MX2017005919A - Produccion de hidroxido de litio. - Google Patents
Produccion de hidroxido de litio.Info
- Publication number
- MX2017005919A MX2017005919A MX2017005919A MX2017005919A MX2017005919A MX 2017005919 A MX2017005919 A MX 2017005919A MX 2017005919 A MX2017005919 A MX 2017005919A MX 2017005919 A MX2017005919 A MX 2017005919A MX 2017005919 A MX2017005919 A MX 2017005919A
- Authority
- MX
- Mexico
- Prior art keywords
- lithium hydroxide
- production
- filtering
- anhydrous
- iii
- Prior art date
Links
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 title abstract 18
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- 239000013078 crystal Substances 0.000 abstract 1
- PQVSTLUFSYVLTO-UHFFFAOYSA-N ethyl n-ethoxycarbonylcarbamate Chemical compound CCOC(=O)NC(=O)OCC PQVSTLUFSYVLTO-UHFFFAOYSA-N 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- GLXDVVHUTZTUQK-UHFFFAOYSA-M lithium hydroxide monohydrate Substances [Li+].O.[OH-] GLXDVVHUTZTUQK-UHFFFAOYSA-M 0.000 abstract 1
- 229940040692 lithium hydroxide monohydrate Drugs 0.000 abstract 1
- 238000010791 quenching Methods 0.000 abstract 1
- 230000000171 quenching effect Effects 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/02—Oxides; Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/04—Halides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/04—Chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/04—Chlorides
- C01D3/06—Preparation by working up brines; seawater or spent lyes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/04—Chlorides
- C01D3/08—Preparation by working up natural or industrial salt mixtures or siliceous minerals
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/14—Purification
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/12—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic alkaline solutions
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Environmental & Geological Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Secondary Cells (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Un proceso (10) para la producción de hidróxido de litio, el proceso que comprende los pasos de: (i) Causticizar el cloruro de litio (12) con hidróxido de sodio (16) para producir un producto de hidróxido de litio; (ii) recolectar los sólidos que resultan de la causticización del paso (i) y filtrar (22) el mismo; (iii) los sólidos filtrados del paso (ii) se hacen pasar a un paso de calentamiento (32) en el cual se produce hidróxido de litio anhidro; (iv) filtrar (34) el producto de hidróxido de litio anhidro del paso (iii); y (y) extinguir el hidróxido de litio anhidro del paso (iv) con agua para producir cristales de monohidrato de hidróxido de litio.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AU2014904449A AU2014904449A0 (en) | 2014-11-05 | Production of Lithium Hydroxide | |
| PCT/AU2014/001142 WO2016070217A1 (en) | 2014-11-05 | 2014-12-17 | Production of lithium hydroxide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2017005919A true MX2017005919A (es) | 2017-08-03 |
Family
ID=55908266
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2017005919A MX2017005919A (es) | 2014-11-05 | 2014-12-17 | Produccion de hidroxido de litio. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US9988279B2 (es) |
