UA81513U - Process for synthesis of thallium selenogallate - Google Patents
Process for synthesis of thallium selenogallateInfo
- Publication number
- UA81513U UA81513U UAA201211109U UAU201211109U UA81513U UA 81513 U UA81513 U UA 81513U UA A201211109 U UAA201211109 U UA A201211109U UA U201211109 U UAU201211109 U UA U201211109U UA 81513 U UA81513 U UA 81513U
- Authority
- UA
- Ukraine
- Prior art keywords
- ampoule
- temperature
- furnace
- working zone
- selenogallate
- Prior art date
Links
- 230000015572 biosynthetic process Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 238000003786 synthesis reaction Methods 0.000 title abstract 2
- BKVIYDNLLOSFOA-UHFFFAOYSA-N thallium Chemical compound [Tl] BKVIYDNLLOSFOA-UHFFFAOYSA-N 0.000 title abstract 2
- 229910052716 thallium Inorganic materials 0.000 title abstract 2
- 239000003708 ampul Substances 0.000 abstract 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000003466 welding Methods 0.000 abstract 1
Landscapes
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
A process for synthesis of thallium selenogallate comprises the placing of elementary components to ampoule of quartz glass, vacuuming and ampoule welding, heating of components and cooling. Components are placed in one end of horizontally adjusted ampoule, which is placed to working zone of a furnace, and another end of ampoule is placed outside of working zone of the furnace, ampoule content is heated to temperature of 270-290 °C, held at this temperature for 4-6 hours and after that heated to temperature of 700-750 °C, the ampoule is introduced to working zone of the furnace with velocity of 3-4 cm/h, the temperature of working zone of the furnace is raised to temperature of 830-850 °C and held at this temperature for 2-3 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| UAA201211109U UA81513U (en) | 2012-09-24 | 2012-09-24 | Process for synthesis of thallium selenogallate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| UAA201211109U UA81513U (en) | 2012-09-24 | 2012-09-24 | Process for synthesis of thallium selenogallate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA81513U true UA81513U (en) | 2013-07-10 |
Family
ID=52024486
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA201211109U UA81513U (en) | 2012-09-24 | 2012-09-24 | Process for synthesis of thallium selenogallate |
Country Status (1)
| Country | Link |
|---|---|
| UA (1) | UA81513U (en) |
-
2012
- 2012-09-24 UA UAA201211109U patent/UA81513U/en unknown
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