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ES2033524T3 - Aparato y metodo para producir polvos ceramicos finos y uniformes. - Google Patents

Aparato y metodo para producir polvos ceramicos finos y uniformes.

Info

Publication number
ES2033524T3
ES2033524T3 ES198989301109T ES89301109T ES2033524T3 ES 2033524 T3 ES2033524 T3 ES 2033524T3 ES 198989301109 T ES198989301109 T ES 198989301109T ES 89301109 T ES89301109 T ES 89301109T ES 2033524 T3 ES2033524 T3 ES 2033524T3
Authority
ES
Spain
Prior art keywords
chamber
reactor chamber
refrigeration
cold
transport member
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES198989301109T
Other languages
English (en)
Inventor
Alan W. Weimer
William G. Moore
Raymond P. Roach
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Chemical Co
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Application granted granted Critical
Publication of ES2033524T3 publication Critical patent/ES2033524T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0095—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes in which two different types of particles react with each other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/12—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by gravity in a downward flow
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C01B21/064—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with boron
    • C01B21/0645—Preparation by carboreductive nitridation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/90—Carbides
    • C01B32/907—Oxycarbides; Sulfocarbides; Mixture of carbides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/90—Carbides
    • C01B32/914—Carbides of single elements
    • C01B32/991—Boron carbide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/02—Boron; Borides
    • C01B35/04—Metal borides
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/56—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
    • C04B35/563—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on boron carbide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00477—Controlling the temperature by thermal insulation means
    • B01J2208/00495—Controlling the temperature by thermal insulation means using insulating materials or refractories
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/85—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by XPS, EDX or EDAX data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/90—Other properties not specified above

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Ceramic Engineering (AREA)
  • Nanotechnology (AREA)
  • Manufacturing & Machinery (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Composite Materials (AREA)
  • Physics & Mathematics (AREA)
  • Structural Engineering (AREA)
  • Toxicology (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Ceramic Products (AREA)
  • Perforating, Stamping-Out Or Severing By Means Other Than Cutting (AREA)
  • Polishing Bodies And Polishing Tools (AREA)
  • Disintegrating Or Milling (AREA)
  • Saccharide Compounds (AREA)

Abstract

SE PREPARA POLVO CERAMICO FINO, UNIFORME, UTILIZANDO UN APARATO QUE CONTIENE UN MIEMBRO DE TRANSPORTE DE REACTIVO FRIO (6); UNA CAMARA REACTOR (16); UN MEDO DE CALENTAMIENTO (4); Y UNA CAMARA DE REFRIGERACION (42); EL MIEMBRO DE TRANSPORTE DE REACTIVO COMUNICA CON LA CAMARA REACTOR, E INCLUYE UN ESPACIO DE FLUJO DE GAS A LO LARGO DEL PERIMETRO DEL MIEMBRO DE TRANSPORTE, TAMBIEN EN COMUNICACION CON LA CAMARA REACTOR. ESTA DEFINE UNA ZONA DE REACCION QUE INCLUYE UN MEDIO DE CALENTAMIENTO. LA CAMARA FRIA DEFINE UNA ZONA DE REFRIGERACION QUE COMUNICA CON LA CAMARA REACTOR. PREFERIBLEMENTE, EL DIAMETRO DE LA ZONA DE REFRIGERACION ES MAYOR QUE EL DIAMETRO DE LA ENTRADA DE REFRIGERACION. LAS TEMPERATURAS DEL MIEMBRO DE TRANSPORTE DE REACTIVO, LA CAMARA REACTOR, Y LA CAMARA FRIA SE CONTROLAN INDEPENDIENTEMENTE. EL APARATO ES PARTICULARMENTE ADECUADO PARA PRODUCIR POLVOS CERAMICOS QUE CONTIENEN BORO POR REDUCCION CARBOTERMICA RAPIDA DE OXIDO BORICO O DE SU HIDRATO Y UNA FUENTE DE CARBON.
ES198989301109T 1988-02-05 1989-02-03 Aparato y metodo para producir polvos ceramicos finos y uniformes. Expired - Lifetime ES2033524T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/152,613 US5110565A (en) 1988-02-05 1988-02-05 Apparatus for producing uniform, fine ceramic powder

Publications (1)

Publication Number Publication Date
ES2033524T3 true ES2033524T3 (es) 1993-03-16

Family

ID=22543648

Family Applications (1)

Application Number Title Priority Date Filing Date
ES198989301109T Expired - Lifetime ES2033524T3 (es) 1988-02-05 1989-02-03 Aparato y metodo para producir polvos ceramicos finos y uniformes.

Country Status (14)

Country Link
US (1) US5110565A (es)
EP (1) EP0327401B1 (es)
JP (1) JP2874925B2 (es)
KR (1) KR900700184A (es)
CN (1) CN1036003A (es)
AT (1) ATE73007T1 (es)
BR (1) BR8905298A (es)
CA (1) CA1334331C (es)
DE (1) DE68900886D1 (es)
ES (1) ES2033524T3 (es)
FI (1) FI894697A7 (es)
IL (1) IL89163A (es)
NO (1) NO174694C (es)
WO (1) WO1989007011A1 (es)

Families Citing this family (31)

* Cited by examiner, † Cited by third party
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US4804525A (en) * 1986-04-14 1989-02-14 The Dow Chemical Company Producing boron carbide
US5126121A (en) * 1991-05-03 1992-06-30 The Dow Chemical Company Process for preparing aluminum nitride powder via controlled combustion nitridation
US5219804A (en) * 1992-01-10 1993-06-15 The Dow Chemical Company Process for preparing ultrafine aluminum nitride powder
US7576296B2 (en) * 1995-03-14 2009-08-18 Battelle Energy Alliance, Llc Thermal synthesis apparatus
AT404912B (de) * 1996-11-04 1999-03-25 Plansee Ag Verfahren zur herstellung von pulver-pressansätzen für feinkörniges hartmetall
US6214078B1 (en) 1997-11-25 2001-04-10 Ferro Corporation High temperature ceramic filter
ES2188298B1 (es) * 1999-06-15 2004-08-16 Fundacion Inasmet Procedimiento continuo de fabricacion de materiales en polvo por combustion y reactor para la puesta en practica del mismo.
WO2001046067A1 (en) * 1999-12-21 2001-06-28 Bechtel Bwxt Idaho, Llc Hydrogen and elemental carbon production from natural gas and other hydrocarbons
CN1419482A (zh) * 2000-02-22 2003-05-21 Omg美国公司 含金属的化合物快速转化形成金属或金属氧化物
CN1289392C (zh) * 2001-07-30 2006-12-13 三菱麻铁里亚尔株式会社 微粒碳化钨粉末的制造方法及粉末
US7303593B1 (en) 2002-09-16 2007-12-04 Sandia Corporation Method to blend separator powders
GB2445218B (en) * 2006-09-21 2011-05-25 Smith International Atomic layer deposition nanocoating on cutting tool powder materials
WO2008102357A2 (en) * 2007-02-22 2008-08-28 Boron Compounds Ltd. Method for the preparation of ceramic materials
JP5168690B2 (ja) * 2007-03-23 2013-03-21 独立行政法人産業技術総合研究所 ホウ素ナノ粒子又はホウ素含有ナノ粒子及びその製造方法
US7919040B2 (en) * 2007-08-08 2011-04-05 Saint-Gobain Ceramics & Plastics, Inc. Method of preparing pressureless sintered, highly dense boron carbide materials
KR101121803B1 (ko) * 2008-01-17 2012-03-20 경희대학교 산학협력단 정밀온도 제어가 가능한 연속식 냉각 결정화 반응장치 및이를 포함하는 결정화 분리공정 시스템
US20100055017A1 (en) * 2008-09-03 2010-03-04 Ppg Industries Ohio, Inc. Methods for the production of ultrafine metal carbide particles and hydrogen
JP2013500227A (ja) * 2009-07-24 2013-01-07 サン−ゴバン セラミックス アンド プラスティクス，インコーポレイティド 焼結炭化ホウ素の形成方法
JP5866690B2 (ja) * 2009-09-04 2016-02-17 国立研究開発法人産業技術総合研究所 球状ナノ粒子の製造方法及び同製造方法によって得られた球状ナノ粒子
EP2493813B1 (en) * 2009-10-30 2019-12-04 Alcoa USA Corp. Methods of making titanium diboride powders
JP5495748B2 (ja) * 2009-12-10 2014-05-21 株式会社トクヤマ 窒化アルミニウム粉末
DE102011050171A1 (de) * 2011-05-06 2012-11-08 Heinrich-Heine-Universität Düsseldorf Verfahren und Anordnung zum Detektieren eines ersten Gases in einem wenigstens ein weiteres Gas umfassenden Gasgemisch
EP3475246A4 (en) * 2016-06-23 2020-01-08 Alcoa USA Corp. SYSTEMS AND METHODS FOR MANUFACTURING CERAMIC POWDERS AND CERAMIC PRODUCTS
EP3490929A1 (en) * 2016-07-26 2019-06-05 Arconic Inc. Methods for making boron nitride ceramic powder
CN106631032B (zh) * 2016-10-12 2019-10-15 淄博晶亿陶瓷科技有限公司 一种高纯二硼化钛粉体及其制备方法
US11193191B2 (en) * 2017-11-28 2021-12-07 University Of Maryland, College Park Thermal shock synthesis of multielement nanoparticles
CN108445146B (zh) * 2018-05-28 2024-02-02 湖南三德科技股份有限公司 一种用于元素分析仪的均流机构
WO2020046229A2 (en) * 2018-08-27 2020-03-05 Ak-Kim Kimya Sanayi Ve Ticaret Anonim Sirketi Production of boron carbide, metal carbide and/or metal boride at high temperature and in continuous production line
CN110937605B (zh) * 2019-12-18 2023-03-28 赛福纳米科技(徐州)有限公司 碳化硼纯化方法
CN114409412A (zh) * 2020-10-28 2022-04-29 中国科学院理化技术研究所 一种SiB6的化学炉合成方法
CN114543523B (zh) * 2022-01-19 2023-10-24 福建华清电子材料科技有限公司 精准控制氮气供应的氮化铝粉末制备石墨炉

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CA665291A (en) * 1963-06-18 Union Carbide Corporation Ultrafine titanium boride
US3353885A (en) * 1966-02-01 1967-11-21 Howard C Hanson Expansible multi-purpose cabinet
US3989782A (en) * 1973-12-29 1976-11-02 Joseph Lucas Limited Method of forming a sintered ceramic product
US4266977A (en) * 1975-02-03 1981-05-12 Ppg Industries, Inc. Submicron carbon-containing titanium boride powder and method for preparing same
DE2620313C3 (de) * 1976-05-07 1981-04-09 Andrjušin, Aleksandr Iosifovič Verfahren zur Erzeugung von Karbiden und Anlage zur Durchführung des Verfahrens
US4597948A (en) * 1982-12-27 1986-07-01 Sri International Apparatus for obtaining silicon from fluosilicic acid
US4666873A (en) * 1983-10-14 1987-05-19 General Electric Company Aluminum nitride-boron nitride composite article and method of making same
US4643890A (en) * 1984-09-05 1987-02-17 J. M. Huber Corporation Perforated reactor tube for a fluid wall reactor and method of forming a fluid wall
FR2591412A1 (fr) * 1985-12-10 1987-06-12 Air Liquide Procede de fabrication de poudres et reacteur etanche a plasma micro-onde
JPH0638911B2 (ja) * 1986-03-08 1994-05-25 日本セメント株式会社 非酸化物粉末の製造方法

Also Published As

Publication number Publication date
ATE73007T1 (de) 1992-03-15
IL89163A0 (en) 1989-09-10
EP0327401A3 (en) 1990-03-07
DE68900886D1 (de) 1992-04-09
BR8905298A (pt) 1990-11-27
NO174694B (no) 1994-03-14
US5110565A (en) 1992-05-05
EP0327401B1 (en) 1992-03-04
FI894697A0 (fi) 1989-10-04
FI894697A7 (fi) 1989-10-04
CA1334331C (en) 1995-02-14
CN1036003A (zh) 1989-10-04
NO893946L (no) 1989-12-04
EP0327401A2 (en) 1989-08-09
WO1989007011A1 (en) 1989-08-10
JPH02503168A (ja) 1990-10-04
IL89163A (en) 1992-07-15
NO893946D0 (no) 1989-10-04
JP2874925B2 (ja) 1999-03-24
NO174694C (no) 1994-06-22
KR900700184A (ko) 1990-08-11

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