FI20105036A0 - Process for preparing a carbamate cellulose solution - Google Patents
Process for preparing a carbamate cellulose solutionInfo
- Publication number
- FI20105036A0 FI20105036A0 FI20105036A FI20105036A FI20105036A0 FI 20105036 A0 FI20105036 A0 FI 20105036A0 FI 20105036 A FI20105036 A FI 20105036A FI 20105036 A FI20105036 A FI 20105036A FI 20105036 A0 FI20105036 A0 FI 20105036A0
- Authority
- FI
- Finland
- Prior art keywords
- solution
- cellulose carbamate
- naoh solution
- preparing
- dissolved
- Prior art date
Links
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 title abstract 4
- 229920002678 cellulose Polymers 0.000 title abstract 4
- 239000001913 cellulose Substances 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 9
- 239000000243 solution Substances 0.000 abstract 6
- 239000003513 alkali Substances 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L1/00—Compositions of cellulose, modified cellulose or cellulose derivatives
- C08L1/08—Cellulose derivatives
- C08L1/10—Esters of organic acids, i.e. acylates
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
In a method, cellulose carbamate is dissolved in an alkaline aqueous solution in different steps with solutions having different concentrations. The dissolving is carried out in three steps: 1) prewetting of the cellulose carbamate is performed with a dilute aqueous NaOH solution, under simultaneous cooling; 2) more concentrated NaOH solution, cooled to a temperature lower than 0°C, is added, under simultaneous stirring, in such a way that the cellulose carbamate is dissolved and the alkali concentration of the solution exceeds 9%, and subsequently, 3) a dilute NaOH solution is added so that the final alkali concentration of the solution drops to a value below 9%.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI20105036A FI20105036A0 (en) | 2010-01-18 | 2010-01-18 | Process for preparing a carbamate cellulose solution |
| PCT/FI2011/050036 WO2011086241A1 (en) | 2010-01-18 | 2011-01-18 | Method for preparing solution of cellulose carbamate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI20105036A FI20105036A0 (en) | 2010-01-18 | 2010-01-18 | Process for preparing a carbamate cellulose solution |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| FI20105036A0 true FI20105036A0 (en) | 2010-01-18 |
Family
ID=41620874
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI20105036A FI20105036A0 (en) | 2010-01-18 | 2010-01-18 | Process for preparing a carbamate cellulose solution |
Country Status (2)
| Country | Link |
|---|---|
| FI (1) | FI20105036A0 (en) |
| WO (1) | WO2011086241A1 (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI20206386A1 (en) * | 2020-12-31 | 2022-07-01 | Infinited Fiber Company Oy | Continuous Dissolution of a Cellulose Derivative |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19757958A1 (en) * | 1997-12-24 | 1999-07-01 | Lurgi Zimmer Ag | Two-stage production of cellulose carbamate solution for the production of spinning solutions used in the manufacture of regenerated cellulose fibers. |
| FI118689B (en) * | 2005-11-23 | 2008-02-15 | Valtion Teknillinen | Process for manufacturing cellulose carbamate solution |
-
2010
- 2010-01-18 FI FI20105036A patent/FI20105036A0/en not_active Application Discontinuation
-
2011
- 2011-01-18 WO PCT/FI2011/050036 patent/WO2011086241A1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| WO2011086241A1 (en) | 2011-07-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD | Application lapsed |