BR0111455B1 - processo para a preparaÇço de oxima de cicloexanona. - Google Patents
processo para a preparaÇço de oxima de cicloexanona.Info
- Publication number
- BR0111455B1 BR0111455B1 BRPI0111455-7A BR0111455A BR0111455B1 BR 0111455 B1 BR0111455 B1 BR 0111455B1 BR 0111455 A BR0111455 A BR 0111455A BR 0111455 B1 BR0111455 B1 BR 0111455B1
- Authority
- BR
- Brazil
- Prior art keywords
- cyclohexanone oxime
- synthesis zone
- hydroxylammonium
- cyclohexanone
- sub
- Prior art date
Links
- VEZUQRBDRNJBJY-UHFFFAOYSA-N cyclohexanone oxime Chemical compound ON=C1CCCCC1 VEZUQRBDRNJBJY-UHFFFAOYSA-N 0.000 title abstract 16
- 238000000034 method Methods 0.000 title abstract 2
- 230000015572 biosynthetic process Effects 0.000 abstract 7
- 238000003786 synthesis reaction Methods 0.000 abstract 7
- RBLWMQWAHONKNC-UHFFFAOYSA-N hydroxyazanium Chemical compound O[NH3+] RBLWMQWAHONKNC-UHFFFAOYSA-N 0.000 abstract 5
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 4
- 239000003960 organic solvent Substances 0.000 abstract 2
- 229910002651 NO3 Inorganic materials 0.000 abstract 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract 1
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- 239000012431 aqueous reaction media Substances 0.000 abstract 1
- 238000010531 catalytic reduction reaction Methods 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1418—Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP00201965 | 2000-06-05 | ||
| PCT/NL2001/000429 WO2001094298A1 (en) | 2000-06-05 | 2001-05-31 | Process for the preparation of cyclohexanone oxime |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR0111455A BR0111455A (pt) | 2003-06-24 |
| BR0111455B1 true BR0111455B1 (pt) | 2012-07-24 |
Family
ID=8171596
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0111455-7A BR0111455B1 (pt) | 2000-06-05 | 2001-05-31 | processo para a preparaÇço de oxima de cicloexanona. |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US7005547B2 (pt) |
| EP (1) | EP1299353B1 (pt) |
| JP (1) | JP2003535842A (pt) |
| KR (1) | KR100763111B1 (pt) |
| CN (1) | CN1203052C (pt) |
| AT (1) | ATE323068T1 (pt) |
| AU (1) | AU2001264409A1 (pt) |
| BR (1) | BR0111455B1 (pt) |
| DE (1) | DE60118745T2 (pt) |
| MX (1) | MXPA02011960A (pt) |
| MY (1) | MY136944A (pt) |
| TW (1) | TW593232B (pt) |
| WO (1) | WO2001094298A1 (pt) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4090885B2 (ja) | 2001-01-31 | 2008-05-28 | 旭化成ケミカルズ株式会社 | シクロヘキサノンオキシムの製造方法 |
| EP1318141A1 (en) * | 2001-12-04 | 2003-06-11 | Dsm Nv | Process for treating an aqueous medium containing phosphate, cyclohexanone and cyclohexanone oxime |
| ATE353871T1 (de) | 2001-12-04 | 2007-03-15 | Dsm Ip Assets Bv | Verfahren zur behandlung eines cyclohexanonoxim und cyclohexanon enthaltenden wässrigen mediums |
| EP1428792A1 (en) * | 2002-12-11 | 2004-06-16 | DSM IP Assets B.V. | Process for mixing an acidic aqueous solution comprising hydroxyl ammonium and phosphate with nitric acid |
| DE602004009173T2 (de) * | 2003-05-23 | 2008-06-26 | Dsm Ip Assets B.V. | Verfahren zur herstellung von caprolactam durch mischen von cyclohexanonoxim mit einer reaktionsmischung unter turbulenten strömungsbedingungen |
| BRPI0613171A2 (pt) * | 2005-07-08 | 2010-12-21 | Dsm Ip Assets Bv | processo e equipamento para a produção contìnua de hidroxilamÈnio |
| ITMI20060279A1 (it) * | 2006-02-15 | 2007-08-16 | Aser S R L | Procedimento per deacidificare oli e-o grassi |
| TW200829544A (en) * | 2007-01-05 | 2008-07-16 | China Petrochemical Dev Corp | Method for preparing cyclohexanone oxime |
| CN103420869B (zh) * | 2012-05-23 | 2015-11-25 | 中国石油化工股份有限公司 | 一种环己烷氨氧化的方法 |
| CN103896803A (zh) * | 2012-12-28 | 2014-07-02 | 帝斯曼知识产权资产管理有限公司 | 蒸汽汽提hpo*萃取区流出的无机工艺液体以及冷凝热的利用 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL6513426A (pt) | 1965-10-16 | 1967-04-17 | ||
| US3862230A (en) * | 1969-09-20 | 1975-01-21 | Stamicarbon | Continuous preparation of cyclohexanone oxime |
| NL141502B (nl) * | 1969-09-20 | 1974-03-15 | Stamicarbon | Continue bereiding van cyclohexanonoxim. |
| BE759915A (fr) * | 1969-12-06 | 1971-06-04 | Stamicarbon | Procede de recyclage pour la preparation et le traitement d'unesolutionde sel d'hydroxylammonium |
| BE759914A (fr) * | 1969-12-06 | 1971-06-04 | Stamicarbon | Procede de recyclage pour la preparation et la traitement d'unesolutionde sel d'hydroxylammonium |
| US3997607A (en) | 1974-04-26 | 1976-12-14 | Stamicarbon B.V. | Recycling process for the preparation of cyclohexanone oxime |
| NL7907395A (nl) * | 1979-10-05 | 1981-04-07 | Stamicarbon | Kringloopproces voor de bereiding en verwerking van een hydroxylammoniumzoutoplossing. |
| US4994613A (en) * | 1983-02-16 | 1991-02-19 | Hoechst Celanese Corporation | Process for preparing 4-hydroxyacetophenone oxime with mother liquor recycle |
-
2001
- 2001-05-31 CN CNB018137547A patent/CN1203052C/zh not_active Expired - Lifetime
- 2001-05-31 EP EP01938833A patent/EP1299353B1/en not_active Expired - Lifetime
- 2001-05-31 DE DE60118745T patent/DE60118745T2/de not_active Expired - Fee Related
- 2001-05-31 AT AT01938833T patent/ATE323068T1/de not_active IP Right Cessation
- 2001-05-31 KR KR1020027016548A patent/KR100763111B1/ko not_active Expired - Lifetime
- 2001-05-31 US US10/297,308 patent/US7005547B2/en not_active Expired - Fee Related
- 2001-05-31 JP JP2002501815A patent/JP2003535842A/ja active Pending
- 2001-05-31 AU AU2001264409A patent/AU2001264409A1/en not_active Abandoned
- 2001-05-31 WO PCT/NL2001/000429 patent/WO2001094298A1/en not_active Ceased
- 2001-05-31 MX MXPA02011960A patent/MXPA02011960A/es unknown
- 2001-05-31 BR BRPI0111455-7A patent/BR0111455B1/pt not_active IP Right Cessation
- 2001-06-05 MY MYPI20012629A patent/MY136944A/en unknown
- 2001-06-26 TW TW090115424A patent/TW593232B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| WO2001094298A1 (en) | 2001-12-13 |
| MXPA02011960A (es) | 2003-07-14 |
| ATE323068T1 (de) | 2006-04-15 |
| EP1299353A1 (en) | 2003-04-09 |
| BR0111455A (pt) | 2003-06-24 |
| US20040116745A1 (en) | 2004-06-17 |
| AU2001264409A1 (en) | 2001-12-17 |
| KR20030007872A (ko) | 2003-01-23 |
| MY136944A (en) | 2008-11-28 |
| CN1446195A (zh) | 2003-10-01 |
| KR100763111B1 (ko) | 2007-10-04 |
| DE60118745T2 (de) | 2006-11-16 |
| US7005547B2 (en) | 2006-02-28 |
| JP2003535842A (ja) | 2003-12-02 |
| DE60118745D1 (de) | 2006-05-24 |
| TW593232B (en) | 2004-06-21 |
| EP1299353B1 (en) | 2006-04-12 |
| CN1203052C (zh) | 2005-05-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B25A | Requested transfer of rights approved |
Free format text: DSM IP ASSETS B.V. (NL) |
|
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B15V | Prolongation of time limit allowed |
Free format text: RECONHECIDO O OBSTACULO ADMINISTRATIVO E DEVOLVIDO O PRAZO DE 57 DIAS PARA MANIFESTACAO A CIENCIA DE PARECER, NOS TERMOS DO ARTIGO 221 PARAGRAFO 2O DA LPI E DA RESOLUCAO 116/04. |
|
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 24/07/2012, OBSERVADAS AS CONDICOES LEGAIS. |
|
| B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE AS 13A E 14A ANUIDADES. |
|
| B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2344 DE 08-12-2015 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |