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NZ603659A - Production of alcohol esters and in situ product removal during alcohol fermentation - Google Patents

Production of alcohol esters and in situ product removal during alcohol fermentation

Info

Publication number
NZ603659A
NZ603659A NZ603659A NZ60365911A NZ603659A NZ 603659 A NZ603659 A NZ 603659A NZ 603659 A NZ603659 A NZ 603659A NZ 60365911 A NZ60365911 A NZ 60365911A NZ 603659 A NZ603659 A NZ 603659A
Authority
NZ
New Zealand
Prior art keywords
butanol
carboxylic acid
feedstock
esters
aqueous stream
Prior art date
Application number
NZ603659A
Inventor
Bruce A Diner
Douglas Robert Anton
Robert Dicosimo
Jelena Cirakovic
Keith H Burlew
Brian Michael Roesch
Stephane Francois Bazzana
Michael Charles Grady
Francis J Woerner
Original Assignee
Butamax Tm Advanced Biofuels
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US13/160,766 external-priority patent/US9012190B2/en
Application filed by Butamax Tm Advanced Biofuels filed Critical Butamax Tm Advanced Biofuels
Publication of NZ603659A publication Critical patent/NZ603659A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N1/00—Microorganisms, e.g. protozoa; Compositions thereof; Processes of propagating, maintaining or preserving microorganisms or compositions thereof; Processes of preparing or isolating a composition containing a microorganism; Culture media therefor
    • C12N1/38—Chemical stimulation of growth or activity by addition of chemical compounds which are not essential growth factors; Stimulation of growth by removal of a chemical compound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N9/00—Enzymes; Proenzymes; Compositions thereof; Processes for preparing, activating, inhibiting, separating or purifying enzymes
    • C12N9/88—Lyases (4.)
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/06—Ethanol, i.e. non-beverage
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/16—Butanols
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12Y—ENZYMES
    • C12Y301/00—Hydrolases acting on ester bonds (3.1)
    • C12Y301/01—Carboxylic ester hydrolases (3.1.1)
    • C12Y301/01003—Triacylglycerol lipase (3.1.1.3)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D21/00—Separation of suspended solid particles from liquids by sedimentation
    • B01D21/26—Separation of sediment aided by centrifugal force or centripetal force
    • B01D21/262—Separation of sediment aided by centrifugal force or centripetal force by using a centrifuge
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Genetics & Genomics (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biomedical Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Molecular Biology (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • Virology (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Micro-Organisms Or Cultivation Processes Thereof (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Fodder In General (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Fats And Perfumes (AREA)

Abstract

The disclosure relates to a method for producing butanol and butyl esters from a feedstock comprising: (a) providing a feedstock; (b) liquefying the feedstock to create a liquefied biomass comprising oligosaccharides; (c) separating the feedstock slurry to produce a product comprising an aqueous stream comprising oligosaccharides, an oil stream, and solids; (d) adding the aqueous stream to a fermentation vessel containing a fermentation broth; (e) saccharifying the oligosaccharides of the aqueous stream; (f) fermenting the products of the oligosaccharide saccharification present in the aqueous stream to produce butanol and concurrently contacting the butanol with at least one carboxylic acid and at least one catalyst capable of esterifying the carboxylic acid with the butanol to form butyl esters of the carboxylic acid wherein the carboxylic acid is present at a concentration sufficient to produce a two-phase mixture, wherein the catalyst is an enzyme selected from an esterase, lipase, phospholipase, or lysophospholipase; (g) separating the butyl ester-containing organic phase from the aqueous phase; and (h) recovering butanol from the butyl esters, wherein recovering butanol from the butyl esters comprises hydrolyzing the esters into carboxylic acid and butanol in the presence of a hydrolysis catalyst selected from the enzymes: esterase, lipase, phospholipase, or lysophospholipase; and optionally steps (e) and (f) occur concurrently.
NZ603659A 2010-06-18 2011-06-17 Production of alcohol esters and in situ product removal during alcohol fermentation NZ603659A (en)

Applications Claiming Priority (9)

Application Number Priority Date Filing Date Title
US35629010P 2010-06-18 2010-06-18
US36843610P 2010-07-28 2010-07-28
US36844410P 2010-07-28 2010-07-28
US36845110P 2010-07-28 2010-07-28
US36842910P 2010-07-28 2010-07-28
US37954610P 2010-09-02 2010-09-02
US201161440034P 2011-02-07 2011-02-07
US13/160,766 US9012190B2 (en) 2011-06-15 2011-06-15 Use of thiamine and nicotine adenine dinucleotide for butanol production
PCT/US2011/040856 WO2011159998A2 (en) 2010-06-18 2011-06-17 Production of alcohol esters and in situ product removal during alcohol fermentation

Publications (1)

Publication Number Publication Date
NZ603659A true NZ603659A (en) 2014-11-28

Family

ID=45348555

Family Applications (3)

Application Number Title Priority Date Filing Date
NZ603659A NZ603659A (en) 2010-06-18 2011-06-17 Production of alcohol esters and in situ product removal during alcohol fermentation
NZ603036A NZ603036A (en) 2010-06-18 2011-06-17 Methods and systems for removing undissolved solids prior to extractive fermentation in the production of butanol
NZ603467A NZ603467A (en) 2010-06-18 2011-06-17 Supplementation of fatty acids for improving alcohol productivity

Family Applications After (2)

Application Number Title Priority Date Filing Date
NZ603036A NZ603036A (en) 2010-06-18 2011-06-17 Methods and systems for removing undissolved solids prior to extractive fermentation in the production of butanol
NZ603467A NZ603467A (en) 2010-06-18 2011-06-17 Supplementation of fatty acids for improving alcohol productivity

Country Status (14)

Country Link
EP (4) EP2582826A2 (en)
JP (4) JP2013535956A (en)
KR (4) KR20130087014A (en)
CN (4) CN102947456A (en)
AR (1) AR083153A1 (en)
AU (4) AU2011268169A1 (en)
BR (3) BR112012032352A2 (en)
CA (4) CA2800719A1 (en)
MX (4) MX2012014687A (en)
NZ (3) NZ603659A (en)
PH (1) PH12012502488A1 (en)
RU (1) RU2013102308A (en)
WO (4) WO2011159991A1 (en)
ZA (3) ZA201208372B (en)

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Also Published As

Publication number Publication date
AU2011268169A1 (en) 2012-12-06
CN102947457B (en) 2016-12-21
AU2011268244A1 (en) 2012-12-06
EP2582825A1 (en) 2013-04-24
AU2011268169A2 (en) 2012-12-06
CN103476936A (en) 2013-12-25
MX2012014784A (en) 2013-03-22
NZ603467A (en) 2014-08-29
BR112012032357A2 (en) 2015-11-24
KR20130032897A (en) 2013-04-02
WO2011159962A1 (en) 2011-12-22
AU2011268201A1 (en) 2012-11-08
CA2801209A1 (en) 2011-12-22
ZA201208677B (en) 2014-03-26
CN102947457A (en) 2013-02-27
KR20130087014A (en) 2013-08-05
BR112012032352A2 (en) 2015-11-24
WO2011160030A2 (en) 2011-12-22
CN102947456A (en) 2013-02-27
ZA201208676B (en) 2014-03-26
CA2800542A1 (en) 2011-12-22
WO2011160030A3 (en) 2012-02-16
AR083153A1 (en) 2013-02-06
JP2013531992A (en) 2013-08-15
KR20130045330A (en) 2013-05-03
MX2012014687A (en) 2013-02-11
EP2582826A2 (en) 2013-04-24
NZ603036A (en) 2014-10-31
WO2011159991A1 (en) 2011-12-22
WO2011159998A2 (en) 2011-12-22
BR112012032166A2 (en) 2015-11-24
JP2013533742A (en) 2013-08-29
KR20130116858A (en) 2013-10-24
WO2011159998A3 (en) 2012-03-08
MX2012014551A (en) 2013-02-07
MX2012014683A (en) 2013-02-11
ZA201208372B (en) 2015-03-25
PH12012502488A1 (en) 2017-08-09
JP2013535956A (en) 2013-09-19
EP2582827A2 (en) 2013-04-24
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