| EP (1) | EP3215461A4 (es) |
| JP (1) | JP2018500261A (es) |
| KR (1) | KR20170088873A (es) |
| CN (1) | CN107108245A (es) |
| AR (1) | AR101079A1 (es) |
| AU (1) | AU2014410711A1 (es) |
| CA (1) | CA2966525A1 (es) |
| CL (1) | CL2017001123A1 (es) |
| MX (1) | MX2017005919A (es) |
| WO (1) | WO2016070217A1 (es) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109803924B (zh) * | 2016-10-10 | 2025-08-29 | 浦项股份有限公司 | 锂化合物的制备方法 |
| WO2018085915A1 (en) * | 2016-11-08 | 2018-05-17 | Mgx Minerals Inc. | Method for the production of lithium carbonate from salt brines |
| WO2018089932A1 (en) | 2016-11-14 | 2018-05-17 | Lilac Solutions, Inc. | Lithium extraction with coated ion exchange particles |
| CN106629787B (zh) * | 2016-12-20 | 2018-09-18 | 阿坝中晟锂业有限公司 | 一种电池级氢氧化锂的制备方法 |
| CN111182953A (zh) | 2017-08-02 | 2020-05-19 | 锂莱克解决方案公司 | 用于锂提取的离子交换系统 |
| AR112663A1 (es) | 2017-08-02 | 2019-11-27 | Lilac Solutions Inc | Extracción de litio con perlas porosas de intercambio iónico |
| US10648090B2 (en) * | 2018-02-17 | 2020-05-12 | Lilac Solutions, Inc. | Integrated system for lithium extraction and conversion |
| KR20200116526A (ko) | 2018-02-28 | 2020-10-12 | 리락 솔루션즈, 인크. | 리튬 추출을 위한 입자 트랩을 가진 이온 교환 반응기 |
| WO2019220003A1 (en) * | 2018-05-18 | 2019-11-21 | Outotec (Finland) Oy | Method for recovering lithium hydroxide |
| US11932550B2 (en) | 2018-10-01 | 2024-03-19 | Reed Advanced Materials Pty Ltd. | Processing of lithium containing brines |
| KR102164661B1 (ko) * | 2018-12-06 | 2020-10-12 | 주식회사 에코프로이노베이션 | 리튬 정광으로부터 황산나트튬 혼합 배소에 의한 수산화리튬 제조방법 |
| CN109553118B (zh) * | 2018-12-19 | 2021-03-16 | 江西赣锋锂业股份有限公司 | 一种工业生产无水氢氧化锂球的方法 |
| CN111439760A (zh) * | 2019-12-24 | 2020-07-24 | 广西天源新能源材料有限公司 | 一种微粉级单水氢氧化锂的生产工艺 |
| CN110950363A (zh) * | 2019-12-25 | 2020-04-03 | 广西天源新能源材料有限公司 | 一种应用新型联合除钙的电池级单水氢氧化锂生产工艺 |
| JP7286800B2 (ja) * | 2020-01-10 | 2023-06-05 | エルジー・ケム・リミテッド | リチウム二次電池用正極活物質の製造方法、前記製造方法により製造された正極活物質を含むリチウム二次電池用正極、およびリチウム二次電池 |
| KR20230023714A (ko) | 2020-06-09 | 2023-02-17 | 리락 솔루션즈, 인크. | 스케일런트의 존재 하에서의 리튬 추출 |
| AU2021417988A1 (en) * | 2021-01-05 | 2023-07-27 | Sociedad Quimica Y Minera De Chile S.A. | Method for the production of lithium hydroxide (lioh) directly from lithium chloride (lici), without the need for an intermediate production of lithium carbonate or similar |
| US20240174527A1 (en) * | 2021-03-22 | 2024-05-30 | Sociedad Quimica Y Minera De Chile S.A. | System for the production of lithium hydroxide (lioh) directly from lithium chloride (lici), without the need for the intermediate production of lithium carbonate or the like |
| WO2022226219A1 (en) | 2021-04-23 | 2022-10-27 | Lilac Solutions, Inc. | Ion exchange devices for lithium extraction |
| US12151211B2 (en) | 2021-07-19 | 2024-11-26 | Aqueous Resources LLC | Electro-pressure membrane method for recovery and concentration of lithium from aqueous sources |
| US11339481B1 (en) * | 2021-08-06 | 2022-05-24 | Lithium Ark Holding B.V. | Production of lithium hydroxide and lithium carbonate |
| CN114956128A (zh) * | 2022-03-08 | 2022-08-30 | 宁夏中化锂电池材料有限公司 | 一种制备电池级氢氧化锂和碳酸锂的方法和系统 |
| WO2023192192A1 (en) | 2022-03-28 | 2023-10-05 | Lilac Solutions, Inc. | Lithium extraction enhanced by an alternate phase |
