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ES2196464T3 - Procedimiento para la recuperacion de acido sulfurico de productos secundarios que contienen sulfatos de un proceso para la preparacion de acido 2-hidroxi-4-metiltiobutirico (mha). - Google Patents

Procedimiento para la recuperacion de acido sulfurico de productos secundarios que contienen sulfatos de un proceso para la preparacion de acido 2-hidroxi-4-metiltiobutirico (mha).

Info

Publication number
ES2196464T3
ES2196464T3 ES98122921T ES98122921T ES2196464T3 ES 2196464 T3 ES2196464 T3 ES 2196464T3 ES 98122921 T ES98122921 T ES 98122921T ES 98122921 T ES98122921 T ES 98122921T ES 2196464 T3 ES2196464 T3 ES 2196464T3
Authority
ES
Spain
Prior art keywords
sulfuric acid
mha
recovery
hydrolysis
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES98122921T
Other languages
English (en)
Inventor
Hans-Albrecht Dr Hasseberg
Hans-Joachim Dr Hasselbach
Klaus Dr Huthmacher
Volker Hafner
Harald Heinzel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik Operations GmbH
Original Assignee
Degussa GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Degussa GmbH filed Critical Degussa GmbH
Application granted granted Critical
Publication of ES2196464T3 publication Critical patent/ES2196464T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/48Sulfur dioxide; Sulfurous acid
    • C01B17/50Preparation of sulfur dioxide
    • C01B17/58Recovery of sulfur dioxide from acid tar or the like or from any waste sulfuric acid
    • C01B17/585Recovery of sulfur dioxide from acid tar or the like or from any waste sulfuric acid from ammonium sulfate containing sulfuric acid solutions
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • C01B17/745Preparation from sulfates
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/26Separation; Purification; Stabilisation; Use of additives
    • C07C319/28Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treating Waste Gases (AREA)

Abstract

LA INVENCION TRATA DE UN PROCEDIMIENTO PARA LA RECUPERACION DE ACIDO SULFURICO A PARTIR DE PRODUCTOS QUE CONTIENEN AZUFRE, QUE SE FORMAN EN PROCESOS PARA LA OBTENCION DEL ACIDO 2 HIDROXI - 4 - METILTIOBUTILICO (MHA), TENIENDO EL ACIDO SULFURICO UNA CALIDAD, QUE SE PUEDE VOLVER A UTILIZAR DIRECTAMENTE EN TALES COMPUESTOS. PARA ESTE OBJETO SE LLEVA GAS DE COMBUSTION QUE CONTIENE SO 2 A TRAVES DE UNA DISOLUCION DE H 2 O SUB,2 ACIDA DE AZUFRE, EN LA CUAL EL SO 2 SE OXIDA PARA DAR ACIDO SULFURICO.
ES98122921T 1997-12-09 1998-12-02 Procedimiento para la recuperacion de acido sulfurico de productos secundarios que contienen sulfatos de un proceso para la preparacion de acido 2-hidroxi-4-metiltiobutirico (mha). Expired - Lifetime ES2196464T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19754562A DE19754562A1 (de) 1997-12-09 1997-12-09 Verfahren zur Rückgewinnung von Schwefelsäure aus schwefelhaltigen Nebenprodukten eines Prozesses zur Herstellung von 2-Hydroxy-4-methylthiobuttersäure (MHA)

Publications (1)

Publication Number Publication Date
ES2196464T3 true ES2196464T3 (es) 2003-12-16

Family

ID=7851227

Family Applications (1)

Application Number Title Priority Date Filing Date
ES98122921T Expired - Lifetime ES2196464T3 (es) 1997-12-09 1998-12-02 Procedimiento para la recuperacion de acido sulfurico de productos secundarios que contienen sulfatos de un proceso para la preparacion de acido 2-hidroxi-4-metiltiobutirico (mha).

Country Status (16)

Country Link
US (1) US6146612A (es)
EP (1) EP0922670B1 (es)
JP (1) JP4511647B2 (es)
KR (1) KR19990063023A (es)
CN (1) CN1119280C (es)
AT (1) ATE236078T1 (es)
AU (1) AU735555B2 (es)
BR (1) BR9805253A (es)
CA (1) CA2255483A1 (es)
DE (2) DE19754562A1 (es)
ES (1) ES2196464T3 (es)
ID (1) ID21414A (es)
PL (1) PL330168A1 (es)
SG (1) SG73595A1 (es)
TR (1) TR199802563A2 (es)
TW (1) TW522139B (es)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6017563A (en) 1997-07-25 2000-01-25 Novus International, Inc. Process for optimizing milk production
AU6525700A (en) 1999-08-05 2001-03-05 Novus International Inc Reductive combustion of ammonium salts of sulfuric acid
DE19963509A1 (de) * 1999-12-28 2001-07-05 Merck Patent Gmbh Verfahren zur Herstellung hochreiner Schwefelsäure
CN114053839B (zh) * 2020-08-05 2023-06-23 中冶长天国际工程有限责任公司 一种含氰srg气体清洁治理及热风炉尾气净化的方法和系统
CN117862142A (zh) * 2024-03-11 2024-04-12 招远市招金金合科技有限公司 一种高铁硫酸送化渣回收精炼设备

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2106950A5 (es) * 1970-09-30 1972-05-05 Air Liquide
US3760061A (en) * 1971-03-02 1973-09-18 Du Pont High-strength acid containing h2o2 to scrub so2
BE794918A (fr) * 1972-02-04 1973-08-02 Oxysynthese Procede d'epuration de fumees industrielles, de produit de combustion et d'efflents gazeux avant rejet a l'atmosphere
US3917798A (en) * 1973-09-24 1975-11-04 Du Pont SO{HD 2{B abatement
JPS59108995A (ja) * 1982-12-14 1984-06-23 日立造船株式会社 放射性廃棄物から硫酸を製造する方法
ES2005784A6 (es) * 1988-02-22 1989-03-16 Desarrollo Tecnico Ind S A Soc Un procedimiento para preparar soluciones acuosas de acido 2-hidroxi-4-metil-tiobutirico.
DE4036899C2 (de) * 1990-11-20 2001-10-25 Degussa Verfahren zur Entschwefelung von SO¶2¶ enthaltenden feuchten Abgasen und Vorrichtung zur Durchführung des Verfahrens
US5498790A (en) * 1993-06-09 1996-03-12 Novus International, Inc. Regeneration of sulfuric acid from sulfate by-products of 2-hydroxy-4-(methylthio)butyric acid manufacture
BR9508383A (pt) * 1994-07-11 1997-12-23 Degussa Processo para a obtenção de ácido 2-hidróxi-4-metiltiobutírico (mha) mha e seu emprego
DE4428608C1 (de) * 1994-08-12 1996-02-29 Degussa Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA)
US5595713A (en) * 1994-09-08 1997-01-21 The Babcock & Wilcox Company Hydrogen peroxide for flue gas desulfurization
DE19525054C2 (de) * 1995-07-10 1999-02-25 Freudenberg Carl Fa Verfahren zur Herstellung eines Radialwellendichtrings
JPH09315806A (ja) * 1996-05-28 1997-12-09 Mitsubishi Gas Chem Co Inc 硫酸および過酸化水素を含む廃液からの硫酸の回収方法

Also Published As

Publication number Publication date
CA2255483A1 (en) 1999-06-09
TR199802563A2 (xx) 1999-06-21
CN1119280C (zh) 2003-08-27
SG73595A1 (en) 2000-06-20
JP4511647B2 (ja) 2010-07-28
AU9698798A (en) 1999-07-01
AU735555B2 (en) 2001-07-12
EP0922670B1 (de) 2003-04-02
EP0922670A1 (de) 1999-06-16
BR9805253A (pt) 2000-02-01
ATE236078T1 (de) 2003-04-15
DE19754562A1 (de) 1999-06-10
ID21414A (id) 1999-06-10
JPH11246207A (ja) 1999-09-14
CN1223230A (zh) 1999-07-21
DE59807725D1 (de) 2003-05-08
TW522139B (en) 2003-03-01
KR19990063023A (ko) 1999-07-26
US6146612A (en) 2000-11-14
PL330168A1 (en) 1999-06-21

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