MY163075A - Processing of lithium containing ore - Google Patents
Processing of lithium containing oreInfo
- Publication number
- MY163075A MY163075A MYPI2014000597A MYPI2014000597A MY163075A MY 163075 A MY163075 A MY 163075A MY PI2014000597 A MYPI2014000597 A MY PI2014000597A MY PI2014000597 A MYPI2014000597 A MY PI2014000597A MY 163075 A MY163075 A MY 163075A
- Authority
- MY
- Malaysia
- Prior art keywords
- spodumene
- passing
- ore
- beta
- lithium containing
- Prior art date
Links
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title abstract 2
- 229910052744 lithium Inorganic materials 0.000 title abstract 2
- CNLWCVNCHLKFHK-UHFFFAOYSA-N aluminum;lithium;dioxido(oxo)silane Chemical compound [Li+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O CNLWCVNCHLKFHK-UHFFFAOYSA-N 0.000 abstract 6
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 abstract 3
- 229910052644 β-spodumene Inorganic materials 0.000 abstract 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 2
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 239000011575 calcium Substances 0.000 abstract 1
- 229910052791 calcium Inorganic materials 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- 238000005868 electrolysis reaction Methods 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 229910052643 α-spodumene Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/14—Alkali metal compounds
- C25B1/16—Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/02—Oxides; Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/04—Halides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/08—Carbonates; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/16—Sintering; Agglomerating
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
- C22B26/10—Obtaining alkali metals
- C22B26/12—Obtaining lithium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
- C22B3/10—Hydrochloric acid, other halogenated acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B4/00—Electrothermal treatment of ores or metallurgical products for obtaining metals or alloys
- C22B4/02—Light metals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Inorganic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
A PROCESS (10) FOR THE TREATMENT OF LITHIUM CONTAINING ORE, THE PROCESS COMPRISING THE STEPS OF: (I) CALCINING AN ALPHA-SPODUMENE ORE OR ORE CONCENTRATE (12) TO PRODUCE BETASPODUMENE; (II) PASSING THE BETA-SPODUMENE OF STEP (I) TO A LEACH STEP IN WHICH THE BETA-SPODUMENE IS LEACHED WITH HYDROCHLORIC ACID TO PRODUCE A PREGNANT LEACH SOLUTION; (III) PASSING THE PREGNANT LEACH SOLUTION FROM STEP (II) TO A SERIES OF IMPURITY REMOVAL STEPS (24) IN WHICH IMPURITIES INCLUDING IRON, CALCIUM AND SODIUM ARE SUBSTANTIALLY REMOVED; AND (IV) PASSING THE PURIFIED LITHIUM CHLORIDE PRODUCT OF STEP (III) TO AN ELECTROLYSIS STEP (44) THEREBY PRODUCING A LITHIUM HYDROXIDE SOLUTION. (FIG. 1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AU2012903483A AU2012903483A0 (en) | 2012-08-13 | Processing of Lithium Containing Ore |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY163075A true MY163075A (en) | 2017-08-15 |
Family
ID=50101101
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYPI2014000597A MY163075A (en) | 2012-08-13 | 2013-08-01 | Processing of lithium containing ore |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20150152523A1 (en) |
| JP (1) | JP6275138B2 (en) |
| KR (1) | KR101857458B1 (en) |
| CN (2) | CN111519042A (en) |
| AU (1) | AU2013201833B2 (en) |
| CA (1) | CA2851786C (en) |
| CL (1) | CL2014001656A1 (en) |
| MY (1) | MY163075A (en) |
| WO (1) | WO2014026217A1 (en) |
Families Citing this family (44)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104030321B (en) * | 2014-06-30 | 2015-09-16 | 青海盐湖工业股份有限公司 | A kind ofly realize production system and the method thereof of comprehensive utilization of resources with Repone K, Sweet natural gas for raw material |
| US10450630B2 (en) * | 2014-10-10 | 2019-10-22 | Li-Technology Pty Ltd. | Recovery process |
| AR100672A1 (en) * | 2015-01-27 | 2016-10-26 | Reed Advanced Mat Pty Ltd | PROCESSING MATERIAL CONTAINING LITHIUM INCLUDING HCl INJECTION |
| CA2996651C (en) * | 2015-08-27 | 2021-06-01 | Nemaska Lithium Inc. | Method for preparing lithium hydroxide and lithium sulfate monohydrate using hydrogen depolarized anode |
| CN106906359B (en) | 2015-12-22 | 2018-12-11 | 理查德.亨威克 | Harvesting lithium from silicate minerals |
| AU2017220394B2 (en) * | 2016-02-18 | 2021-12-23 | Cornish Lithium plc | Lithium recovery from phosphate minerals |
| CN105907983A (en) * | 2016-04-20 | 2016-08-31 | 天齐锂业股份有限公司 | Method of extracting lithium from furnace slag generated from pyrogenic process recovery of lithium battery |
| CN106148730B (en) * | 2016-07-05 | 2018-05-25 | 广东道氏技术股份有限公司 | A kind of method that alkali metal is extracted from lepidolite |
| CN108070725B (en) * | 2016-11-07 | 2021-06-25 | 尤米科尔公司 | Method for recovering lithium |
| EP3538266B1 (en) | 2016-11-14 | 2024-08-21 | Lilac Solutions, Inc. | Lithium extraction with coated ion exchange particles |
| WO2018145142A1 (en) * | 2017-02-08 | 2018-08-16 | Inneovation Pty Ltd | Combined processing method incorporating electrolysis for lithium containing solutions |
| DE102017221268A1 (en) | 2017-02-28 | 2018-08-30 | Sms Group Gmbh | Process for producing lithium hydroxide from lithiated ore by means of chlorination and chloralkali process |
| DE102017221288A1 (en) * | 2017-02-28 | 2018-08-30 | Sms Group Gmbh | Process for producing lithium hydroxide from lithiated ore |
| WO2018193993A1 (en) * | 2017-04-19 | 2018-10-25 | 株式会社アルバック | Film forming apparatus and film forming method |
| EP3661619A4 (en) | 2017-08-02 | 2021-05-05 | Lilac Solutions, Inc. | Lithium extraction with porous ion exchange beads |
| EP3661620A4 (en) | 2017-08-02 | 2021-05-12 | Lilac Solutions, Inc. | ION EXCHANGE SYSTEM FOR LITHIUM EXTRACTION |
| CN108660476B (en) * | 2017-08-10 | 2019-04-02 | 青海盐湖工业股份有限公司 | A kind of new process of salt lake bittern production high-purity hydrogen lithia |
| JP7427598B2 (en) | 2018-02-28 | 2024-02-05 | ライラック ソリューションズ，インク． | Ion exchange reactor with particle trap for lithium extraction |
| CN108217700B (en) * | 2018-03-12 | 2024-01-26 | 安徽科达新能源装备有限公司 | System and method for preparing battery-grade lithium carbonate |
| EP3887315A4 (en) | 2018-11-29 | 2022-09-07 | ICSIP Pty Ltd | Production of lithium chemicals and metallic lithium |
| CN113453788A (en) * | 2019-02-20 | 2021-09-28 | 笹仓机械工程有限公司 | Lithium recovery method |
| CN109678183B (en) * | 2019-02-22 | 2021-07-27 | 北京廷润膜技术开发股份有限公司 | A method for preparing lithium hydroxide from an industrial-grade soluble lithium salt |
| KR102278372B1 (en) * | 2019-04-29 | 2021-07-19 | 고등기술연구원연구조합 | Method for recoering lithium from lithium compound |
| JP2023514803A (en) | 2020-01-09 | 2023-04-11 | ライラック ソリューションズ，インク． | Methods for separating unwanted metals |
| CN111302365A (en) * | 2020-02-13 | 2020-06-19 | 雅化锂业(雅安)有限公司 | Production process of battery-grade lithium hydroxide |
| WO2021212018A1 (en) * | 2020-04-17 | 2021-10-21 | Northstar 620 | Electrolysis process for making lithium hydroxide |
| JP2023529444A (en) | 2020-06-09 | 2023-07-10 | ライラック ソリューションズ，インク． | Lithium extraction in presence of scale material |
| WO2021252381A1 (en) * | 2020-06-09 | 2021-12-16 | Lilac Solutions, Inc. | Lithium extraction in the presence of scalants |
| CN111826531A (en) * | 2020-07-07 | 2020-10-27 | 浙江衢州明德新材料有限公司 | Method for extracting lithium from brine using powdered adsorbent |
| EP4247759A1 (en) | 2020-11-20 | 2023-09-27 | Lilac Solutions, Inc. | Lithium production with volatile acid |
| MX2023008588A (en) * | 2021-01-22 | 2023-08-09 | Extrakt Process Solutions Llc | Recovery of metal from leach processing. |
| RU2769609C2 (en) * | 2021-03-31 | 2022-04-04 | Общество с ограниченной ответственностью "Экостар-Наутех" | Method for obtaining lithium hydroxide monohydrate of high purity from materials containing lithium salts |
| AR125722A1 (en) | 2021-04-23 | 2023-08-09 | Lilac Solutions Inc | ION EXCHANGE DEVICES FOR LITHIUM EXTRACTION |
| EP4186997A1 (en) | 2021-11-26 | 2023-05-31 | K-UTEC AG Salt Technologies | Preparation of lithium hydroxide |
| CN118871390A (en) | 2022-01-17 | 2024-10-29 | Icsip私人有限公司 | Method and system for lithium production |
| CN114590829A (en) * | 2022-03-25 | 2022-06-07 | 郑州中科新兴产业技术研究院 | A kind of aluminum-containing lithium solid waste recycling method |
| WO2023192192A1 (en) | 2022-03-28 | 2023-10-05 | Lilac Solutions, Inc. | Lithium extraction enhanced by an alternate phase |
| WO2023192623A2 (en) | 2022-04-01 | 2023-10-05 | Lilac Solutions, Inc. | Extraction of lithium with chemical additives |
| WO2024043228A1 (en) * | 2022-08-22 | 2024-02-29 | 株式会社アサカ理研 | Method for producing lithium hydroxide aqueous solution |
| CN116332208A (en) * | 2023-02-28 | 2023-06-27 | 四川顺应锂材料科技有限公司 | A method for preparing battery-grade lithium hydroxide monohydrate from spodumene acid leaching solution |
| JP2024151485A (en) * | 2023-04-12 | 2024-10-25 | 株式会社アサカ理研 | Membrane electrolysis method for lithium salt aqueous solution |
| CN116425180A (en) * | 2023-05-04 | 2023-07-14 | 四川顺应锂材料科技有限公司 | Method for producing battery grade lithium carbonate by using membrane method for lithium-base hydrochloric acid method |
| KR102858342B1 (en) | 2024-12-17 | 2025-09-11 | 주식회사 티앨씨 | Facility and method for manufacturing lithium metal from lithium chloride |
| KR102858340B1 (en) | 2024-12-17 | 2025-09-11 | 주식회사 티앨씨 | Facility and method for manufacturing lithium metal using plasma from lithium carbonate |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE521159A (en) * | 1952-08-22 | 1900-01-01 | ||
| US2803518A (en) * | 1955-05-10 | 1957-08-20 | Foote Mineral Co | Method of recovering lithium values |
| US3112170A (en) * | 1961-01-16 | 1963-11-26 | Dept Of Natural Resources Of T | Sodium-ammonium compounds process for extracting lithium from spodumene |
| US4036713A (en) * | 1976-03-04 | 1977-07-19 | Foote Mineral Company | Process for the production of high purity lithium hydroxide |
| GB1576130A (en) * | 1976-08-10 | 1980-10-01 | Quebec Ministere Des Richesses | Continuous production of lithium carbonate |
| RU2157338C2 (en) * | 1998-08-24 | 2000-10-10 | Закрытое акционерное общество "Экостар-Наутех" | Method of production of high-purity lithium hydroxide from natural brines |
| US7390466B2 (en) * | 1999-07-14 | 2008-06-24 | Chemetall Foote Corporation | Production of lithium compounds directly from lithium containing brines |
| CN1559902A (en) * | 2004-02-26 | 2005-01-05 | 东北大学 | A purification method for removing impurity sodium in lithium chloride |
| RU2283283C1 (en) * | 2004-12-30 | 2006-09-10 | Закрытое акционерное общество (ЗАО) "Экостар-Наутех" | Process of producing h-purity lithium carbonate from lithium-bearing chloride brines |
| RU2330810C2 (en) * | 2006-04-03 | 2008-08-10 | Открытое акционерное общество "Новосибирский завод химконцентратов" | Method of lithium chloride purification |
| US8961649B2 (en) * | 2007-08-29 | 2015-02-24 | Vale Canada Limited | System and method for extracting base metal values from oxide ores |
| US20110044882A1 (en) * | 2008-04-22 | 2011-02-24 | David Buckley | Method of making high purity lithium hydroxide and hydrochloric acid |
| JP2009269810A (en) * | 2008-05-07 | 2009-11-19 | Kee:Kk | Method for producing high-purity lithium hydroxide |
| JP2011031232A (en) * | 2009-08-04 | 2011-02-17 | Kee:Kk | Method of manufacturing lithium hydroxide |
| CA2786317C (en) * | 2010-01-07 | 2020-07-07 | Galaxy Resources Limited | Process for the production of lithium carbonate |
| US8287829B2 (en) * | 2010-02-17 | 2012-10-16 | Simbol Mining Corp. | Processes for preparing highly pure lithium carbonate and other highly pure lithium containing compounds |
| EP3770117A1 (en) * | 2010-04-23 | 2021-01-27 | TerraLithium LLC | A process for making lithium carbonate from lithium chloride |
| CN102432046B (en) * | 2011-09-26 | 2013-02-13 | 江苏海龙锂业科技有限公司 | Utilization method of chloride type salt lake brine |
-
2013
- 2013-03-22 AU AU2013201833A patent/AU2013201833B2/en active Active
- 2013-08-01 CA CA2851786A patent/CA2851786C/en active Active
- 2013-08-01 MY MYPI2014000597A patent/MY163075A/en unknown
- 2013-08-01 CN CN202010274898.7A patent/CN111519042A/en active Pending
- 2013-08-01 JP JP2015526829A patent/JP6275138B2/en active Active
- 2013-08-01 KR KR1020157006360A patent/KR101857458B1/en active Active
- 2013-08-01 CN CN201380003136.1A patent/CN104271781A/en active Pending
- 2013-08-01 WO PCT/AU2013/000857 patent/WO2014026217A1/en not_active Ceased
- 2013-08-01 US US14/344,632 patent/US20150152523A1/en not_active Abandoned
-
2014
- 2014-06-20 CL CL2014001656A patent/CL2014001656A1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AU2013201833A1 (en) | 2014-02-27 |
| KR20150041661A (en) | 2015-04-16 |
| CL2014001656A1 (en) | 2014-10-10 |
| JP6275138B2 (en) | 2018-02-07 |
| WO2014026217A1 (en) | 2014-02-20 |
| CA2851786A1 (en) | 2014-02-20 |
| AU2013201833B2 (en) | 2014-07-17 |
| KR101857458B1 (en) | 2018-05-14 |
| CA2851786C (en) | 2016-04-12 |
| CN104271781A (en) | 2015-01-07 |
| CN111519042A (en) | 2020-08-11 |
| US20150152523A1 (en) | 2015-06-04 |
| JP2015531826A (en) | 2015-11-05 |
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