CA2027445A1 - Fluides dielectriques par condensation de composes aromatiques dont certains halogenes - Google Patents
Fluides dielectriques par condensation de composes aromatiques dont certains halogenesInfo
- Publication number
- CA2027445A1 CA2027445A1 CA2027445A CA2027445A CA2027445A1 CA 2027445 A1 CA2027445 A1 CA 2027445A1 CA 2027445 A CA2027445 A CA 2027445A CA 2027445 A CA2027445 A CA 2027445A CA 2027445 A1 CA2027445 A1 CA 2027445A1
- Authority
- CA
- Canada
- Prior art keywords
- condensation
- synthesis
- aromatic compounds
- dielectric fluids
- including halides
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001491 aromatic compounds Chemical class 0.000 title abstract 2
- 230000015572 biosynthetic process Effects 0.000 title abstract 2
- 238000009833 condensation Methods 0.000 title abstract 2
- 230000005494 condensation Effects 0.000 title abstract 2
- 239000012530 fluid Substances 0.000 title abstract 2
- 238000003786 synthesis reaction Methods 0.000 title abstract 2
- 150000004820 halides Chemical class 0.000 title 1
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 229910021578 Iron(III) chloride Inorganic materials 0.000 abstract 1
- -1 aromatic halides Chemical class 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/20—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances liquids, e.g. oils
- H01B3/22—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances liquids, e.g. oils hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
- C10M105/02—Well-defined hydrocarbons
- C10M105/06—Well-defined hydrocarbons aromatic
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
- C10M105/50—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing halogen
- C10M105/52—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing halogen containing carbon, hydrogen and halogen only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/06—Well-defined aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/02—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only
- C10M2211/024—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only aromatic
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/06—Perfluorinated compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/14—Electric or magnetic purposes
- C10N2040/16—Dielectric; Insulating oil or insulators
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/14—Electric or magnetic purposes
- C10N2040/17—Electric or magnetic purposes for electric contacts
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Insulating Materials (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Inorganic Insulating Materials (AREA)
- Lubricants (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Compounds Of Iron (AREA)
Abstract
PRECIS DE LA DIVULGATION:
La présente invention concerne une simplification des procédés de synthèse de fluides diélectriques par condensation d'halogénures aromatiques et de composés aromatiques en présence de chlorure ferrique. La demanderesse à découvert qu'il n'est plus nécessaire de neutraliser le catalyseur ni d'effectuer des lavages avec des solutions aqueuses. On évite ainsi de générer des solutions aqueuses contaminées par des produits organiques et qu'il est difficile et coûteux de traiter avant leur rejet. Le procédé consiste donc dans les étapes successives suivantes: condensation d'halogénures aromatiques et de composés aromatiques en présence de chlorure ferrique, comme catalyseur, puis distillation éventuelle de l'excédent des réactifs. Cette dernière est suivie de la distillation de l'ensemble des produits de condensation ou d'au moins l'un d'entre eux suivie de son conditionnement en fluide diélectrique.
La présente invention concerne une simplification des procédés de synthèse de fluides diélectriques par condensation d'halogénures aromatiques et de composés aromatiques en présence de chlorure ferrique. La demanderesse à découvert qu'il n'est plus nécessaire de neutraliser le catalyseur ni d'effectuer des lavages avec des solutions aqueuses. On évite ainsi de générer des solutions aqueuses contaminées par des produits organiques et qu'il est difficile et coûteux de traiter avant leur rejet. Le procédé consiste donc dans les étapes successives suivantes: condensation d'halogénures aromatiques et de composés aromatiques en présence de chlorure ferrique, comme catalyseur, puis distillation éventuelle de l'excédent des réactifs. Cette dernière est suivie de la distillation de l'ensemble des produits de condensation ou d'au moins l'un d'entre eux suivie de son conditionnement en fluide diélectrique.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8913451A FR2653134B1 (fr) | 1989-10-13 | 1989-10-13 | Procede de synthese de fluides dielectriques. |