| EP4504988A2 (en) | 2022-04-01 | 2025-02-12 | Lilac Solutions, Inc. | Extraction of lithium with chemical additives |
| KR102857165B1 (ko) * | 2023-03-06 | 2025-09-09 | (주)테크윈 | 수산화리튬의 제조시스템 |
| KR102648802B1 (ko) | 2023-07-25 | 2024-03-18 | 주식회사 리켐텍 | 메카노케미스트리 및 알카리프리팅 공정을 이용하여 폐 탈황분진을 리튬 제조 공정에 활용하는 방법. |
| WO2025036769A1 (en) * | 2023-08-11 | 2025-02-20 | Nobian Chemicals Bv | Process for producing lithium hydroxide monohydrate |
| KR20250094408A (ko) * | 2023-12-18 | 2025-06-25 | 포스코홀딩스 주식회사 | 양극재 수세액으로부터 리튬을 회수하는 방법 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3597340A (en) * | 1968-11-05 | 1971-08-03 | Lithium Corp | Recovery of lithium as lioh.h20 from aqueous chloride brines containing lithium chloride and sodium chloride |
| US4207297A (en) * | 1978-03-27 | 1980-06-10 | Foote Mineral Company | Process for producing high purity lithium carbonate |
| US4221775A (en) * | 1978-12-26 | 1980-09-09 | Research Dynamics, Inc. | Method of producing porous lithium oxide |
| JP3384608B2 (ja) * | 1994-03-23 | 2003-03-10 | 出光石油化学株式会社 | リチウムイオンの回収方法 |
| US6555078B1 (en) * | 1996-09-26 | 2003-04-29 | Fmc Corporation | Method of preparing lithium salts |
| JP2000256010A (ja) * | 1999-03-11 | 2000-09-19 | Idemitsu Petrochem Co Ltd | リチウムの回収方法 |
| JP2006265023A (ja) * | 2005-03-23 | 2006-10-05 | Mitsubishi Chemicals Corp | 水酸化リチウム一水塩の無水化方法 |
| KR100725589B1 (ko) * | 2006-04-19 | 2007-06-08 | 한밭대학교 산학협력단 | 리튬 폐기물로부터 고순도 수산화 리튬 제일수화물의제조방법 |
| CN100455512C (zh) * | 2007-12-28 | 2009-01-28 | 四川天齐锂业股份有限公司 | 电池级单水氢氧化锂的制备方法 |
| AU2010351550B2 (en) * | 2010-04-23 | 2014-03-20 | Terralithium Llc | A process for making lithium carbonate from lithium chloride |
| CN102701239B (zh) * | 2012-03-19 | 2014-12-03 | 江西赣锋锂业股份有限公司 | 一种从锂辉石提锂制备单水氢氧化锂的方法 |
| CN102659144B (zh) * | 2012-04-26 | 2014-02-12 | 雅安华汇锂业科技材料有限公司 | 高纯级单水氢氧化锂的制备方法 |
-
2014
- 2014-12-17 CA CA2966525A patent/CA2966525A1/en not_active Abandoned
- 2014-12-17 JP JP2017524044A patent/JP2018500261A/ja active Pending
- 2014-12-17 AU AU2014410711A patent/AU2014410711A1/en not_active Abandoned
- 2014-12-17 WO PCT/AU2014/001142 patent/WO2016070217A1/en not_active Ceased
- 2014-12-17 CN CN201480084516.7A patent/CN107108245A/zh active Pending
- 2014-12-17 MX MX2017005919A patent/MX2017005919A/es unknown
- 2014-12-17 KR KR1020177015290A patent/KR20170088873A/ko not_active Withdrawn
- 2014-12-17 US US14/427,646 patent/US9988279B2/en not_active Expired - Fee Related
- 2014-12-17 EP EP14905540.2A patent/EP3215461A4/en not_active Withdrawn
-
2015
- 2015-04-21 AR ARP150101197A patent/AR101079A1/es unknown
-
2017
- 2017-05-05 CL CL2017001123A patent/CL2017001123A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AU2014410711A1 (en) | 2017-05-25 |
| EP3215461A4 (en) | 2018-07-11 |
| CA2966525A1 (en) | 2016-05-12 |
| KR20170088873A (ko) | 2017-08-02 |
| EP3215461A1 (en) | 2017-09-13 |
| CL2017001123A1 (es) | 2017-12-01 |
| US9988279B2 (en) | 2018-06-05 |
| CN107108245A (zh) | 2017-08-29 |
| WO2016070217A1 (en) | 2016-05-12 |
| JP2018500261A (ja) | 2018-01-11 |
| AR101079A1 (es) | 2016-11-23 |
| US20170233261A1 (en) | 2017-08-17 |
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