SU511328A1 - The method of obtaining anion exchange resin - Google Patents
The method of obtaining anion exchange resinInfo
- Publication number
- SU511328A1 SU511328A1 SU2040099A SU2040099A SU511328A1 SU 511328 A1 SU511328 A1 SU 511328A1 SU 2040099 A SU2040099 A SU 2040099A SU 2040099 A SU2040099 A SU 2040099A SU 511328 A1 SU511328 A1 SU 511328A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- exchange resin
- anion exchange
- obtaining anion
- obtaining
- water
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 3
- 239000003957 anion exchange resin Substances 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000012153 distilled water Substances 0.000 description 2
- 101100380569 Neurospora crassa (strain ATCC 24698 / 74-OR23-1A / CBS 708.71 / DSM 1257 / FGSC 987) apg-5 gene Proteins 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 150000001923 cyclic compounds Chemical class 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 150000004885 piperazines Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
Description
(54) СПОСОБ ПОЛУЧЕНИЯ АНИОНИТА(54) METHOD OF OBTAINING ANIONITE
Уделмшй объем, МП/г10,4Specified volume, MP / g 10.4
Мехавичеосм прочность по ГОСТ 13504-68,%99,8Mekhavicheosm strength according to GOST 13504-68,% 99.8
Перманган лв ок сл емость,Permangan lv ok slama,
мг Oj/r1,2mg Oj / r1,2
Кржлюст осветлевв еомшош 7,45Krzhlust lightened eomshosh 7.45
Выход веомзщшй после пхорбаки, % 90,8Yield after phorbaki,% 90.8
Количество орпшических а{шмвсей в фалыр те вослв ароаускшш воды 1ф«20°С, мл/гСледыThe number of orpschic a {shmvsey in the falyr of the ascent of aroauscshsh water 1f "20 ° C, ml / g
Примеров реактор, осабжеивый мешалк(Л н термометром, загруж апг 5 г крахм ла, 130 г дисшллнрованиой воды, 43 г аолиэтмленпсшиамиш , содержащего 75 % циклических соединений 1Шперазш , и перемешивают в течение 15 мин. Затем смесь шареваюу до 40-50 С и добавл ют по (сшш м 92,5 г зшилоргндршв. Тешкратуру при :JTOM поддерж{аают в пределах от 55 до 65° С. По окоичанйв ар кшаылшш эпихлоргидрина темгг ратуру реакционной массы повшомот до 85°f и выдерживают арш этой теАОЮратуре до в зкости реакционной юссы 450 - 475 свз. Обрвэовюшийс гель сушат при 310° С в течеш|е 24 час. Затем твердую массу дроб т, отбирают фракпю 1,6 - 0,4 мм, промьшаlOfT 4 - 5%-ным раствором едасого натра и дистиллирсванной водой до нейтралш ш реакции промывных вод. Полученньга &нио{{И1 обладает обесцвечи вамндей оюсобностью ио МРГУ 6 - 05 - 948 - 65 99,7% и имеет удальный объем 10,4 мл/г.Examples of the reactor, the obscuteful agitator (Ln thermometer, load apg 5 g starch, 130 g dissociating water, 43 g aleatmlenpschiamish containing 75% cyclic compounds 1Sperex and mix for 15 min. yachts by (ush 92.5 g zshilorgndrsvv. Teshkratura with: JTOM support {ayut in the range from 55 to 65 ° C. Jussy 450 - 475 overhead obrévus gel is dried at 310 ° C for 24 hours. Then the solid mass was crushed, taken with a fraction of 1.6–0.4 mm, washed with 4–5% solution of sodium hydroxide and distilled water to neutralize the reaction of the washing water. Received & {{I1 has discoloration with you 6 - 05 - 948 - 65 99.7% and has a specific volume of 10.4 ml / g.
П р и м е р 2, Процесс провод т как в примере 1 с использованием полиэтиле1шолиамнна с 31 % соединений пиперазина. Затем до стадии отверждени гел в трансформаторное масло ввод т жидкуюExample 2: The process is carried out as in Example 1 using polyethylamine with 31% piperazine compounds. Then, prior to the stage of curing the gel, liquid is introduced into the transformer oil.
массу с в зксютью 450-500 спз, температуру повышают до 75° С и систему выдерживают при этой температуре 6 - 8 час. Полученный иошгг в ф(ме гранул отдел ют от масла, промьшают 0,25%-ным раствором (XI-1, обрабатывают 5%-ным раствором едкого натра и промывают дистиллирсванной водой до нейтральной реакции промывных вод. Полученный анионит обладает обесцвечивающей способностью 92,7 %, механической прочностью по ГОСТ 13504-68 99,8% и имеет удельный объемmass of 450-500 spz, the temperature is raised to 75 ° С and the system is kept at this temperature for 6-8 hours. The resulting ice in f (the granules are separated from the oil, rinsed with a 0.25% solution (XI-1, treated with 5% sodium hydroxide solution and washed with distilled water until the wash water is neutral. The anion exchanger has a bleaching ability of 92, 7%, mechanical strength according to GOST 13504-68 is 99.8% and has a specific volume
5,3 мг/л.5.3 mg / l.
Claims (3)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU2040099A SU511328A1 (en) | 1974-07-02 | 1974-07-02 | The method of obtaining anion exchange resin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU2040099A SU511328A1 (en) | 1974-07-02 | 1974-07-02 | The method of obtaining anion exchange resin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU511328A1 true SU511328A1 (en) | 1976-04-25 |
Family
ID=20589715
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU2040099A SU511328A1 (en) | 1974-07-02 | 1974-07-02 | The method of obtaining anion exchange resin |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU511328A1 (en) |
-
1974
- 1974-07-02 SU SU2040099A patent/SU511328A1/en active
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