| FR8913451 | 1989-10-13 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2027445A1 true CA2027445A1 (fr) | 1991-04-14 |
| CA2027445C CA2027445C (fr) | 1994-03-22 |
Family
ID=9386400
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002027445A Expired - Fee Related CA2027445C (fr) | 1989-10-13 | 1990-10-12 | Fluides dielectriques par condensation de composes aromatiques dont certains halogenes |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US5186864A (fr) |
| EP (1) | EP0422986B1 (fr) |
| JP (1) | JP2569214B2 (fr) |
| KR (1) | KR930005531B1 (fr) |
| CN (1) | CN1029005C (fr) |
| AT (1) | ATE80176T1 (fr) |
| CA (1) | CA2027445C (fr) |
| DE (1) | DE69000288T2 (fr) |
| DK (1) | DK0422986T3 (fr) |
| ES (1) | ES2034844T3 (fr) |
| FI (1) | FI97478C (fr) |
| FR (1) | FR2653134B1 (fr) |
| GR (1) | GR3006387T3 (fr) |
| IE (1) | IE64608B1 (fr) |
| NO (1) | NO904393L (fr) |
| PT (1) | PT95588B (fr) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5977422A (en) * | 1997-06-09 | 1999-11-02 | The Dow Chemical Company | Organoaluminum catalysis of alkylation reactions |
| US20060100466A1 (en) * | 2004-11-08 | 2006-05-11 | Holmes Steven A | Cycloalkane base oils, cycloalkane-base dielectric liquids made using cycloalkane base oils, and methods of making same |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2012302A (en) * | 1933-04-04 | 1935-08-27 | Gen Electric | Halogenated material and process of preparing the same |
| US2556880A (en) * | 1945-08-17 | 1951-06-12 | Solar Mfg Corp | Synthetic oils and resins and methods of producing same |
| BE533352A (fr) * | 1953-11-17 | 1954-12-15 | ||
| US3006972A (en) * | 1959-08-21 | 1961-10-31 | Standard Oil Co | Coupling of aromatic rings |
| US4197417A (en) * | 1977-09-28 | 1980-04-08 | Imperial Chemical Industries Limited | Process for the manufacture of o-benzyl toluenes |
| DE2962136D1 (en) * | 1978-07-27 | 1982-03-25 | Ugine Kuhlmann | Dielectric liquids, manufacturing process and uses |
| IT1138101B (it) * | 1981-07-24 | 1986-09-17 | Caffaro Ind Chimica Ed Elettro | Fluido dielettrico per trasformatori e procedimento per la sua preparazione |
| FR2552423B1 (fr) * | 1983-09-23 | 1985-10-25 | Ugine Kuhlmann | Compositions d'oligomeres de polyarylalcanes et leur procede de fabrication |
| DE3836780A1 (de) * | 1988-10-28 | 1990-05-03 | Bayer Ag | Verfahren zur herstellung von gegebenenfalls substituierten benzylbenzolen |
-
1989
- 1989-10-13 FR FR8913451A patent/FR2653134B1/fr not_active Expired - Lifetime
-
1990
- 1990-10-02 DE DE9090402722T patent/DE69000288T2/de not_active Expired - Fee Related
- 1990-10-02 DK DK90402722.4T patent/DK0422986T3/da active
- 1990-10-02 EP EP90402722A patent/EP0422986B1/fr not_active Expired - Lifetime
- 1990-10-02 ES ES199090402722T patent/ES2034844T3/es not_active Expired - Lifetime
- 1990-10-02 AT AT90402722T patent/ATE80176T1/de active
- 1990-10-11 NO NO90904393A patent/NO904393L/no unknown
- 1990-10-12 CA CA002027445A patent/CA2027445C/fr not_active Expired - Fee Related
- 1990-10-12 PT PT95588A patent/PT95588B/pt not_active IP Right Cessation
- 1990-10-12 FI FI905033A patent/FI97478C/fi not_active IP Right Cessation
- 1990-10-12 KR KR1019900016202A patent/KR930005531B1/ko not_active Expired - Fee Related
- 1990-10-12 JP JP2275155A patent/JP2569214B2/ja not_active Expired - Lifetime
- 1990-10-13 CN CN90108455A patent/CN1029005C/zh not_active Expired - Fee Related
- 1990-10-15 US US07/597,030 patent/US5186864A/en not_active Expired - Fee Related
- 1990-10-15 IE IE369290A patent/IE64608B1/en not_active IP Right Cessation
-
1992
- 1992-11-30 GR GR920402760T patent/GR3006387T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NO904393D0 (no) | 1990-10-11 |
| CN1050894A (zh) | 1991-04-24 |
| CA2027445C (fr) | 1994-03-22 |
| FI905033A0 (fi) | 1990-10-12 |
| PT95588B (pt) | 1997-08-29 |
| KR930005531B1 (ko) | 1993-06-22 |
| GR3006387T3 (fr) | 1993-06-21 |
| PT95588A (pt) | 1991-09-13 |
| IE64608B1 (en) | 1995-08-23 |
| EP0422986A1 (fr) | 1991-04-17 |
| KR910008113A (ko) | 1991-05-30 |
| ATE80176T1 (de) | 1992-09-15 |
| US5186864A (en) | 1993-02-16 |
| FI97478C (fi) | 1996-12-27 |
| DE69000288T2 (de) | 1993-03-18 |
| DE69000288D1 (de) | 1992-10-08 |
| JPH03134095A (ja) | 1991-06-07 |
| ES2034844T3 (es) | 1993-04-01 |
| IE903692A1 (en) | 1991-04-24 |
| CN1029005C (zh) | 1995-06-21 |
| FR2653134A1 (fr) | 1991-04-19 |
| DK0422986T3 (da) | 1992-10-05 |
| FR2653134B1 (fr) | 1991-12-13 |
| NO904393L (no) | 1991-04-15 |
| EP0422986B1 (fr) | 1992-09-02 |
| JP2569214B2 (ja) | 1997-01-08 |
| FI97478B (fi) | 1996-09-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |