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EA200700843A1 - METHOD AND DEVICE FOR OBTAINING METAL BY ELECTROLYSIS OF SALT MELT - Google Patents

METHOD AND DEVICE FOR OBTAINING METAL BY ELECTROLYSIS OF SALT MELT

Info

Publication number
EA200700843A1
EA200700843A1 EA200700843A EA200700843A EA200700843A1 EA 200700843 A1 EA200700843 A1 EA 200700843A1 EA 200700843 A EA200700843 A EA 200700843A EA 200700843 A EA200700843 A EA 200700843A EA 200700843 A1 EA200700843 A1 EA 200700843A1
Authority
EA
Eurasian Patent Office
Prior art keywords
electrolysis
cathode
space
anode
molten salt
Prior art date
Application number
EA200700843A
Other languages
Russian (ru)
Other versions
EA011903B1 (en
Inventor
Масанори Ямагути
Юйти Оно
Сусуму Косемура
Еидзи Нисимура
Тадаси Огасавара
Макото Ямагути
Масахико Хори
Тору Уениси
Original Assignee
Тохо Титаниум Ко., Лтд.
Сумитомо Титаниум Корпорейшн
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Тохо Титаниум Ко., Лтд., Сумитомо Титаниум Корпорейшн filed Critical Тохо Титаниум Ко., Лтд.
Publication of EA200700843A1 publication Critical patent/EA200700843A1/en
Publication of EA011903B1 publication Critical patent/EA011903B1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/129Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds by dissociation, e.g. thermic dissociation of titanium tetraiodide, or by electrolysis or with the use of an electric arc
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25CPROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C3/00Electrolytic production, recovery or refining of metals by electrolysis of melts
    • C25C3/02Electrolytic production, recovery or refining of metals by electrolysis of melts of alkali or alkaline earth metals
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25CPROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C3/00Electrolytic production, recovery or refining of metals by electrolysis of melts
    • C25C3/26Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium
    • C25C3/28Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium of titanium
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25CPROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C7/00Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
    • C25C7/02Electrodes; Connections thereof
    • C25C7/025Electrodes; Connections thereof used in cells for the electrolysis of melts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Electrolytic Production Of Metals (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

Способ получения металла электролизом солевого расплава, осуществляемый с заполнением солевым расплавом хлорида кальция электролизной ванны, снабженной анодом и катодом, характеризующийся тем, что любой один электрод из анода и катода устанавливают так, чтобы он окружал другой электрод, катод снабжен по меньшей мере одним сообщающим отверстием, которое обеспечивает сообщение между окруженным катодом внутренним пространством и внешним пространством, и солевому расплаву дают возможность перетекать из одного пространства, внутреннего или внешнего, на снабженной анодом стороне в другое пространство через сообщающее отверстие.A method for producing metal by electrolysis of a molten salt, carried out by filling an electrolysis bath equipped with an anode and a cathode with a molten salt of calcium chloride, characterized in that any one electrode of the anode and cathode is installed so that it surrounds another electrode, the cathode is equipped with at least one communicating hole which provides communication between the cathode-enclosed internal space and the external space, and the molten salt is allowed to flow from one space, internal or external, on the anode-equipped side to the other space through the communication opening.

EA200700843A 2004-10-12 2005-10-05 Metal producing method and producing device by molten salt electrolysis EA011903B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2004297865A JP4247792B2 (en) 2004-10-12 2004-10-12 Method and apparatus for producing metal by molten salt electrolysis
PCT/JP2005/018449 WO2006040978A1 (en) 2004-10-12 2005-10-05 Metal producing method and producing device by molten salt electrolysis

Publications (2)

Publication Number Publication Date
EA200700843A1 true EA200700843A1 (en) 2007-08-31
EA011903B1 EA011903B1 (en) 2009-06-30

Family

ID=36148273

Family Applications (1)

Application Number Title Priority Date Filing Date
EA200700843A EA011903B1 (en) 2004-10-12 2005-10-05 Metal producing method and producing device by molten salt electrolysis

Country Status (9)

Country Link
US (1) US20080078679A1 (en)
EP (1) EP1811062A4 (en)
JP (1) JP4247792B2 (en)
CN (1) CN101044268A (en)
AU (1) AU2005293038A1 (en)
CA (1) CA2582035A1 (en)
EA (1) EA011903B1 (en)
NO (1) NO20072241L (en)
WO (1) WO2006040978A1 (en)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4193984B2 (en) * 2003-08-28 2008-12-10 株式会社大阪チタニウムテクノロジーズ Metal manufacturing equipment
JPWO2006115027A1 (en) * 2005-04-25 2008-12-18 東邦チタニウム株式会社 Molten salt electrolytic bath and method for producing metal using the same
JP2007063585A (en) * 2005-08-30 2007-03-15 Sumitomo Titanium Corp MOLTEN SALT ELECTROLYSIS METHOD, ELECTROLYTIC CELL, AND METHOD FOR PRODUCING Ti BY USING THE SAME
WO2008038405A1 (en) * 2006-09-28 2008-04-03 Toho Titanium Co., Ltd. Molten salt electrolyzing vessel for metal production and process for producing metal therewith
JP5226700B2 (en) 2007-01-22 2013-07-03 マテリアルズ アンド エレクトロケミカル リサーチ コーポレイション Metallic thermal reduction of in situ generated titanium chloride
EP2123798A4 (en) * 2007-02-19 2010-03-17 Toho Titanium Co Ltd Apparatus for producing metal by molten salt electrolysis, and process for producing metal using the apparatus
KR101237327B1 (en) 2007-05-11 2013-02-28 엠 히카리 앤 에너지 레보레토리 컴퍼니 리미티드 On-site integrated production plant
JP2009019250A (en) * 2007-07-13 2009-01-29 Osaka Titanium Technologies Co Ltd Method and apparatus for producing metal
CN101649472B (en) * 2008-08-15 2012-06-06 攀钢集团钢铁钒钛股份有限公司 Method for preparing metallic titanium
MD168Z (en) * 2009-06-04 2010-10-31 Институт Прикладной Физики Академии Наук Молдовы Device for electroplating of inner surfaces of the cylindrical parts of small and medium diameter
MY180279A (en) 2010-11-18 2020-11-26 Metalysis Ltd Electrolysis apparatus
NZ610339A (en) * 2010-11-18 2015-11-27 Metalysis Ltd Method and system for electrolytically reducing a solid feedstock
CN102517611B (en) * 2011-12-27 2015-08-26 宁波江丰电子材料股份有限公司 The method of fused salt electrolysis refining equipment and extracting metals thereof
JP6270446B2 (en) * 2013-12-06 2018-01-31 東邦チタニウム株式会社 Method for producing metal by molten salt electrolysis
CN103774180B (en) * 2014-01-28 2016-03-02 东北大学 A kind of apparatus and method producing metal and alloy integrating chlorination-electrolysis
CN103898553B (en) * 2014-03-25 2016-06-22 中国科学院过程工程研究所 A kind of electrodeposition and refine are synchronously performed the method producing calcium metal
KR102341029B1 (en) * 2014-06-30 2021-12-21 도호 티타늄 가부시키가이샤 Method for producing metal and method for producing refractory metal
CN104668557B (en) * 2015-02-06 2018-12-28 安徽腾拓新材料科技有限公司 A kind of calcium metal briquetting molding equipment
WO2016129009A1 (en) * 2015-02-09 2016-08-18 国立大学法人北海道大学 Method for manufacturing metallic vanadium
CN104928721B (en) * 2015-06-12 2017-09-22 中南大学 A kind of preparation of low-valence titanium chloride molten salt electrolyte and purifier
CN106835203B (en) * 2016-12-26 2019-05-31 宝纳资源控股(集团)有限公司 A kind of purification device and method of fused salt
CN107164781A (en) * 2017-06-05 2017-09-15 攀钢集团研究院有限公司 A kind of method for preparing purification ultrafine titanium powder
CN107059067A (en) * 2017-06-05 2017-08-18 攀钢集团研究院有限公司 A kind of method for preparing ultra-fine Titanium Powder
CN109881200B (en) * 2019-04-10 2021-05-11 深圳市铿东科技有限公司 Regeneration of alkaline etching solution and copper recovery method thereof
KR20250093304A (en) * 2022-09-09 2025-06-24 파닉스 테일링 인크. Systems and methods for supplying solid materials and gases to an electrolytic cell
CN116949520B (en) * 2023-08-04 2025-12-12 重庆天齐锂业有限责任公司 A lithium metal electrolytic cell and a method for preparing lithium metal.

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES257371A1 (en) * 1959-05-13 1960-11-16 Solvay Process of producing calcium by electrolysis
JPS61186489A (en) * 1985-02-13 1986-08-20 Hiroshi Ishizuka Device for electrolyzing molten chloride of alkali metal or alkaline earth metal
FR2589169B1 (en) * 1985-10-25 1990-08-31 Commissariat Energie Atomique ELECTROLYZER FOR THE EXTRACTION OF A SUBSTANCE, IN PARTICULAR FROM AN ALKALI METAL, FROM AN ELECTROLYTIC BATH
ITTO970080A1 (en) * 1997-02-04 1998-08-04 Marco Vincenzo Ginatta PROCEDURE FOR THE ELECTROLYTIC PRODUCTION OF METALS
JP2003129268A (en) * 2001-10-17 2003-05-08 Katsutoshi Ono Method for smelting metallic titanium and smelter therefor
JP3718691B2 (en) * 2002-04-18 2005-11-24 財団法人生産技術研究奨励会 Titanium production method, pure metal production method, and pure metal production apparatus

Also Published As

Publication number Publication date
JP4247792B2 (en) 2009-04-02
NO20072241L (en) 2007-04-30
EP1811062A4 (en) 2009-04-29
US20080078679A1 (en) 2008-04-03
CA2582035A1 (en) 2006-04-20
EP1811062A1 (en) 2007-07-25
WO2006040978A1 (en) 2006-04-20
AU2005293038A1 (en) 2006-04-20
JP2006111895A (en) 2006-04-27
CN101044268A (en) 2007-09-26
EA011903B1 (en) 2009-06-30

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Legal Events

Date Code Title Description
MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): AM AZ BY KZ KG MD TJ TM RU