AR068801A1 - Proceso para la produccion de un compuesto de toluidina como ingrediente activo de plaguicidas - Google Patents
Proceso para la produccion de un compuesto de toluidina como ingrediente activo de plaguicidasInfo
- Publication number
- AR068801A1 AR068801A1 ARP080103356A ARP080103356A AR068801A1 AR 068801 A1 AR068801 A1 AR 068801A1 AR P080103356 A ARP080103356 A AR P080103356A AR P080103356 A ARP080103356 A AR P080103356A AR 068801 A1 AR068801 A1 AR 068801A1
- Authority
- AR
- Argentina
- Prior art keywords
- alpha
- chloro
- toluidine
- pesticides
- production
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- -1 TOLUIDINE COMPOUND Chemical class 0.000 title 1
- 239000004480 active ingredient Substances 0.000 title 1
- 239000000575 pesticide Substances 0.000 title 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 abstract 2
- UZCGKGPEKUCDTF-UHFFFAOYSA-N fluazinam Chemical compound [O-][N+](=O)C1=CC(C(F)(F)F)=C(Cl)C([N+]([O-])=O)=C1NC1=NC=C(C(F)(F)F)C=C1Cl UZCGKGPEKUCDTF-UHFFFAOYSA-N 0.000 abstract 2
- 150000004679 hydroxides Chemical class 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- DPQYRXNRGNLPFC-UHFFFAOYSA-N 2,4-dichloro-1,3-dinitro-5-(trifluoromethyl)benzene Chemical compound [O-][N+](=O)C1=CC(C(F)(F)F)=C(Cl)C([N+]([O-])=O)=C1Cl DPQYRXNRGNLPFC-UHFFFAOYSA-N 0.000 abstract 1
- WXNPZQIRDCDLJD-UHFFFAOYSA-N 3-chloro-5-(trifluoromethyl)pyridin-2-amine Chemical compound NC1=NC=C(C(F)(F)F)C=C1Cl WXNPZQIRDCDLJD-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 1
- 150000001342 alkaline earth metals Chemical class 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 239000007810 chemical reaction solvent Substances 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 150000002170 ethers Chemical class 0.000 abstract 1
- 150000002576 ketones Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 238000006386 neutralization reaction Methods 0.000 abstract 1
- 150000002825 nitriles Chemical class 0.000 abstract 1
- 230000020477 pH reduction Effects 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/72—Nitrogen atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/72—Nitrogen atoms
- C07D213/74—Amino or imino radicals substituted by hydrocarbon or substituted hydrocarbon radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pyridine Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Plural Heterocyclic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
Abstract
Reivindicacion 1: Un proceso para producir 3-cloro-N-(3-cloro-5-trifluorometil-2-piridil)-alfa,alfa,alfa-trifluoro-2,6-dinitro-p-toluidina, el cual comprende (i) una etapa de hacer reaccionar 2-amino-3-cloro-5-trifluorometilpiridina y 2,4-dicloro-3,5-dinitrobenzotrifluoruro en presencia de un componente alcalino seleccionado del grupo integrado por hidroxidos y carbonatos de metales alcalinos e hidroxidos y carbonatos de metales alcalinotérreos como sustancia básica, un solvente seleccionado del grupo integrado por cetonas, nitrilos, éteres y ésteres y una cantidad suficiente de agua para disolver sustancialmente el componente alcalino, (ii) una etapa de neutralizacion o acidificacion de la mezcla de reaccion con un ácido y (iii) una etapa de remocion del solvente de una mezcla que contiene 3-cloro-N-(3-cloro-5-trifluorometil-2-piridil)-alfa,alfa,alfa-trifluoro-2,6-dinitro-p-toluidina como el producto de reaccion y el solvente de la reaccion mediante destilacion para precipitar cristales del producto.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2007202210 | 2007-08-02 | ||
| JP2007202220 | 2007-08-02 | ||
| JP2007266000 | 2007-10-12 | ||
| JP2008037841 | 2008-02-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR068801A1 true AR068801A1 (es) | 2009-12-09 |
Family
ID=40120103
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP080103356A AR068801A1 (es) | 2007-08-02 | 2008-08-01 | Proceso para la produccion de un compuesto de toluidina como ingrediente activo de plaguicidas |
Country Status (25)
| Country | Link |
|---|---|
| US (1) | US8338612B2 (es) |
| EP (1) | EP2170829B1 (es) |
| JP (1) | JP5390800B2 (es) |
| KR (1) | KR101461259B1 (es) |
| CN (1) | CN101778824B (es) |
| AR (1) | AR068801A1 (es) |
| AU (1) | AU2008283242B2 (es) |
| BR (1) | BRPI0814887B1 (es) |
| CA (1) | CA2694939C (es) |
| CL (1) | CL2008002275A1 (es) |
| DK (1) | DK2170829T3 (es) |
| ES (1) | ES2503541T3 (es) |
| GE (1) | GEP20135742B (es) |
| HR (1) | HRP20140960T1 (es) |
| IL (1) | IL203608A (es) |
| MX (1) | MX2010001191A (es) |
| NZ (1) | NZ582589A (es) |
| PL (1) | PL2170829T3 (es) |
| PT (1) | PT2170829E (es) |
| RS (1) | RS53735B1 (es) |
| RU (1) | RU2470919C2 (es) |
| SI (1) | SI2170829T1 (es) |
| TW (1) | TWI417285B (es) |
| WO (1) | WO2009017241A2 (es) |
| ZA (1) | ZA201000670B (es) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1954271A4 (en) | 2005-11-23 | 2010-09-01 | Makhteshim Chem Works Ltd | PROCESS FOR THE PREPARATION OF PYRIDINAMINES AND NEW POLYMORPHET THEREOF |
| ITBS20100012A1 (it) * | 2010-01-28 | 2011-07-29 | Finchimica Srl | Procedimento per la preparazione di fluazinam |
| CN103626695B (zh) * | 2013-12-04 | 2015-04-22 | 泰州百力化学股份有限公司 | 一种以混合溶剂为介质制备氟啶胺的新方法 |
| CN106316937A (zh) * | 2015-06-29 | 2017-01-11 | 江苏威耳化工有限公司 | 一种氟啶胺的制备方法 |
| CN109988103A (zh) * | 2017-12-29 | 2019-07-09 | 江苏扬农化工股份有限公司 | 一种合成氟啶胺的方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6052146B2 (ja) * | 1979-12-25 | 1985-11-18 | 石原産業株式会社 | Ｎ−ピリジルアニリン系化合物、それらの製造方法及びそれらを含有する有害生物防除剤 |
| JPS57126475A (en) * | 1981-01-28 | 1982-08-06 | Ishihara Sangyo Kaisha Ltd | N-pyridylaniline and pest controller containing the same |
| JPS60123471A (ja) * | 1983-12-07 | 1985-07-02 | Ishihara Sangyo Kaisha Ltd | Ν−（３−クロロ−５−トリフルオロメチル−２−ピリジル）−３−クロロ−２，６−ジニトロ−４−トリフルオロメチルアニリンの製造方法 |
| DE3905238A1 (de) * | 1989-02-21 | 1990-08-23 | Basf Ag | 2-anilino-cyanopyridine und diese enthaltende fungizide |
| EP1954271A4 (en) * | 2005-11-23 | 2010-09-01 | Makhteshim Chem Works Ltd | PROCESS FOR THE PREPARATION OF PYRIDINAMINES AND NEW POLYMORPHET THEREOF |
-
2008
- 2008-07-08 JP JP2008178336A patent/JP5390800B2/ja active Active
- 2008-07-22 TW TW097127805A patent/TWI417285B/zh active
- 2008-07-29 ES ES08792139.1T patent/ES2503541T3/es active Active
- 2008-07-29 PT PT87921391T patent/PT2170829E/pt unknown
- 2008-07-29 GE GEAP200811705A patent/GEP20135742B/en unknown
- 2008-07-29 HR HRP20140960AT patent/HRP20140960T1/hr unknown
- 2008-07-29 PL PL08792139T patent/PL2170829T3/pl unknown
- 2008-07-29 CN CN2008801016245A patent/CN101778824B/zh active Active
- 2008-07-29 RU RU2010107469/04A patent/RU2470919C2/ru active
- 2008-07-29 MX MX2010001191A patent/MX2010001191A/es active IP Right Grant
- 2008-07-29 AU AU2008283242A patent/AU2008283242B2/en active Active
- 2008-07-29 KR KR1020107002325A patent/KR101461259B1/ko active Active
- 2008-07-29 CA CA2694939A patent/CA2694939C/en active Active
- 2008-07-29 SI SI200831323T patent/SI2170829T1/sl unknown
- 2008-07-29 EP EP08792139.1A patent/EP2170829B1/en active Active
- 2008-07-29 RS RS20140647A patent/RS53735B1/sr unknown
- 2008-07-29 BR BRPI0814887A patent/BRPI0814887B1/pt active IP Right Grant
- 2008-07-29 WO PCT/JP2008/063933 patent/WO2009017241A2/en not_active Ceased
- 2008-07-29 NZ NZ582589A patent/NZ582589A/en unknown
- 2008-07-29 DK DK08792139.1T patent/DK2170829T3/en active
- 2008-07-29 US US12/671,050 patent/US8338612B2/en active Active
- 2008-08-01 CL CL2008002275A patent/CL2008002275A1/es unknown
- 2008-08-01 AR ARP080103356A patent/AR068801A1/es active IP Right Grant
-
2010
- 2010-01-28 ZA ZA2010/00670A patent/ZA201000670B/en unknown
- 2010-01-31 IL IL203608A patent/IL203608A/en active IP Right Grant
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant, registration |