CN107384636A - A kind of relatively mild Transparent soap base cleaning formulation - Google Patents
A kind of relatively mild Transparent soap base cleaning formulation Download PDFInfo
- Publication number
- CN107384636A CN107384636A CN201710649513.9A CN201710649513A CN107384636A CN 107384636 A CN107384636 A CN 107384636A CN 201710649513 A CN201710649513 A CN 201710649513A CN 107384636 A CN107384636 A CN 107384636A
- Authority
- CN
- China
- Prior art keywords
- soap base
- relatively mild
- transparent soap
- acid
- skin cleansing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000344 soap Substances 0.000 title claims abstract description 66
- 239000000203 mixture Substances 0.000 title claims abstract description 36
- 238000009472 formulation Methods 0.000 title claims abstract description 26
- 238000004140 cleaning Methods 0.000 title claims abstract description 15
- 239000002253 acid Substances 0.000 claims abstract description 36
- 125000001931 aliphatic group Chemical group 0.000 claims abstract description 29
- 150000001412 amines Chemical class 0.000 claims abstract description 26
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 11
- 239000000194 fatty acid Substances 0.000 claims description 11
- 229930195729 fatty acid Natural products 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 10
- 239000002562 thickening agent Substances 0.000 claims description 9
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical group OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 claims description 9
- 229960000281 trometamol Drugs 0.000 claims description 9
- -1 carbon fatty acids Chemical class 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 150000005846 sugar alcohols Polymers 0.000 claims description 8
- 239000004094 surface-active agent Substances 0.000 claims description 8
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- 239000006260 foam Substances 0.000 claims description 6
- 239000003755 preservative agent Substances 0.000 claims description 6
- 230000002335 preservative effect Effects 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical compound CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 claims description 5
- 235000011187 glycerol Nutrition 0.000 claims description 5
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 4
- 235000021355 Stearic acid Nutrition 0.000 claims description 4
- 239000003963 antioxidant agent Substances 0.000 claims description 4
- 230000003078 antioxidant effect Effects 0.000 claims description 4
- 239000001913 cellulose Substances 0.000 claims description 4
- 229920002678 cellulose Polymers 0.000 claims description 4
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 claims description 4
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 4
- 229940070765 laurate Drugs 0.000 claims description 4
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 4
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 4
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 4
- 239000008117 stearic acid Substances 0.000 claims description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 3
- 239000002738 chelating agent Substances 0.000 claims description 3
- 230000003750 conditioning effect Effects 0.000 claims description 3
- 239000000686 essence Substances 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 235000021314 Palmitic acid Nutrition 0.000 claims description 2
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- 229920002125 Sokalan® Polymers 0.000 claims description 2
- OBETXYAYXDNJHR-UHFFFAOYSA-N alpha-ethylcaproic acid Natural products CCCCC(CC)C(O)=O OBETXYAYXDNJHR-UHFFFAOYSA-N 0.000 claims description 2
- 239000002280 amphoteric surfactant Substances 0.000 claims description 2
- 239000003945 anionic surfactant Substances 0.000 claims description 2
- 239000003093 cationic surfactant Substances 0.000 claims description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 2
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 2
- 239000000049 pigment Substances 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- AXPZIVKEZRHGAS-UHFFFAOYSA-N 3-benzyl-5-[(2-nitrophenoxy)methyl]oxolan-2-one Chemical compound [O-][N+](=O)C1=CC=CC=C1OCC1OC(=O)C(CC=2C=CC=CC=2)C1 AXPZIVKEZRHGAS-UHFFFAOYSA-N 0.000 claims 1
- 230000003213 activating effect Effects 0.000 claims 1
- 229960001631 carbomer Drugs 0.000 claims 1
- 238000005187 foaming Methods 0.000 abstract description 8
- 238000000034 method Methods 0.000 abstract description 8
- 238000011010 flushing procedure Methods 0.000 abstract description 2
- 239000002585 base Substances 0.000 description 52
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 18
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- 238000002360 preparation method Methods 0.000 description 9
- 238000012360 testing method Methods 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 6
- 230000001815 facial effect Effects 0.000 description 6
- 238000001556 precipitation Methods 0.000 description 6
- 230000008859 change Effects 0.000 description 5
- 238000002845 discoloration Methods 0.000 description 5
- 150000004665 fatty acids Chemical class 0.000 description 5
- 238000007127 saponification reaction Methods 0.000 description 4
- 235000011121 sodium hydroxide Nutrition 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 235000019441 ethanol Nutrition 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 150000007524 organic acids Chemical class 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- WLAMNBDJUVNPJU-UHFFFAOYSA-N 2-methylbutyric acid Chemical compound CCC(C)C(O)=O WLAMNBDJUVNPJU-UHFFFAOYSA-N 0.000 description 2
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 2
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 229940082484 carbomer-934 Drugs 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 235000019197 fats Nutrition 0.000 description 2
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 2
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 description 2
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 description 2
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 description 2
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- LNAZSHAWQACDHT-XIYTZBAFSA-N (2r,3r,4s,5r,6s)-4,5-dimethoxy-2-(methoxymethyl)-3-[(2s,3r,4s,5r,6r)-3,4,5-trimethoxy-6-(methoxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6r)-4,5,6-trimethoxy-2-(methoxymethyl)oxan-3-yl]oxyoxane Chemical compound CO[C@@H]1[C@@H](OC)[C@H](OC)[C@@H](COC)O[C@H]1O[C@H]1[C@H](OC)[C@@H](OC)[C@H](O[C@H]2[C@@H]([C@@H](OC)[C@H](OC)O[C@@H]2COC)OC)O[C@@H]1COC LNAZSHAWQACDHT-XIYTZBAFSA-N 0.000 description 1
- 229940058015 1,3-butylene glycol Drugs 0.000 description 1
- SPSPIUSUWPLVKD-UHFFFAOYSA-N 2,3-dibutyl-6-methylphenol Chemical group CCCCC1=CC=C(C)C(O)=C1CCCC SPSPIUSUWPLVKD-UHFFFAOYSA-N 0.000 description 1
- JVTIXNMXDLQEJE-UHFFFAOYSA-N 2-decanoyloxypropyl decanoate 2-octanoyloxypropyl octanoate Chemical compound C(CCCCCCC)(=O)OCC(C)OC(CCCCCCC)=O.C(=O)(CCCCCCCCC)OCC(C)OC(=O)CCCCCCCCC JVTIXNMXDLQEJE-UHFFFAOYSA-N 0.000 description 1
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 description 1
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- 235000009024 Ceanothus sanguineus Nutrition 0.000 description 1
- 241000040710 Chela Species 0.000 description 1
- 241001269238 Data Species 0.000 description 1
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical group [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 240000003553 Leptospermum scoparium Species 0.000 description 1
- 235000015459 Lycium barbarum Nutrition 0.000 description 1
- 206010054949 Metaplasia Diseases 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical class CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 1
- 208000028990 Skin injury Diseases 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- YOUBLKPZGAHMAH-UHFFFAOYSA-N azane;butan-2-ol Chemical compound N.CCC(C)O YOUBLKPZGAHMAH-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229960003237 betaine Drugs 0.000 description 1
- 235000019437 butane-1,3-diol Nutrition 0.000 description 1
- 235000010354 butylated hydroxytoluene Nutrition 0.000 description 1
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical class [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000013538 functional additive Substances 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 1
- 235000021552 granulated sugar Nutrition 0.000 description 1
- 239000003845 household chemical Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 230000015689 metaplastic ossification Effects 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- CKQVRZJOMJRTOY-UHFFFAOYSA-N octadecanoic acid;propane-1,2,3-triol Chemical compound OCC(O)CO.CCCCCCCCCCCCCCCCCC(O)=O CKQVRZJOMJRTOY-UHFFFAOYSA-N 0.000 description 1
- 229960002446 octanoic acid Drugs 0.000 description 1
- 229940097411 palm acid Drugs 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 229910001950 potassium oxide Inorganic materials 0.000 description 1
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 description 1
- YPFDHNVEDLHUCE-UHFFFAOYSA-N propane-1,3-diol Chemical class OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- 238000000518 rheometry Methods 0.000 description 1
- 229960004889 salicylic acid Drugs 0.000 description 1
- 230000001835 salubrious effect Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 229960004274 stearic acid Drugs 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/007—Soaps or soap mixtures with well defined chain length
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/08—Water-soluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/225—Polymers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
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- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
- A61K2800/262—Transparent; Translucent
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
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Abstract
The invention discloses a kind of relatively mild Transparent soap base skin cleansing formulations, it is characterised in that including organic amine and aliphatic acid with dissolving and heat absorbing, wherein described aliphatic acid and organic amine weight are than 1：(1 2.5), using in organic amine and the method for aliphatic acid makes Transparent soap base cleaning formulation, there is foaming abundancy, easily flushing, and the features such as high temperature is non-discolouring, and 5 DEG C of low temperature does not separate out, and the pH scopes of human body skin are more nearly, more gently.
Description
Technical field
The present invention relates to household chemicals field, especially designs a kind of gentle Transparent soap base Cleasing compositions.
Background technology
Recently as the improvement of people's living standards, to cosmetics requirement also more and more higher, for washing class product, soap
The foaming power of base face cleaning is good, foaming abundancy, is easily rinsed after, carrys out clean salubrious sense to skin tape, exactly because these characteristics, soap
Base class product is liked by everybody deeply, but has the product of many soaps, such as solid soap on the market, face cleaning cream, liquid facial soap, is all white
The outward appearance of color, and the PH of soap base face cleaning class product is generally in 9.5-10.5 or so, and few soap base face cleaning gels.Face cleaning gel
Also more AES, glycine betaine etc. are principal surfactant to shape product, do not have the easy flushing sense of soap base in cleaning process.It is such as special
Sharp CN103126911A discloses a kind of gentle Soap-base facial cleanser composition, and it includes the Soap-base facial cleanser composition gross weight
The soap base of amount 2.0% to 50.0%, the anion surface active of the Soap-base facial cleanser composition total weight 2.0%-30.0%
Agent, account for the rheology control agent of the Soap-base facial cleanser composition total weight 0.1% to 10.0%, and excess water.The soap base is clean
Face composite cream pH value is 8.0-11.0, wherein the soap base is made up of 2.0-40.0% aliphatic acid and 0-10% alkali, wherein
Alkali is sodium hydroxide, potassium hydroxide, triethanolamine, solve moisten after gentle wash it is not tight, but with three ethanol in the patent
Amine neutralizes, and the soap surfactant produced has the shortcomings that easy high-temperature discoloration, and the soap made is put also can become yellow by transparent long afterwards
It is transparent.As patent CN201611247052A discloses a kind of in the transparent soap sill of low-temperature stabilization and composition, solves technical problem
Low temperature separates out discoloration problem, there is provided a kind of aliphatic acid comprising higher concentration and polytype surfactant, alkali selection hydrogen
Potassium oxide, the composition keep transparent appearance after recovering room temperature at transparent state and (- 5 ± 2) DEG C at 5 DEG C, avoid making
Used with triethanolamine with potassium hydroxide and prepare Transparent soap base with comprising higher concentration aliphatic acid.CN201611242812 is disclosed
A kind of high-temperature stable, cost-effective, foaming abundancy, not tight Soap-base facial cleanser is moistened after washing, it includes stearic acid, bay
Acid, myristic acid, rilanit special, stearine, PGE-100 stearates, potassium hydroxide, glycerine, propane diols, EDTA
Disodium, preservative, essence, hydroxypropyl methyl cellulose, preservative etc., in the patent and with potassium hydroxide with aliphatic acid come
Prepare the soap base of high-temperature stable.But the highly basic such as sodium hydroxide, potassium is very big to human body skin injury, in plant produced, dissolving
Potassium hydroxide, sodium hydroxide can be highly exothermic, have certain danger in operation.CN201310522853A discloses one kind
Transparent soap base, including liquid caustic soda, palm oil, coconut oil, castor oil, alcohol, glycerine, granulated sugar and water, by adjusting said components
Ratio controls the transparency of soap base, inoxidizability and moisturizing function.
Therefore, a kind of Transparent soap base and product has foaming abundancy, easily rinse, and high temperature is non-discolouring, and 5 ° of low temperature is not analysed
Go out, be gently the product of market in urgent need to the inirritative soap based cleansing product of skin.
The content of the invention
In order to solve the above-mentioned technical problem, the present invention provides a kind of relatively mild Transparent soap base skin cleansing formulations, should
Preparation has that transparent, high temperature is non-discolouring, and low temperature does not separate out, gentle inirritative effect, and in technological operation, the neutralization used
Agent organic amine is endothermic process in course of dissolution, safe operation.
A kind of preparation method of relatively mild Transparent soap base skin cleansing formulations of another object of the present invention.
To achieve the above object, the present invention is achieved through the following technical solutions：
A kind of relatively mild Transparent soap base skin cleansing formulations, it is characterised in that including with the organic of dissolving and heat absorbing
Amine and aliphatic acid, wherein described aliphatic acid and organic amine weight are than 1：(1-2.5).Said preparation is genuine soap base.
Preferably, in above-mentioned technical proposal, aliphatic acid is with organic amine weight than 1：(2-2.5).
A kind of relatively mild Transparent soap base skin cleansing formulations, including following materials by weight percentage
Aliphatic acid 6-20%
Organic amine 13-35%
Thickener 0-2%
Helper component 0-30%
Water surplus.
Preferably, a kind of relatively mild Transparent soap base skin cleansing formulations, including following materials by weight percentage
Aliphatic acid 6-20%
Organic amine 13-20%
Thickener 1-2%
Helper component 3-30%
Water surplus.
It is further preferred that a kind of relatively mild Transparent soap base skin cleansing formulations, including following weight percentage
Raw material
Aliphatic acid 6-10%
Organic amine 13-20%
Thickener 1-2%
Helper component 3-30%
Water surplus.
Preferably, in above-mentioned technical proposal, a kind of relatively mild Transparent soap base skin cleansing formulations pH value of the present invention≤
9, preferable ph 8.0-9.0, the pH value be not tight closer to the pH value range of human body skin, comfort level milder.
Preferably, in above-mentioned technical proposal, the aliphatic acid includes but is not limited to octanoic acid, laurate, myristic acid, palm
Acid, stearic acid, one in mountain Yu acid, 12 carbon fatty acids, tetradecacarbon fatty acid, 16 carbon fatty acids, 22 carbon fatty acids
Kind or its more than.It is preferred that laurate, myristic acid, palmitic acid, stearic acid is one or more of in Yu's acid of mountain.Selected by the present invention
Higher fatty acids prepare Transparent soap base molten point can control, the water-soluble of soap is more preferable, and foam gently enriches.
Preferably, in above-mentioned technical proposal, described organic amine is tromethamine, one or two kinds of groups in aminomethyl propanol
Close.The tromethamine, aminomethyl propanol reacts as nertralizer and aliphatic acid to be prepared soap base and plays cleaning action,
Prevent high temperature soap base body from changing colour, and in technique preparation, it is endothermic process in course of dissolution, and safe operation is adapted to industry
Metaplasia is produced.Using tromethamine, aminomethyl propanol makes soap base pH value≤9 being prepared, it is not necessary to reuses acid-base modifier.
The no discoloration of soap base high temperature low temperature prepared present invention preferably employs tromethamine and precipitation problem, and foaming abundancy.And ammonia
Methylpropanol high temperature is non-discolouring, and low temperature does not separate out, but foam is not very abundant relatively.
Preferably, in above-mentioned technical proposal, described thickener includes but is not limited to cellulose, carbomer series etc., institute
State cellulose and include but is not limited to hydroxyethyl cellulose, methylcellulose, hydroxypropyl methyl cellulose, carboxymethyl cellulose etc..
The carbomer series includes Acritamer 940, Carbopol 941, carbomer 934, carbomer934, Carbopol etc..The present invention
Preferred thickener is cellulose, and it can increase the vicidity of soap base, reaches suitable use feeling, so as to ensure that soap base is low in high temperature
Stablize under the conditions of temperature not stratified.
Preferably, in above-mentioned technical proposal, after adding helper component, the soap base of preparation more moistens skin sensitivity height.
Described helper component includes but is not limited to polyalcohol, surfactant, skin conditioning agent, antioxidant, preservative, essence, chela
Several combinations one or more of mixture, pigment etc..
The polyalcohol include but is not limited to 1,2- propane diols, 1,3- propane diols, 1,3 butylene glycol, glycerine, polyethylene glycol-
8, the one or more combination in polyethylene glycol -32, pungent glycol.Dosage 5-30%.It can increase solubility after increase polyalcohol,
Strengthen stability.
The surfactant includes but is not limited to anion surfactant, cationic surfactant and nonionic table
Face activity, the one or more combination of amphoteric surfactant, for adjusting abundant degree and the different skin senses experience of foam.
Dosage 0-10%.
Described skin conditioning agent refers to conventional functional additive such as salicylic acid, tea tree ethereal oil etc..Dosage 0-3%.
The antioxidant is dibutyl hydroxy toluene.
The chelating agent is EDTA-2Na.
It can be used for including but is not limited to thoroughly present invention also offers a kind of relatively mild Transparent soap base skin cleansing formulations
Used in clear and bright face gel, transparent bath foam, the transparent formula for washing hair care.
Present invention also offers a kind of preparation method of relatively mild Transparent soap base skin cleansing formulations, it includes as follows
Step：
1. water is added in main still, thickener normal temperature is added to the water to stir it is heated to 80-85 DEG C, swelling is abundant, adds
Enter organic amine, dissolve, polyalcohol is added before saponification；
2. aliphatic acid, antioxidant are heated into 80-85 DEG C of dissolving, add in aqueous phase, be incubated saponification, add chelating agent, stir
Mix dissolving；
3. it is cooled to 60-65 DEG C of addition surfactant；
4. being cooled to 40-45 DEG C, preservative is added, is cooled to 38 DEG C, detection discharging.
In order to preferably embody beneficial effects of the present invention, illustrated by following test examples
The stability of test example one and contrast test
1. method：Of the present invention group, contrast groups and ratio are shown in Table 1, compare stability table 2 Fig. 1, Fig. 2 after 2 months.
2. result：Visible by table 2, the embodiment of the present invention 1 and comparative example 1 compare, and the present invention is prepared using tromethamine
Soap base high temperature low temperature without change colour and separate out problem, pellucidity is very stable always.And comparative example 1 is matched somebody with somebody using triethanolamine
There is discoloration for 40,48 degrees Celsius in high temperature in the soap base of system, and gradually deepens with the rise color of temperature, occurs in low temperature
Precipitation problem.Comparative example 2 using potassium hydroxide configuration soap base, high temperature is non-discolouring, can low temperature can separate out.The embodiment of the present invention
2.3 and embodiment 1 compare, embodiment 2.3 is that the assisted groups such as polyalcohol, surfactant are added on the basis of embodiment 1
Point, but helper component does not influence on the stability of Transparent soap base, the problem of high-temperature discoloration low temperature precipitation does not occur.
Table 1 is grouped and prescription
Table 2, PH are two months stability datas of 8.5-9.0：
Test example difatty acid, organic amine selection or proportioning screening test
The gentle Transparent soap base preparation of the present invention can obtain not by aliphatic acid, any selection of organic amine or cooperation,
But soap base in background technology can be just overcome some unsatisfactory parameters or phenomenon to be present by the screening of characteristic ratio.Specifically
It is shown in Table 3.It is visible by table 3：Content of fatty acid is higher, and viscosity is bigger, and foam is also abundanter.It can according to demand be adjusted, send out
A person of good sense has found, when content of fatty acid is too high, it may appear that low temperature precipitation phenomenon.In order to avoid foaming abundancy, aliphatic acid is saltoutd simultaneously
Go out, then need to increase the organic amine i.e. dosage of tromethamine simultaneously, you can avoid the precipitation of high fatty acid, it is therefore necessary to meet fat
Fat acid maintains 1 with organic amine ratio:(1-2.5), preferably 1：Precipitation phenomenon is avoided when (2-2.5).But in comparative example 2, right
Even if inventor has found aliphatic acid and organic amine amount ratio 1 in 3 groups of ratio:In (1-2.5), when aliphatic acid is total with organic acid
When dosage reaches 40%, 5 DEG C of low temperature slightly separate out, when aliphatic acid and the total dosage of organic acid are higher than 60%, it may appear that low temperature is a large amount of
Separate out.Therefore, inventor is drawn only in the case of meeting that aliphatic acid and the total dosage of organic acid are no more than 40%, no matter soap base system
Whether the auxiliary auxiliary material such as polyalcohol is dosed in agent, it is necessary to meets that aliphatic acid and organic amine ratio maintain 1:(1-2.5), preferably 1：
Under (2-2.5) state, obtained soap base high temperature is non-discolouring, and low temperature does not separate out.
Table 3 is grouped
The skin sense of test example three is tested
Method：Human body face cleaning test assessment determines
10 volunteers are chosen, formulation product face cleaning in table 4 is taken, is evaluated by scoring mechanism, it is more by washing Experimental comparison by rubbing with the hands
The compounding of first alcohol is can be improved to the tight feeling after soap base system is washed.
Table 4
Compared with prior art, the present invention has the advantages that
The present invention utilizes the method in organic amine with aliphatic acid to make Transparent soap base cleaning formulation, has foaming abundancy, easily
Rinse, and the features such as high temperature is non-discolouring, and 5 DEG C of low temperature does not separate out, and the pH scopes of human body skin are more nearly, more gently.
It can be configured by compounding the auxiliary element such as polyalcohol and table work with the Transparent soap base cleaning formulation for moistening skin sense.This hair
It is bright to select organic amine species dissolving and heat absorbing in production, operational hazards are avoided, are easy to industrialization.And pH value≤9 pH value is more
It is not tight close to the pH value range of human body skin, comfort level milder.
Brief description of the drawings
Fig. 1 be according to an embodiment of the invention 1 and contrast 1 at 48 DEG C, 2 months stability experiment figures.
The wherein colourless transparent solution of embodiment 1, comparative example 1 are yellow solution
Fig. 2 be according to an embodiment of the invention 1 and contrast 1 at 5 DEG C, 2 months stability experiment figures
The wherein colourless transparent solution of embodiment 1, the white crystals of comparative example 1
Embodiment
Below in conjunction with the accompanying drawings, the embodiment of the present invention is described in detail, it is to be understood that the guarantor of the present invention
Shield scope is not limited by embodiment.
Explicitly indicated that unless otherwise other, otherwise in entire disclosure and claims, term " comprising " or its change
Change such as "comprising" or " including " etc. and will be understood to comprise stated element or part, and do not exclude other members
Part or other parts.
Embodiment 1-8
A kind of gentle Transparent soap base preparation of the present invention
Preparation method：Water is added in main still, hydroxyethyl cellulose normal temperature is added to the water to stir is heated to 80-85
DEG C, swelling is abundant, adds tromethamine, dissolving, PEG-8, glycerine is added before saponification；By laurate, myristic acid, dibutyl hydroxyl
Base toluene is heated to 80-85 DEG C of dissolving, adds in aqueous phase, is incubated saponification 20min, adds EDTA2NA, stirring and dissolving；It is cooled to
60-65 DEG C adds Cocoamidopropyl betaine, LAA；40-45 DEG C is cooled to, adds preservative, drop
Temperature is to 38 DEG C, detection discharging.
Embodiment 9-16
Change tromethamine in embodiment 1-8 into aminomethyl propanol, other compositions are constant.
Embodiment 17-24
The description of the foregoing specific illustrative embodiment to the present invention is to illustrate and the purpose of illustration.These descriptions
It is not wishing to limit the invention to disclosed precise forms, and it will be apparent that according to above-mentioned teaching, can be much changed
And change.The purpose of selecting and describing the exemplary embodiment is that explain that the certain principles of the present invention and its reality should
With so that those skilled in the art can realize and utilize the present invention a variety of exemplaries and
Various chooses and changes.The scope of the present invention is intended to be limited by claims and its equivalents.
Claims (10)
1. a kind of relatively mild Transparent soap base skin cleansing formulations, it is characterised in that including the organic amine with dissolving and heat absorbing
And aliphatic acid, wherein the aliphatic acid and organic amine weight are than 1：(1-2.5).
2. a kind of relatively mild Transparent soap base skin cleansing formulations as claimed in claim 1, including following weight percentage
Raw material
Aliphatic acid 6-20%
Organic amine 13-35%
Thickener 0-2%
Helper component 0-30%
Water surplus.
3. a kind of relatively mild Transparent soap base skin cleansing formulations as claimed in claim 2, including following weight percentage
Raw material
Aliphatic acid 6-20%
Organic amine 13-20%
Thickener 1-2%
Helper component 3-30%
Water surplus.
A kind of 4. relatively mild Transparent soap base skin cleansing formulations as described in claim 1-3 is any, it is characterised in that institute
Aliphatic acid is stated as octanoic acid, laurate, myristic acid, palmitic acid, stearic acid, mountain Yu acid, 12 carbon fatty acids, 14 carbocyclic aliphatics
Acid, 16 carbon fatty acids, one kind in 22 carbon fatty acids or its more than.
A kind of 5. relatively mild Transparent soap base skin cleansing formulations as described in claim 1-3 is any, it is characterised in that institute
It is tromethamine to state organic amine, one or two kinds of combinations in aminomethyl propanol.
A kind of 6. relatively mild Transparent soap base skin cleansing formulations as described in Claims 2 or 3 is any, it is characterised in that
The thickener is cellulose or carbomer.
7. such as claim 2 or a kind of described relatively mild Transparent soap base skin cleansing formulations, it is characterised in that described auxiliary
Helping component includes polyalcohol, antioxidant, chelating agent, surfactant, skin conditioning agent, preservative, essence, pigment it is a kind of or with
Upper several combinations.
8. a kind of relatively mild Transparent soap base skin cleansing formulations as claimed in claim 7, it is characterised in that described polynary
Alcohol is 1,2-PD, 1,3-PD, 1,3-BDO, glycerine, PEG-8, one in polyethylene glycol -32, pungent glycol
Kind or several combinations, dosage 5-30%.
A kind of 9. relatively mild Transparent soap base skin cleansing formulations as claimed in claim 7, it is characterised in that the surface
Activating agent is anion surfactant, cationic surfactant and non-ionic surface active, the one of amphoteric surfactant
Kind or several combinations, dosage 0-10%.
A kind of 10. relatively mild Transparent soap base skin cleansing formulations as described in claim 1-3 is any, it is characterised in that：
For being used in transparent face cleaning gel, transparent bath foam, the transparent formula for washing hair care.
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