GB1393929A - Production of di-4-chlorophenyl sulphone - Google Patents
Production of di-4-chlorophenyl sulphoneInfo
- Publication number
- GB1393929A GB1393929A GB4754772A GB4754772A GB1393929A GB 1393929 A GB1393929 A GB 1393929A GB 4754772 A GB4754772 A GB 4754772A GB 4754772 A GB4754772 A GB 4754772A GB 1393929 A GB1393929 A GB 1393929A
- Authority
- GB
- United Kingdom
- Prior art keywords
- chlorobenzene
- vapour
- reaction mixture
- production
- sulphonic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C317/00—Sulfones; Sulfoxides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1393929 Di-4-chlorophenyl sulphone IMPERIAL CHEMICAL INDUSTRIES Ltd 3 Jan 1974 [16 Oct 1972] 47547/72 Heading C2C Di-4-chlorophenylsulphone is prepared by (a) maintaining a reaction mixture containing 4-chlorobenzene sulphonic acid and chlorobenzene at a temperature of 220-260‹ C. and a superatmospheric pressure between 30 and 1100 kN./m.<SP>2</SP>; (b) removing water as vapour continuously as it is formed; and (c) condensing the water vapour and accompanying chlorobenzene vapour, separating them and returning the chlorobenzene to the reaction mixture. The 4-chlorobenzene sulphonic acid may be formed in situ from chlorobenzene and a sulphonating agent, e.g. concentrated sulphuric acid.
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB4754772A GB1393929A (en) | 1972-10-16 | 1972-10-16 | Production of di-4-chlorophenyl sulphone |
| US00300871A US3855312A (en) | 1970-02-06 | 1972-10-25 | Production of di-4-chlorophenyl sulphone |
| DE2252571A DE2252571C2 (en) | 1972-10-16 | 1972-10-26 | Process for the preparation of 4,4'-dichlorodiphenyl sulfone |
| IT2942273A IT998657B (en) | 1972-10-16 | 1973-09-26 | PRODUCTION OF 4 CHLOROPHENYL SULPHONE |
| SU731965207A SU611589A3 (en) | 1972-10-16 | 1973-10-15 | Method of preparing di-4-chlorphenylsulfone |
| BE136768A BE806163A (en) | 1972-10-16 | 1973-10-16 | PRODUCTION OF DI-4-CHLOROPHENYLSULFONE |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB4754772A GB1393929A (en) | 1972-10-16 | 1972-10-16 | Production of di-4-chlorophenyl sulphone |
| DE2252571A DE2252571C2 (en) | 1972-10-16 | 1972-10-26 | Process for the preparation of 4,4'-dichlorodiphenyl sulfone |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1393929A true GB1393929A (en) | 1975-05-14 |
Family
ID=25764010
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB4754772A Expired GB1393929A (en) | 1970-02-06 | 1972-10-16 | Production of di-4-chlorophenyl sulphone |
Country Status (3)
| Country | Link |
|---|---|
| BE (1) | BE806163A (en) |
| DE (1) | DE2252571C2 (en) |
| GB (1) | GB1393929A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8853444B2 (en) | 2010-03-05 | 2014-10-07 | Basf Se | Processes for preparing 4-chlorobenzenesulfonic acid and 4,4′-dichlorodiphenyl sulfone |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1572916A (en) * | 1976-02-11 | 1980-08-06 | Union Carbide Corp | Process for production of 4,4'-dichlorodiphenyl sulphone |
| US4778932A (en) * | 1986-07-16 | 1988-10-18 | New Japan Chemical Co., Ltd. | Process for preparing diarylsulfones |
| DE3835562A1 (en) * | 1988-10-19 | 1990-05-03 | Basf Ag | METHOD FOR PRODUCING BIS (4-CHLORPHENYL) SULPHONE |
| DE3902894A1 (en) * | 1989-02-01 | 1990-08-02 | Basf Ag | METHOD FOR PRODUCING BIS (4-CHLORPHENYL) SULPHONE |
| GB0921069D0 (en) | 2009-12-01 | 2010-01-13 | Bandodkar Hemant R | Process for the production of a sulfone polymer |
| WO2011107465A1 (en) | 2010-03-05 | 2011-09-09 | Basf Se | Method for producing 5-chlorobenzene sulphonic acid and 4,4'-dichlorodiphenylsulphone |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2593001A (en) * | 1950-01-31 | 1952-04-15 | Stauffer Chemical Co | Process for manufacture of a diphenyl sulfone |
| DE1087592B (en) * | 1958-07-05 | 1960-08-25 | Roussel Uclaf | Process for the preparation of 4,4'-dichlorodiphenyl sulfone |
| US3309409A (en) * | 1964-04-10 | 1967-03-14 | Stauffer Chemical Co | Purification of acidic chlorophenylsulfones |
| US3334146A (en) * | 1964-08-19 | 1967-08-01 | Stauffer Chemical Co | Method for the purification of bis(4-chlorophenyl) sulfone |
| US3415887A (en) * | 1966-06-10 | 1968-12-10 | Union Carbide Corp | Process for the preparation of 4,4'-dichlorodiphenyl sulfone |
-
1972
- 1972-10-16 GB GB4754772A patent/GB1393929A/en not_active Expired
- 1972-10-26 DE DE2252571A patent/DE2252571C2/en not_active Expired
-
1973
- 1973-10-16 BE BE136768A patent/BE806163A/en not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8853444B2 (en) | 2010-03-05 | 2014-10-07 | Basf Se | Processes for preparing 4-chlorobenzenesulfonic acid and 4,4′-dichlorodiphenyl sulfone |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2252571A1 (en) | 1974-05-09 |
| BE806163A (en) | 1974-04-16 |
| DE2252571C2 (en) | 1988-12-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |