[go: up one dir, main page]

CN1284571A - Process and apparatus of direct producing high-grade zinc oxide - Google Patents

Process and apparatus of direct producing high-grade zinc oxide Download PDF

Info

Publication number
CN1284571A
CN1284571A CN 00107928 CN00107928A CN1284571A CN 1284571 A CN1284571 A CN 1284571A CN 00107928 CN00107928 CN 00107928 CN 00107928 A CN00107928 A CN 00107928A CN 1284571 A CN1284571 A CN 1284571A
Authority
CN
China
Prior art keywords
powder
furnace
zinc oxide
pond
zinc
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 00107928
Other languages
Chinese (zh)
Other versions
CN1127577C (en
Inventor
沈奕林
何明德
熊志军
骆裕航
刘小明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LIUZHOU NON-FERROUS SMELTING Co Ltd
Original Assignee
LIUZHOU NON-FERROUS SMELTING Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by LIUZHOU NON-FERROUS SMELTING Co Ltd filed Critical LIUZHOU NON-FERROUS SMELTING Co Ltd
Priority to CN 00107928 priority Critical patent/CN1127577C/en
Publication of CN1284571A publication Critical patent/CN1284571A/en
Application granted granted Critical
Publication of CN1127577C publication Critical patent/CN1127577C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Manufacture And Refinement Of Metals (AREA)

Abstract

The apparatus consists of furnace stack, oxidizing door, oxidizing chamber, heat maintaining smoke channel, gate, heat maintaining settling chamber, heat maintaining powder pond, afterheat boilet, cooler aluminum pipe, cloth bag chamber, ash eliminating door, cleaning doors, powder discharging door, drawing fan and motor. The furnace stack is one double hearth structure and the two hearths are used in smelting alternately. When pellets are mselted in the furnace, they are covered with one layer of sulfur-fixing agent. Product powder is collected in the heat maintaining powder pond at 770-1100 deg.C.

