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US1829750A - Stencil sheet - Google Patents

Stencil sheet Download PDF

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Publication number
US1829750A
US1829750A US472500A US47250030A US1829750A US 1829750 A US1829750 A US 1829750A US 472500 A US472500 A US 472500A US 47250030 A US47250030 A US 47250030A US 1829750 A US1829750 A US 1829750A
Authority
US
United States
Prior art keywords
esters
acid
naphthenic acid
polysaccharides
stencil sheet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US472500A
Inventor
Horii Shinjiro
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Application granted granted Critical
Publication of US1829750A publication Critical patent/US1829750A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B41PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41NPRINTING PLATES OR FOILS; MATERIALS FOR SURFACES USED IN PRINTING MACHINES FOR PRINTING, INKING, DAMPING, OR THE LIKE; PREPARING SUCH SURFACES FOR USE AND CONSERVING THEM
    • B41N1/00Printing plates or foils; Materials therefor
    • B41N1/24Stencils; Stencil materials; Carriers therefor
    • B41N1/243Stencils; Stencil materials; Carriers therefor characterised by the ink pervious sheet, e.g. yoshino paper
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S428/00Stock material or miscellaneous articles
    • Y10S428/908Impression retention layer, e.g. print matrix, sound record
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/249921Web or sheet containing structurally defined element or component
    • Y10T428/249953Composite having voids in a component [e.g., porous, cellular, etc.]
    • Y10T428/249962Void-containing component has a continuous matrix of fibers only [e.g., porous paper, etc.]
    • Y10T428/249963And a force disintegratable component [e.g., stencil sheet, etc.]
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/31504Composite [nonstructural laminate]
    • Y10T428/31971Of carbohydrate
    • Y10T428/31975Of cellulosic next to another carbohydrate
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/31504Composite [nonstructural laminate]
    • Y10T428/31971Of carbohydrate
    • Y10T428/31975Of cellulosic next to another carbohydrate
    • Y10T428/31978Cellulosic next to another cellulosic
    • Y10T428/31982Wood or paper

Definitions

  • My invention relates to improvements in stencil sheets for use 1n duplicating manuscript and typewritten documents, drawings of polysaccharides and a tempering agent,.
  • the 2 stencil sheet comprises a base of fibrous material having a coating including esters of polysaccharides, a metallic soap of naphthenic acid, a suitable tempering agent.
  • the stencil sheet pro-.
  • esters of polysaccharides such as starch acetate. mannan acetate. cellulose acetate. cellulose stearate and cellulose ni-- trate, are dissolved in a Volatile solvent. such as ether. alcohol. acetone. ethvl acetate. butyl acetate, butyl alcohol. benzine. benzol or a mixture of them. and then the solution is mixed with a solution of a metallic soap of naphthenic acid dissolved in a suitable tion is coated on a base material such as J apane e yoshino paper.
  • a Volatile solvent such as ether. alcohol. acetone. ethvl acetate. butyl acetate, butyl alcohol. benzine. benzol or a mixture of them.
  • the proportions of the ingredients may vary according to several circumstances. By the way of example particulars are given as follows Em I Parts by weight Fatty acid of Tsubaki oil 5 Paraffin oil. 5
  • Example II Parts by weight Cellulose acetate Mannan acetate 5 Acetone 50 Cyclohexanon 1O Ethyl acetate 20 Calcium naphthenate 1 5 Ethyl naphthenate 10 Naphthenic acid glycerides 1-0 Chlorinated naphthalene 5 Fatty acid of Tsubaki oil 5
  • the above coating compositions may be diluted with any suitable solvents to the desired consistency.
  • esters of polysaccharides is intended to include not only one of definite esters of polysaccharides, but also a mixture of them.
  • a stencil sheet adapted for stencilizing by pressure comprising, a base of fibrous material having a coating including esters of polysaccharides, a metallic soap of naphthenic acid, and a tempering agent.
  • a stencil sheet adapted for stencilizing by pressure comprising a base of fibrous material having a coating including esters of polysaccharides, a metallic soap of naphthenic acid, an alkyl ester of naphthenic acid, and a tempering agent.
  • a stencil sheet adapted for stencilizing by pressure comprising a base of fibrous material having aqcoating including esters of polysaccharides, a metallic soap of naphthenic acid, ethyl naphthenate, and a tempering agent.
  • a stencil sheet adapted for stenciliz- SHINJIRO HOB-II.

Landscapes

  • Printing Plates And Materials Therefor (AREA)

Description

Patented Nov. 3, 1931 SH INJ'IRO HORII, 0F KANDA-KU, TOKYO, JAPAN STENCIL SHEET No Drawing. Application filed August 1, 1930, Serial No 472,500, and in Japan June 28, 1930.
My invention relates to improvements in stencil sheets for use 1n duplicating manuscript and typewritten documents, drawings of polysaccharides and a tempering agent,.
such as naphthenic acid glycerides, chlorinated naphthalene, fatty acid of Tsubaki oil or a mixture of them.
It has also been proposed to produce a stencil sheet of loose-fibered tissue coated with I cellulose acetate plastified and stabilized by acetanilid, combined with a softening agent, such as glycerine and diethyl phthalate.
According to the present invention the 2 stencil sheetcomprises a base of fibrous material having a coating including esters of polysaccharides, a metallic soap of naphthenic acid, a suitable tempering agent.
A metallic soap of napthenic acid is prepared by heating and combining together the equivalent portions of naphthenic acid and an oxide of metal, or by the double-decomposition of a solution of an alkali soap of naphthenic acid with a solution of some salt of metals, such as aluminum, iron, calcium or magnesium.
The film of cellulose esters as well as of the other esters of polysaccharides, however, is highly unstable and considerable deteriorates when stored for a long period of time.
Moreover, it is extremely sensitive to sunlight. A clear film exposed for a few days only becomes brittle so that it will not withstand mild bending even without cracking. The use of oils and plasticizers will extend the life, but eventually failure will occur. The fatty oils becomerancid on exposure and make the film sticky. Consequently, a stencil sheet having such a coating is unstable for ,the esters.
It is common practice to neutralize the free acid and the acid which may be produced afterwards with feeble alkalies, such as urea and other amines, but these substances make them unsafe because of producing a harmful product which decreases the colloidal propcity of the esters, and acts to decompose the esters, as the majority of the stabilizing ma terials exert an alkaline reaction upon the esters. The choice of the stabilizing material is in practice preferably restricted to such as will not harmfully affect the coating of the stencil sheet of the kind above referred to. Now, it has been found that metallic soaps of naphthenic acid, for example calcium naphthenate, will overcome the above defects. The metallic soaps of naphthenic acid are the most efiective stabilizers for the esters of polysaccharides. They exert no adverse action on the esters of polysaccharides U and combine with the free acid present in the esters, forming salts of the metals in volved and liberating the naphthenicacid. The naphthenic acid produced is a feeble acid of saturated constitution and exerts no saponifying action on the esters of polysaccharides, improving the durability and toughness of the cellulosic film. Metallic soaps of naphthenic acid and naphthenic acid also are the plasticizers for the esters of polysaccharides. Furthermore, it has been found to be more effective to use them in combination with an alkyl ester of naphthenic tempering agents, but the alkali soap are weak alkalies, and they act on the cellulose esters, decreasing their colloidal property. The alkali soaps of oleic acid combine with the free acid present in the'cellulose esters, and there will be produced the salts of the metals and free oleicacid. The oleic acid is a stronger acid than naphthenic acid and is an unsaturated one. Consequently, it accelerates the ranciditv of the oils present and also exerts the saponification of the cellulose esters of the coating. Therefore. the use of alkali soaps. or other soaps of fatty acids, gives no good results.
As already described. the stencil sheet pro-.
duced in accordance with the present invention is very durable. owing to its stability. and the stencil is also remarkably soft and pliable because of the combined use of an alkyl ester of naphthenic acid with a metallic soap of naphthenic acid giving a clear stencil by the pressure of a writing machine.
In carrying out the invention into practice. first the esters of polysaccharides. such as starch acetate. mannan acetate. cellulose acetate. cellulose stearate and cellulose ni-- trate, are dissolved in a Volatile solvent. such as ether. alcohol. acetone. ethvl acetate. butyl acetate, butyl alcohol. benzine. benzol or a mixture of them. and then the solution is mixed with a solution of a metallic soap of naphthenic acid dissolved in a suitable tion is coated on a base material such as J apane e yoshino paper.
The proportions of the ingredients may vary according to several circumstances. By the way of example particulars are given as follows Em I Parts by weight Fatty acid of Tsubaki oil 5 Paraffin oil. 5
Ewample II Parts by weight Cellulose acetate Mannan acetate 5 Acetone 50 Cyclohexanon 1O Ethyl acetate 20 Calcium naphthenate 1 5 Ethyl naphthenate 10 Naphthenic acid glycerides 1-0 Chlorinated naphthalene 5 Fatty acid of Tsubaki oil 5 The above coating compositions may be diluted with any suitable solvents to the desired consistency.
The term esters of polysaccharides is intended to include not only one of definite esters of polysaccharides, but also a mixture of them.
lVhat I claim is 1. A stencil sheet adapted for stencilizing by pressure, comprising, a base of fibrous material having a coating including esters of polysaccharides, a metallic soap of naphthenic acid, and a tempering agent.
2. A stencil sheet adapted for stencilizing by pressure, comprising a base of fibrous material having a coating including esters of polysaccharides, a metallic soap of naphthenic acid, an alkyl ester of naphthenic acid, and a tempering agent.
3. A stencil sheet adapted for stencilizing by pressure, comprising a base of fibrous material having aqcoating including esters of polysaccharides, a metallic soap of naphthenic acid, ethyl naphthenate, and a tempering agent.
4. A stencil sheet adapted for stenciliz- SHINJIRO HOB-II.
Cellulose nitrate 20 Alcohol 2O Ethyl acetate; 30 Butyl acetate 10 Calcium naphthenate 1 5 Ethyl naphthenate 5 Cyclohexanon "5 20 Benzol 2O Butyl phthalate A 2 Naphthenic acid glycerides 15 Tsubaki oil 10
US472500A 1930-06-28 1930-08-01 Stencil sheet Expired - Lifetime US1829750A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1829750X 1930-06-28

Publications (1)

Publication Number Publication Date
US1829750A true US1829750A (en) 1931-11-03

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2756161A (en) * 1952-07-30 1956-07-24 Horii Shinjiro Stencil sheets

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2756161A (en) * 1952-07-30 1956-07-24 Horii Shinjiro Stencil sheets

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