SU64311A1 - The method of obtaining adhesive substances from proteins - Google Patents
The method of obtaining adhesive substances from proteinsInfo
- Publication number
- SU64311A1 SU64311A1 SU516A SU322444A SU64311A1 SU 64311 A1 SU64311 A1 SU 64311A1 SU 516 A SU516 A SU 516A SU 322444 A SU322444 A SU 322444A SU 64311 A1 SU64311 A1 SU 64311A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- proteins
- precipitate
- adhesive substances
- obtaining adhesive
- acid
- Prior art date
Links
- 102000004169 proteins and genes Human genes 0.000 title description 9
- 108090000623 proteins and genes Proteins 0.000 title description 9
- 239000000853 adhesive Substances 0.000 title description 4
- 230000001070 adhesive effect Effects 0.000 title description 4
- 238000000034 method Methods 0.000 title description 2
- 239000000126 substance Substances 0.000 title 1
- 239000002244 precipitate Substances 0.000 description 8
- 235000018102 proteins Nutrition 0.000 description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 239000007864 aqueous solution Substances 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 210000000988 bone and bone Anatomy 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- -1 alkyl naphthalene sulfonic acid Chemical compound 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 239000012460 protein solution Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 102000009027 Albumins Human genes 0.000 description 1
- 108010088751 Albumins Proteins 0.000 description 1
- 235000017399 Caesalpinia tinctoria Nutrition 0.000 description 1
- 108010082495 Dietary Plant Proteins Proteins 0.000 description 1
- 241000388430 Tara Species 0.000 description 1
- 235000021120 animal protein Nutrition 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000010633 broth Nutrition 0.000 description 1
- 239000005018 casein Substances 0.000 description 1
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
- 235000021240 caseins Nutrition 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
Landscapes
- Compounds Of Unknown Constitution (AREA)
- Treatment Of Sludge (AREA)
Description
Большое распространение в качестве клеющих материа; ов имеют, как известно, белки, получаемые, например, вываркой костей, кожи, а также в виде крови животных в консервированном или сухом виде (альбумин) или в виде казеина из молока и т. д. Кроме животных белков , наход т применение также и растительные белки. Большинство этих белков растворимо в воде и примен етс в водных растворах. При выварке костей или кожи получаютс довольно разбавленные растворы (бульоны), которые необходимо выпаривать, с целью получени кле , до высокой концентрации . Это св зано с расходом топлива и снижением качества кле .Large spread as adhesive materials; s are, as is well known, proteins obtained, for example, by evaporation of bones, skin, and also in the form of animal blood in canned or dry form (albumin) or in the form of casein from milk, etc. In addition to animal proteins, there are also and vegetable proteins. Most of these proteins are soluble in water and are used in aqueous solutions. By drying out bones or skin, rather dilute solutions (broths) are obtained, which must be evaporated, in order to obtain glue, to a high concentration. This is associated with fuel consumption and lower adhesive quality.
Предлагаемый способ получени клеющих веществ состоит в том, что водные растворы белков осаждают алкилнафталинсульфокислотой , полученный осадок промывают водой, а затем его расплавл ют.The proposed method for producing adhesives is that the aqueous solutions of the proteins precipitate with alkyl naphthalene sulfonic acid, the precipitate is washed with water, and then it is melted.
Вместо алкилнафталинсульфокислоты можно примен ть её соли с добавкой какой-либо минеральЕОй кислоты, лучше всего серной.Instead of alkylnaphthalenesulfonic acid, its salts can be used with the addition of a mineral EO acid, preferably sulfuric acid.
Пример 1. К 100 ч. раствора белка. полученного вываркой костей пли кожи, добавл ют на холоду при посто нном перемешивании 3--5% алкинафталинсульфокислоты , по отношению к белку, содержащемус в растворе.Example 1. To 100 hours protein solution. obtained by boiling out the bones of the skin or skin, add 3--5% alkyne-naphthalene sulfonic acid, with constant stirring, relative to the protein contained in the solution.
Из раствора выпадает хлопьевидный осадок. Дав отсто тьс последнему , с него сливают жидкость и промывают осадок холодной водой 2-3 раза, или же в начале осадок нагревают до 50 - 60 (дл ускорени отделени воды), с него вновь сливают выделившуюс жидкость и только после этого перенос т осадок в тару.A flocculent precipitate falls out of solution. After allowing to settle last, the liquid is drained from it and the precipitate is washed with cold water 2-3 times, or at the beginning the precipitate is heated to 50-60 (to accelerate the separation of water), the separated liquid is again drained and only after that the precipitate is transferred to tara
Пример 2. К 100 ч. раствора белка на холоду добавл ют 5-8% соли алкилнафталинсульфокислоты, по отношению к белку. При употреблении водных растворов реактива делаетс соответствующий расчёт количества его, необходимого дл осаждени . После энергичного перемешивани в масс} добавл ют струей при размешивании 10-процентный раствор серной кислоты до тех пор, пока не перестанет выпадать осадок, дл чего бывает достаточно 2-3%, по отношению к белку, 100-процентнои серной кислоты. № 64311 Обработка осадка производитс по вышеописанному. Продукт может быть высушен, причём на сушку его расходуетс немного тепла. Предмет изобретени 1. Способ получени клёющих веш,еств из водных растворов белков , отличающийс тем, что водные растворы белков осаждают алкилнафталинсульфокислотой, полученный осадок промывают, после чего его расплавл ют, 2. Видоизменение способа по п. 1, отличающеес тем, что вме алкилнафталинсульфокислоты примен ют ее соли с добавкой какой-либо минеральной кислоты, например серной.Example 2. To 100 parts of a cold protein solution, 5-8% of an alkyl naphthalene sulfonic acid salt are added, relative to the protein. When using aqueous solutions of the reagent, an appropriate calculation is made of the quantity required for precipitation. After vigorous stirring in the masses, a 10% solution of sulfuric acid is added by a stream while stirring until the precipitate ceases to fall, for which 2-3% is sufficient, relative to protein, 100% sulfuric acid. No. 64311 Sludge is treated as described above. The product can be dried, and a little heat is used to dry it. Subject of the invention 1. A method for producing agglomerates from aqueous solutions of proteins, characterized in that aqueous solutions of proteins are precipitated by alkylnaphthalenesulfonic acid, the precipitate is washed, after which it is melted 2. A method modified according to claim 1, characterized in that its salts are used with the addition of any mineral acid, for example sulfuric.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU516A SU64311A1 (en) | 1943-07-17 | 1943-07-17 | The method of obtaining adhesive substances from proteins |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU516A SU64311A1 (en) | 1943-07-17 | 1943-07-17 | The method of obtaining adhesive substances from proteins |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1773120A Addition SU459544A2 (en) | 1972-04-14 | 1972-04-14 | Semiautomatic pom-pom |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU64311A1 true SU64311A1 (en) | 1944-11-30 |
Family
ID=48245065
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU516A SU64311A1 (en) | 1943-07-17 | 1943-07-17 | The method of obtaining adhesive substances from proteins |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU64311A1 (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2558365C2 (en) * | 2009-03-06 | 2015-08-10 | Байополимер Текнолоджиз, Лтд. | Emulsions and adhesives containing proteins, producing and using them |
| US9816019B2 (en) | 2010-06-07 | 2017-11-14 | Evertree | Protein-containing adhesives, and manufacture and use thereof |
| US9873823B2 (en) | 2012-07-30 | 2018-01-23 | Evertree | Protein adhesives containing an anhydride, carboxylic acid, and/or carboxylate salt compound and their use |
| US10125295B2 (en) | 2011-09-09 | 2018-11-13 | Evertree | Protein-containing adhesives, and manufacture and use thereof |
| US10160842B2 (en) | 2009-03-06 | 2018-12-25 | Evertree | Protein-containing foams, manufacture and use thereof |
| US11028298B2 (en) | 2011-09-09 | 2021-06-08 | Evertree | Protein-containing adhesives, and manufacture and use thereof |
-
1943
- 1943-07-17 SU SU516A patent/SU64311A1/en active
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2558365C2 (en) * | 2009-03-06 | 2015-08-10 | Байополимер Текнолоджиз, Лтд. | Emulsions and adhesives containing proteins, producing and using them |
| US9909044B2 (en) | 2009-03-06 | 2018-03-06 | Evertree | Protein-containing emulsions and adhesives, and manufacture and use thereof |
| US10160842B2 (en) | 2009-03-06 | 2018-12-25 | Evertree | Protein-containing foams, manufacture and use thereof |
| US10745601B2 (en) | 2009-03-06 | 2020-08-18 | Evertree | Protein-containing emulsions and adhesives, and manufacture and use thereof |
| US9816019B2 (en) | 2010-06-07 | 2017-11-14 | Evertree | Protein-containing adhesives, and manufacture and use thereof |
| US10465103B2 (en) | 2010-06-07 | 2019-11-05 | Evertree | Protein-containing adhesives, and manufacture and use thereof |
| US10913880B2 (en) | 2010-06-07 | 2021-02-09 | Evertree | Protein-containing adhesives, and manufacture and use thereof |
| US10125295B2 (en) | 2011-09-09 | 2018-11-13 | Evertree | Protein-containing adhesives, and manufacture and use thereof |
| US11028298B2 (en) | 2011-09-09 | 2021-06-08 | Evertree | Protein-containing adhesives, and manufacture and use thereof |
| US11072731B2 (en) | 2011-09-09 | 2021-07-27 | Evertree | Protein-containing adhesives, and manufacture and use thereof |
| US9873823B2 (en) | 2012-07-30 | 2018-01-23 | Evertree | Protein adhesives containing an anhydride, carboxylic acid, and/or carboxylate salt compound and their use |
| US10526516B2 (en) | 2012-07-30 | 2020-01-07 | Evertree | Protein adhesives containing an anhydride, carboxylic acid, and/or carboxylate salt compound and their use |
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