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RU96109107A - METHOD FOR PRODUCING FLORORATED CARBON AND DEVICE FOR ITS IMPLEMENTATION - Google Patents

METHOD FOR PRODUCING FLORORATED CARBON AND DEVICE FOR ITS IMPLEMENTATION

Info

Publication number
RU96109107A
RU96109107A RU96109107/25A RU96109107A RU96109107A RU 96109107 A RU96109107 A RU 96109107A RU 96109107/25 A RU96109107/25 A RU 96109107/25A RU 96109107 A RU96109107 A RU 96109107A RU 96109107 A RU96109107 A RU 96109107A
Authority
RU
Russia
Prior art keywords
reactor
gas
carbon material
fluorine
carbon
Prior art date
Application number
RU96109107/25A
Other languages
Russian (ru)
Other versions
RU2119448C1 (en
Inventor
Н.С. Аккузин
Л.И. Варфоломеев
Г.Г. Виноградов
Г.В. Зеленков
В.Р. Катьянова
Е.В. Кузнецов
А.И. Струшляк
Е.Д. Черниговский
С.К. Шуруев
В.М. Юрочкин
Original Assignee
Ангарский электролизный химический комбинат
Filing date
Publication date
Application filed by Ангарский электролизный химический комбинат filed Critical Ангарский электролизный химический комбинат
Priority to RU96109107/25A priority Critical patent/RU2119448C1/en
Priority claimed from RU96109107/25A external-priority patent/RU2119448C1/en
Publication of RU96109107A publication Critical patent/RU96109107A/en
Application granted granted Critical
Publication of RU2119448C1 publication Critical patent/RU2119448C1/en

Links

Claims (6)

1. Способ получения фторированного углерода, заключающийся в обработке углеродного материала фтором и фтористым водородом, отличающийся тем, что в качестве реакционного газа используют анодный газ фторного электролизера, получающийся при электролизе расплава кислых фторидов калия.1. The method of producing fluorinated carbon, which consists in treating the carbon material with fluorine and hydrogen fluoride, characterized in that the anode gas of a fluorine electrolyzer obtained by electrolysis of a molten acid potassium fluoride is used as a reaction gas. 2. Способ по п.1, отличающийся тем, что процесс фторирования углеродного материала контролируют по содержанию фтора и летучих фторуглеродов в газах на входе и выходе из реакционной зоны. 2. The method according to claim 1, characterized in that the process of fluorination of the carbon material is controlled by the content of fluorine and volatile fluorocarbons in the gases at the inlet and outlet of the reaction zone. 3. Способ по пп.1 и 2, отличающийся тем, что обработку углеродного материала ведут смесью анодного газа и азота, содержащей 12 - 21 об.% фтора, при температуре 320 - 500oC.3. The method according to claims 1 and 2, characterized in that the carbon material is treated with a mixture of anode gas and nitrogen containing 12 to 21 vol.% Fluorine, at a temperature of 320 - 500 o C. 4. Способ по пп.1 - 3, отличающийся тем, что в качестве исходного углеродного материала используют порошкообразный углерод любой структуры - аморфный или кристаллический. 4. The method according to claims 1 to 3, characterized in that as the starting carbon material, powdered carbon of any structure is used - amorphous or crystalline. 5. Устройство для получения фторированного углерода, включающее реактор, подогреватель реактора, смеситель фтора и инертного газа, газопроницаемую оснастку для углеродного материала, узел ввода газа в реактор и патрубок вывода газа из реактора, отличающееся тем, что соотношение объема (м3) реактора к геометрической поверхности оснастки (м2) для углеродного материала выполняют равным 0,3 - 0,4.5. A device for producing fluorinated carbon, comprising a reactor, a reactor heater, a fluorine and inert gas mixer, a gas-permeable tooling for carbon material, a gas inlet to the reactor and a gas outlet from the reactor, characterized in that the ratio of the volume (m 3 ) of the reactor to the geometric surface of the snap (m 2 ) for the carbon material is equal to 0.3 - 0.4. 6. Устройство по п.5, отличающееся тем, что узел ввода газа в реактор снабжен термокамерой и распределительной гребенкой, расположенной внутри реактора. 6. The device according to claim 5, characterized in that the node for introducing gas into the reactor is equipped with a heat chamber and a distribution comb located inside the reactor.
RU96109107/25A 1996-04-30 1996-04-30 Method and apparatus for producing fluorinated carbon RU2119448C1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU96109107/25A RU2119448C1 (en) 1996-04-30 1996-04-30 Method and apparatus for producing fluorinated carbon

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU96109107/25A RU2119448C1 (en) 1996-04-30 1996-04-30 Method and apparatus for producing fluorinated carbon

Publications (2)

Publication Number Publication Date
RU96109107A true RU96109107A (en) 1998-07-27
RU2119448C1 RU2119448C1 (en) 1998-09-27

Family

ID=20180279

Family Applications (1)

Application Number Title Priority Date Filing Date
RU96109107/25A RU2119448C1 (en) 1996-04-30 1996-04-30 Method and apparatus for producing fluorinated carbon

Country Status (1)

Country Link
RU (1) RU2119448C1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2170701C2 (en) * 1999-10-18 2001-07-20 ГУП "Ангарский электролизный химический комбинат" Method of preparing fluorinated caron
RU2211210C1 (en) * 2002-04-22 2003-08-27 ФГУП "Ангарский электролизный химический комбинат" Method for preparing tetrafluoromethane and device for its realization
RU2241664C1 (en) * 2003-07-16 2004-12-10 Открытое акционерное общество "Кирово-Чепецкий химический комбинат им. Б.П. Константинова" Fluorinated carbon production process
RU2350554C1 (en) * 2007-05-21 2009-03-27 Федеральное государственное унитарное предприятие "Научно-исследователький и проектно-технологический институт электроугольных изделий Method of fluorinated carbon-base material production and related device

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6041603B2 (en) * 1981-09-02 1985-09-18 セントラル硝子株式会社 Manufacturing method and equipment for graphite fluoride
JPS6041604B2 (en) * 1981-12-17 1985-09-18 セントラル硝子株式会社 Manufacturing method of graphite fluoride

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