Description

Produce the method and apparatus of high-grade zinc oxide with direct method
The invention belongs to field of metallurgy, relate to pyrogenic process and produce zinc oxide, particularly, the present invention relates to produce the method and apparatus of high-grade zinc oxide with direct method.
Pyrogenic process is the method for the present production zinc oxide that generally adopts in the world, and this method is the zinc raw material to be reduced into zinc fume combine with oxygen again, makes zinc oxide.This method is broadly divided into two kinds of indirect method and direct methods.Indirect method is an evaporated metal zinc in a rectifying jar, and with zinc fume and airborne oxygen reaction generation zinc oxide, this method has constant product quality, zinc oxide purity height, the advantage that impurity is few, the first grade zinc oxide content reaches more than 99.7%, but because this method is a raw material with expensive metal zinc ingot, the production cost height.Direct method is produced the zinc oxide outstanding feature and is to use zinc baking sand or other material containing zinc to finish the redox process in same equipment, direct output zinc oxide, avoided using metallic zinc to reduce production cost as raw material, but because impurity is many in the raw material, the volatile impurity of part enters into finished product with the zinc fume oxidation, influence the purity of product, American process zinc oxide first grade zinc oxide content can only reach 99.5%, can not produce 99.7% grade zinc oxide, value of the product is lower than indirect method, and the ratio of first-grade products can only reach 60-70%.
At present in the world particularly China's American process zinc oxide generally adopt dimension to cut the rel method to produce, its technical process is as follows:
1, roasting: zinc ore concentrate high-temperature roasting desulfurization is obtained zinc baking sand;
2, briquetting: with zinc baking sand with go back raw coal under the effect of tackiness agent, be pressed into pellet;
3, redox: smelting palletizing ore deposit in Vickers stove (claiming Furnace for obtaining white zinc again), the zinc fume that is reduced causes in oxidizing chamber and the secondary air oxygen reaction by blower fan and generates zinc oxide, by the cooling system of back segment with receive powder system and captured, obtains zinc oxide.
Common Furnace for obtaining white zinc system is shown in figure one, by body of heater (1), oxidation door (2), oxidizing chamber (3), water-cooled cigarette lane (4), gate (5), settling pocket (6), cooling water tank (7), surface cooler (8,9), aluminum pipe (10), cloth bag chamber (11), soot door (12), cleaning door (13,14,15), powder exit (16), receipts powder pond (17), vacuum fan (18), motor (19) are formed.In addition, for improving UTILIZATION OF VESIDUAL HEAT IN, existing also have some production systems to adopt waste heat boiler to replace settling pocket (6) and cooling water tank (7).This system is periodical operation, and each operational cycle comprises into ground coal, the nodulizing of scoring, takes out operations such as waste gas, smelting, deslagging, and the time is 2.5-3 hour, wherein be 1.5-2 hour tap to tap time, other operating time is 1 hour, and can only smelt the 8-9 stove every day, with 12M 2The zinc white furnace gauge, monthly output is about 200 tons.Product zinc oxide is mainly collected in powder pond (17) and cloth bag chamber (11), and during smelting, receiving powder pond temperature in is about 900 ℃, and temperature out is below 200 ℃, promptly receives powder pond receipts powder and carries out between 200-900 ℃.
The object of the present invention is to provide a kind of direct method that adopts is the production technique of raw material production 99.7% grade zinc oxide with the zinc baking sand, and provide device--the novel Furnace for obtaining white zinc of realizing this technology, can reduce production costs significantly, output is doubled, enhance productivity.Adopt this Furnace for obtaining white zinc to produce other grade zinc oxide, also can improve the product purity and the rate of classification of product.
The present invention carries out following improvement for achieving the above object with American process zinc oxide production method and device: 1. when the smelting palletizing ore deposit, cover one deck sulphur-fixing agent on pellet, reduce major impurity sulphur and enter the receipts powder system; 2. adopt the Furnace for obtaining white zinc device smelting palletizing ore deposit of accompanying drawing 2, after making the reaction of zinc fume and secondary air, without cooling, directly under 770-1100 ℃ high temperature, receive powder in the insulating powder pond, stop the formation of water-soluble salt impurity, improve zinc oxide product purity, the purpose of producing 99.7% grade zinc oxide with the zinc ore direct method thereby reach.
Accompanying drawing 2 is Furnace for obtaining white zinc schematic representation of apparatus of the present invention, and this device is made up of body of heater (20), oxidation door (21), oxidizing chamber (22), temperature keeping smoke lane (23), gate (24), insulation settling pocket (25), insulating powder pond (26), waste heat boiler (27), water cooler (28), aluminum pipe (29), cloth bag chamber (30), soot door (31), cleaning door (32,33,34,37), powder exit (35,36), vacuum fan (38), motor (39).
Accompanying drawing 3 is vertical views of apparatus of the present invention.
This device has following characteristics: 1, adopt the twin furnace header structure: the present invention adopts the twin furnace header structure, and two burner wheel flow operations make receipts powder ponds (26) have high-temperature furnace gas to pass through always.And existing Furnace for obtaining white zinc all is single furnace head structures, and batch operation stops to smelt when carrying out other operation, and gate (5) puts down, and the system of gate (5) back does not have furnace gas to pass through, and temperature can reduce.The twin furnace header structure can reach two purposes, and the one, can guarantee that total system receives the powder temperature and remain on more than 770 ℃ always, the 2nd, can increase the throughput of system, output can increase and is twice, and enhances productivity; 2, the lagging material insulation is all adopted in former water-cooled cigarette lane (4), settling pocket (6) and receipts powder ponds (17), and removed cooling water tank (7) and surface cooler (8,9), receipts powder temperature is remained on more than 770 ℃; 3, waste heat boiler (27) and water cooler (28) are arranged between insulating powder pond (26) and the vacuum fan (38), neither influence high temperature and receive the powder operation, recyclable again used heat reduces flue-gas temperature, make flue gas enter cloth bag chamber (30) below 200 ℃, do not influence cloth bag and receive the powder operation.
Adopt other zinc oxide series product of this explained hereafter, also can improve the rate of classification of product and the direct yield of product, for example with because of the foreign matter content height, the off-specification material calcining that existing Furnace for obtaining white zinc system can not produce stair oxidation zinc (99.5%) is a raw material, produces first grade zinc oxide (99.5%).Further describe the present invention below in conjunction with accompanying drawing 2.
In embodiment of the present invention, complete ground coal with one group in the body of heater (20), the goal nodulizing, and on pellet, spread one deck sulphur-fixing agent, as lime, Wingdale, carbide slag, alkaline materials such as sodium hydroxide, require its particle about 30-50MM, waste gas is taken out in air blast then, when presenting a large amount of blue look flame in the stove, can stop to take out waste gas, close fire door, open induced draft fan (38), mention gate (24), begin formal smelting operation, zinc fume is oxidized to zinc oxide through oxidizing chamber, temperature enters settling pocket (25) by cigarette lane (23) about 1200-1300 ℃, because settling pocket is a void tower, sectional area increases, gas velocity reduces, and according to the gravity principle of gathering dust, coarse particles is in this powder sedimentation, contain more PbO, CuO, the particle of impurity such as Cro is thicker, can be removed by settling pocket.Furnace gas enters insulating powder pond (26) then, and its temperature out remains on more than 770 ℃, and when making powder pond (26) receive powder, temperature is higher than ZnSO 4, ZnSO 3, ZnCO 3Decomposition temperature Deng water-soluble salt impurity, stop water-soluble salt to form, the zinc oxide foreign matter content that powder pond (26) is collected is few, obtain meeting 99.7% grade zinc oxide of GB GB/T3185-92, the furnace gas that comes out in powder pond (26) reduces the temperature to below 200 ℃ through waste heat boiler (27), water cooler (28), enter the back emptying of gathering dust of cloth bag chamber, the zinc oxide quality of cloth bag chamber is lower than powder pond (26) slightly.
In first group of burner smelting process, second group of burner begins into operations such as ground coal, pellet, sulphur-fixing agent, waste discharge gas in the body of heater (20).When first group of burner smelting enters the tail powder during phase, second group of burner mentioned gate (24) and begun to smelt, when second group of burner smelting enters the tail powder during phase, first group of burner begins to carry out the smelting of second stove, alternate cycles is smelted like this, can keep receiving the relatively stable of powder pond (26) temperature, thereby guarantee to receive powder pond (26) zinc oxide product quality.This Furnace for obtaining white zinc every day (24 hours) can be smelted the 16-17 stove, and the existing Furnace for obtaining white zinc of output doubles.
The present invention compares with existing zinc oxide production technique, and have the following advantages: 1, production cost is low, and replacing expensive metallic zinc with zinc baking sand is raw material production 99.7% grade zinc oxide, and cost 30-40% can save material.2, production efficiency height owing to adopt the twin furnace header structure, is alternately smelted, and can improve one times of output.3, utilization rate of waste heat height, because the total system major part is taked the insulation measure, waste heat is concentrated by waste heat boiler (27) and water cooler (28) and is reclaimed, and has improved utilization rate of waste heat.4, the novel Furnace for obtaining white zinc of technology of the present invention and isolated plant also can be used for producing other zinc oxide series product, improves the rate of classification of product and the direct yield of product.For example will be owing to the foreign matter content height, existing Furnace for obtaining white zinc can not be produced the off-specification material zinc baking sand of 99.5% grade zinc oxide as raw material, produces 99.5% grade zinc oxide, and the direct yield of first grade (99.5%) can reach more than 80%.
Embodiment:
Below be 12M 2Novel Furnace for obtaining white zinc is produced the implementation data of zinc oxide; And the zinc oxide monthly output is 400 tons.Embodiment 1:produce 99.7% grade zinc oxide zinc baking sand composition, (%): Zn Pb Cd Cu S 69.06 0.011 0.012 0.26 0.41 pellet compositions, (%): Zn Pb Cu As S 36.52 0.038 0.17 0.07 0.69 technical qualification:cover the thick lime particle of one deck 60MM on pellet; Particle diameter is between 30-50MM; 120 minutes tap to tap time, 1090-850 ℃ of in powder. of receive pond temperature receives powder pond zinc oxide composition (%): the water-soluble salt igloss of ZnO PbO CuO hydrochloric acid insoluble substance 99.72 0.030 0.0001 0.07 0.15 0.003 embodiment 2: produce 99.7% grade zinc oxide zinc calcine composition (%): Zn Pb Cd Cu S 68.83 0.033 0.014 0.21 0.25 pellet compositions (%): Zn Pb Cu As S 36.55 0.027 0.16 0.08 0.52 technical conditions: cover the thick lime particle of one deck 60MM at pellet; Particle diameter is between 30-50MM; 130 minutes durations of heat, receive pond temperature 1030-770 ℃ of of in powder. Receive powder pond zinc oxide composition (%): Zn0 PbO CuO water-soluble salt igloss hydrochloric acid insoluble substance 99.70 0.021 0.0001 0.10 0.19 0.005 embodiment 3:produce 99.7% grade zinc oxide zinc baking sand composition (%): Zn Pb Cd Cu S 67.95 0.035 0.015 0.20 0.39 pellet compositions (%): Zn Pb Cu As S 36.12 0.032 0.17 0.08 0.56 technical qualification:on pellet, cover the thick lime particle of one deck 60MM, particle diameter is between 30-50MM, 125 minutes tap to tap time, receive pond temperature 1080-800 ℃ of of of in powder.Receive powder pond zinc oxide composition (%): ZnO PbO CuO water-soluble salt igloss hydrochloric acid insoluble substance 99.70 0.027 0.0001 0.08 0.17 0.005 embodiment 4:produce 99.5% grade zinc oxide with the off-specification material calcining.Zinc baking sand composition (%): Zn Pb Cd Cu S 63.80 0.35 0.026 0.47 0.58 pellet compositions (%): Zn Pb Cu As S 33.41 0.18 0.31 0.25 0.86 technical qualification:on pellet, cover the thick lime particle of one deck 60MM, particle diameter is between 30-50MM, 120 minutes tap to tap time, receive pond temperature 1080-810 ℃ of of of in powder.Receive powder pond zinc oxide composition (%): ZnO PbO CuO water-soluble salt igloss hydrochloric acid insoluble substance 99.52 0.10 0.005 0.32 0.35 0.018

Claims (4)

1. Furnace for obtaining white zinc device of producing high-grade zinc oxide, by body of heater (20), oxidation door (21), oxidizing chamber (22), temperature keeping smoke lane (23), gate (24), insulation settling pocket (25), insulating powder pond (26), waste heat boiler (27), water cooler (28), aluminum pipe (29), cloth bag chamber (30), soot door (31), cleaning door (32,33,34,37), powder exit (35,36), vacuum fan (38), motor (39) is formed, it is characterized in that adopting temperature keeping smoke lane (23), powder pond (26) is received in insulation settling pocket (25) and insulation, and adopt the twin furnace header structure, two bodies of heater (20) are arranged, two oxidizing chambers (22), two temperature keeping smoke lanes (23), two insulation settling pockets (25) and two gates (24).
2. according to the Furnace for obtaining white zinc device of claim 1, it is characterized in that temperature keeping smoke lane (23), insulation settling pocket (25) and insulation receipts powder ponds (26) are all at its external coating lagging material.
3. according to the Furnace for obtaining white zinc device of claim 1, it is characterized in that waste heat boiler (27) and water cooler (28) are arranged between receipts powder pond (26) and the vacuum fan (38).
4. method of producing high-grade zinc oxide, it is characterized in that using the Furnace for obtaining white zinc device of claim 1, adopt twin furnace header structure wheel flow operation to smelt, cover one deck sulphur-fixing agent when body of heater (20) smelting palletizing ore deposit on pellet, insulating powder pond (26) receive powder under 770-1100 ℃ high temperature.
CN 00107928 2000-05-30 2000-05-30 Process and apparatus of direct producing high-grade zinc oxide Expired - Fee Related CN1127577C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 00107928 CN1127577C (en) 2000-05-30 2000-05-30 Process and apparatus of direct producing high-grade zinc oxide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 00107928 CN1127577C (en) 2000-05-30 2000-05-30 Process and apparatus of direct producing high-grade zinc oxide

Publications (2)

Publication Number Publication Date
CN1284571A true CN1284571A (en) 2001-02-21
CN1127577C CN1127577C (en) 2003-11-12

Family

ID=4579029

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 00107928 Expired - Fee Related CN1127577C (en) 2000-05-30 2000-05-30 Process and apparatus of direct producing high-grade zinc oxide

Country Status (1)

Country Link
CN (1) CN1127577C (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103834819A (en) * 2013-12-05 2014-06-04 湖南水口山有色金属集团有限公司 Method for direct production of high-grade zinc oxide from zinc material containing high chlorine and fluorine
CN103861440A (en) * 2013-12-26 2014-06-18 张明鑫 Layer burning furnace desulfurization and denitrification flue gas treatment technology
CN104212980A (en) * 2014-09-01 2014-12-17 常熟市荣兴化纺有限责任公司 Zinc oxide collecting device
CN104232930A (en) * 2014-09-01 2014-12-24 常熟市荣兴化纺有限责任公司 Air pulse zinc oxide collecting device
CN108220621A (en) * 2018-01-09 2018-06-29 石家庄市龙力化工有限公司 A kind of technique of direct method production high-purity zinc oxide
CN110592395A (en) * 2019-10-25 2019-12-20 赫章领轩环保科技有限公司 Production line for producing high-grade direct method zinc oxide and technological process thereof
CN112391535A (en) * 2020-10-27 2021-02-23 山西于斯为盛环保科技有限公司 Treatment and utilization device and method for recovering zinc oxide from metallurgical zinc-containing ash by suspension smelting reduction
CN114309020A (en) * 2022-01-04 2022-04-12 重庆赛迪热工环保工程技术有限公司 Pyrogenic time-sharing treatment method for metallurgical zinc-containing dust sludge
CN117663743A (en) * 2023-12-14 2024-03-08 高邑县永昌锌业有限责任公司 Zinc oxide smelting furnace and smelting method

