimally-invasive optical-acoustic imaging
US9198581B2 (en) 2005-11-22 2015-12-01 Vascular Imaging Corporation Optical imaging probe
WO2016003911A1 (fr) * 2014-06-30 2016-01-07 Baker Hughes Incorporated Systèmes et dispositifs de détection de corrosion et de dépôt pour des applications de pétrole et de gaz
US9532766B2 (en) 1998-03-05 2017-01-03 Vascular Imaging Corporation Optical-acoustic imaging device
US9579026B2 (en) 2008-10-02 2017-02-28 Vascular Imaging Corporation Optical ultrasound receiver
US20180252555A1 (en) * 2015-11-24 2018-09-06 Halliburton Energy Services, Inc. Fiber Optic Sensing Using Soluble Layers
US20190011491A1 (en) * 2017-07-06 2019-01-10 Palo Alto Research Center Incorporated Optical monitoring for power grid systems
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US11585692B2 (en) 2019-10-24 2023-02-21 Palo Alto Research Center Incorporated Fiber optic sensing system for grid-based assets
US11719559B2 (en) 2019-10-24 2023-08-08 Palo Alto Research Center Incorporated Fiber optic sensing system for grid-based assets
US11829294B2 (en) 2018-12-21 2023-11-28 Home Box Office, Inc. Preloaded content selection graph generation

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DE10137011C2 (de) * 2001-07-28 2003-12-04 Aesculap Ag & Co Kg Medizinisches Implantatsystem
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EP0795117B1 (fr) 1999-01-27
CN1166872A (zh) 1997-12-03
EP0795117A1 (fr) 1997-09-17
KR100322430B1 (ko) 2002-03-08
US6885785B2 (en) 2005-04-26
JP3410101B2 (ja) 2003-05-26
GR3029748T3 (en) 1999-06-30
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CN1090317C (zh) 2002-09-04
JPH11514432A (ja) 1999-12-07

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