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103834819A (en) * 2013-12-05 2014-06-04 湖南水口山有色金属集团有限公司 Method for direct production of high-grade zinc oxide from zinc material containing high chlorine and fluorine
CN103834819B (en) * 2013-12-05 2016-04-27 湖南水口山有色金属集团有限公司 A kind of method containing the zinc material direct producing high-grade zinc oxide of high chlorine and fluorine
CN103861440A (en) * 2013-12-26 2014-06-18 张明鑫 Layer burning furnace desulfurization and denitrification flue gas treatment technology
CN103861440B (en) * 2013-12-26 2016-01-20 张明鑫 Layer burning stove desulfurization removing nitric flue gas treating process
CN104212980A (en) * 2014-09-01 2014-12-17 常熟市荣兴化纺有限责任公司 Zinc oxide collecting device
CN104232930A (en) * 2014-09-01 2014-12-24 常熟市荣兴化纺有限责任公司 Air pulse zinc oxide collecting device
CN108220621A (en) * 2018-01-09 2018-06-29 石家庄市龙力化工有限公司 A kind of technique of direct method production high-purity zinc oxide
CN110592395A (en) * 2019-10-25 2019-12-20 赫章领轩环保科技有限公司 Production line for producing high-grade direct method zinc oxide and technological process thereof
CN112391535A (en) * 2020-10-27 2021-02-23 山西于斯为盛环保科技有限公司 Treatment and utilization device and method for recovering zinc oxide from metallurgical zinc-containing ash by suspension smelting reduction
CN112391535B (en) * 2020-10-27 2025-12-16 山西于斯为盛环保科技有限公司 Treatment and utilization device and method for recycling zinc oxide by suspension smelting reduction of metallurgical zinc-containing ash
CN114309020A (en) * 2022-01-04 2022-04-12 重庆赛迪热工环保工程技术有限公司 Pyrogenic time-sharing treatment method for metallurgical zinc-containing dust sludge
CN114309020B (en) * 2022-01-04 2023-06-13 重庆赛迪热工环保工程技术有限公司 Pyrometallurgical zinc-containing dust sludge pyrogenic time-sharing disposal method
CN117663743A (en) * 2023-12-14 2024-03-08 高邑县永昌锌业有限责任公司 Zinc oxide smelting furnace and smelting method
CN117663743B (en) * 2023-12-14 2024-06-21 高邑县永昌锌业有限责任公司 Zinc oxide smelting furnace and smelting method

Also Published As

Publication number Publication date
CN1127577C (en) 2003-11-12

Similar Documents

Publication Publication Date Title
CN102181663B (en) Method for producing zinc powder by treating zinc-containing miscellaneous material through electric furnace
CN103805787B (en) A kind of method reclaiming valuable metal from iron concentrate slag
CN107760875B (en) Production line and process for producing metallized furnace burden from blast furnace gas ash
CN103131869A (en) Extraction method for high-lead high-silver arsenious complex gold concentrate
CN1127577C (en) Process and apparatus of direct producing high-grade zinc oxide
CN110283996A (en) A kind of smelting process of energy-saving and environment-friendly copper-contained sludge
CN1035831C (en) Direct reduction process for oxygen-rich fusion gasifying furnace
CN102102153B (en) Method for producing zinc oxide and iron by treating zinc ore (slag) in reduction rotary kiln
CN1644720A (en) Oxygen-enriched zinc smelting method
CN113981228A (en) A method for inhibiting ring formation in kiln and improving zinc recovery rate
CN108759461B (en) Equipment and method for graded production of direct zinc oxide by tunnel kiln
CN114317965A (en) Process and device for smelting and reducing zinc-containing material by thermite method
CN101525685B (en) High-alkali clinker sodium roasting hydrometallurgy method
CN1587060A (en) Method for producing zinc suboxide
CN206828592U (en) A kind of system for handling lead and zinc smelting dreg
CN208620816U (en) A kind of equipment of Novel tunnel-type kiln classification production American process zinc oxide
CN116287761B (en) Method, device and application of pyrometallurgical lead and zinc smelting
CN116240393B (en) Process for directly producing grade zinc oxide by utilizing dangerous waste electric furnace steelmaking dust collection ash
CN201779968U (en) Roasting system of moving bed
CN116065024A (en) A method for preparing zinc calcined sand by utilizing zinc-containing waste slag
CN102409162B (en) Method and device for roasting sodium oxide by using shaft furnace
CN1239719C (en) Circulating fluidized bed mineral reducing roasting device and reducing roasting method
CN115584373A (en) Direct reduction process and device for dedusting ash of steel plant
CN209292440U (en) A kind of device that metallurgy dedusting ash containing zinc is administered and utilized
CN202347064U (en) Shaft furnace type oxidization and sodium treatment roasting device

Legal Events

Date Code Title Description
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C06 Publication
PB01 Publication
C14 Grant of patent or utility model
GR01 Patent grant
C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee