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WO2024250638A1 - Aerosol generating matrix manufacturing method and manufacturing device - Google Patents

Aerosol generating matrix manufacturing method and manufacturing device Download PDF

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Publication number
WO2024250638A1
WO2024250638A1 PCT/CN2023/140421 CN2023140421W WO2024250638A1 WO 2024250638 A1 WO2024250638 A1 WO 2024250638A1 CN 2023140421 W CN2023140421 W CN 2023140421W WO 2024250638 A1 WO2024250638 A1 WO 2024250638A1
Authority
WO
WIPO (PCT)
Prior art keywords
extruded matrix
manufacturing
matrix
extruded
negative pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
PCT/CN2023/140421
Other languages
French (fr)
Chinese (zh)
Inventor
倪军
魏明文
李文凤
廖桂民
汤建国
廖晓祥
金祖涛
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen Smoore Technology Ltd
Smoore International Holdings Ltd
Original Assignee
Shenzhen Smoore Technology Ltd
Smoore International Holdings Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shenzhen Smoore Technology Ltd, Smoore International Holdings Ltd filed Critical Shenzhen Smoore Technology Ltd
Publication of WO2024250638A1 publication Critical patent/WO2024250638A1/en
Anticipated expiration legal-status Critical
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances

Definitions

  • the present application relates to the technical field of smoking products, and in particular to a method and equipment for manufacturing an aerosol generating substrate.
  • Smoking articles include smoking articles that form aerosols by ignition and smoking articles that form aerosols by heating without burning.
  • a typical smoking article that heats without burning it contains an aerosol-generating substrate such as tobacco or other plant materials, flavor materials and/or atomizers that can volatilize when heated to produce an aerosol.
  • the aerosol-generating substrate is heated by an external heat source so that it is heated just enough to emit a fragrance.
  • the aerosol-generating substrate does not burn, but instead loads the atomizer and releases the atomizer by heating when used to form smoke.
  • Aerosol generating substrates There are three main types of aerosol generating substrates: particle type, traditional tobacco type and sheet type.
  • particle type particle type
  • traditional tobacco type traditional tobacco type
  • sheet type traditional tobacco type
  • the manufacturing method of the aerosol generating substrate is complicated, the equipment investment is high, the production efficiency is low and the environmental pollution is great.
  • the embodiments of the present application hope to provide a method and a manufacturing device for an aerosol generating substrate with high production efficiency and low cost.
  • the present application provides a method for manufacturing an aerosol generating substrate, the manufacturing method comprising:
  • the extruded matrix is dried under negative pressure in a vacuum environment.
  • the extrusion temperature of the room temperature extrusion molding is 10°C to 90°C.
  • the temperature of the vacuum environment is greater than 20°C and less than 100°C.
  • the absolute pressure of the vacuum environment is 0 kPa to 101.325 kPa.
  • the extrusion pressure of the room temperature extrusion molding is 0.5 bar to 300 bar.
  • the extrusion temperature is 35°C to 70°C.
  • the absolute pressure is 4 kPa to 20 kPa.
  • the extrusion pressure is 20 bar to 80 bar.
  • the extrusion method of the room temperature extrusion molding is one of horizontal extrusion, vertical extrusion and inclined extrusion.
  • the extruded matrix is subjected to negative pressure drying, comprising:
  • the extruded matrix is dried under negative pressure by using at least one heating method selected from microwave heating, resistance heating and infrared heating.
  • the manufacturing method further comprises: slitting the extruded matrix into set lengths.
  • the cutting the extruded matrix into the set length comprises: before the extruded matrix is subjected to the negative pressure drying, the cutting the extruded matrix into the set length.
  • the cutting of the extruded matrix into set lengths comprises: pre-cutting the extruded matrix before the negative pressure drying of the extruded matrix, and cutting the pre-cut extruded matrix into the set lengths after the negative pressure drying of the extruded matrix.
  • the slitting is performed by physical contact slitting in which a slitting tool contacts the extruded matrix.
  • the slitting is performed by non-physical contact slitting between a slitting tool and the extruded matrix.
  • the manufacturing method before the negative pressure drying of the extruded matrix, the manufacturing method further comprises: cooling and hardening the extruded matrix.
  • the cooling and hardening of the extruded matrix comprises:
  • the extruded matrix is placed in a low temperature environment for cooling, wherein the temperature of the low temperature environment is lower than the hardening temperature of the extruded matrix.
  • the hardening temperature is -100°C to 60°C
  • the temperature of the low temperature environment is -270°C to 60°C.
  • the cooling and hardening of the extruded matrix comprises: directly exchanging heat between the extruded matrix and a refrigerant.
  • the cooling and hardening of the extruded matrix comprises: indirectly exchanging heat between the extruded matrix and a refrigerant.
  • the manufacturing method further comprises: cutting the extruded matrix into set lengths.
  • the hardness of the extruded matrix after cooling and hardening is 1HB to 200HB.
  • the temperature of the extruded matrix after cooling and hardening is -50°C to 5°C.
  • the hardness of the extruded matrix after the negative pressure drying is 40HB to 300HB.
  • the water content of the extruded matrix after the negative pressure drying is 3% to 20% of the total weight of the extruded matrix.
  • the components of the mixed material include a solid material and a liquid material.
  • the manufacturing method further includes:
  • the solid material and the liquid material are divided into two modules for feeding respectively.
  • the solid material and the liquid material are divided into two modules for feeding respectively, comprising:
  • the manufacturing method further comprises: The method comprises: wrapping a packaging layer on the outer surface of the extruded matrix.
  • the manufacturing method further comprises: sealing and packaging the extruded matrix.
  • the plant raw material in 100 parts by weight of the mixed material, is 30 to 90 parts, the auxiliary raw material is 1 to 15 parts, the smoke agent raw material is 5 to 30 parts, the adhesive raw material is 1 to 10 parts, and the fragrance raw material is 1 to 15 parts.
  • the present application embodiment provides a manufacturing device for an aerosol generating substrate, comprising:
  • An extruder the extruder is used to perform room temperature extrusion molding on the mixed material so that the mixed material forms an extrusion matrix;
  • a vacuum drying device is used to perform negative pressure drying on the extruded matrix.
  • the extrusion die of the extruder is a single-die single-mouth die having a bottom die, and a mouth die at the discharge end of the bottom die.
  • the extrusion die of the extruder is a single-die multi-die having a bottom die, and a discharge end of the bottom die having a plurality of die openings.
  • the extrusion die of the extruder is a multi-opening die having a plurality of bottom dies, and the discharge end of each bottom die has a plurality of opening dies.
  • the manufacturing apparatus further comprises a hardening device and two slitting devices;
  • the hardening device is disposed between the extruder and the vacuum drying device to cool and harden the extruded matrix before the negative pressure drying;
  • One of the two slitting devices is arranged between the hardening device and the vacuum drying device, so as to pre-slit the extruded matrix that has undergone the cooling and hardening before the negative pressure drying; the other of the two slitting devices is arranged downstream of the vacuum drying device along the material conveying direction, so as to cut the extruded matrix that has undergone the negative pressure drying into set lengths.
  • the manufacturing equipment further comprises a hardening device and a slitting device
  • the hardening device is disposed between the extruder and the vacuum drying device to cool and harden the extruded matrix before the negative pressure drying;
  • the slitting device is arranged between the hardening device and the vacuum drying device to Before performing the negative pressure drying, the extruded matrix that has been cooled and hardened is cut into set lengths.
  • the embodiment of the present application provides a method and equipment for manufacturing an aerosol generating matrix, the manufacturing method mainly involves extrusion molding the mixed material at room temperature, and then negative pressure drying the extruded matrix in a vacuum environment.
  • Room temperature extrusion molding can ensure the stability of the rheological properties of the slurry, and the endogenous components of the extruded extruded matrix are stable, while negative pressure drying can ensure that the shrinkage rate of the extruded matrix is small and the drying time is short, which is convenient for realizing continuous production.
  • the combination of room temperature extrusion molding and negative pressure drying can not only realize the uniformity and stability of the aerosol generating matrix, the uniform distribution of internal pores, and the high processability of the aerosol generating matrix, but also realize the continuous production of the aerosol generating matrix, with high production efficiency and low manufacturing cost.
  • FIG1 is a schematic diagram of a method for manufacturing an aerosol generating substrate according to an embodiment of the present application
  • FIG2 is a schematic structural diagram of an aerosol generating substrate manufacturing device according to an embodiment of the present application, wherein a mixed material and an extruded substrate are shown at the same time;
  • FIG3 is a cross-sectional view of the manufacturing equipment shown in FIG2 ;
  • FIG4 is a schematic structural diagram of another aerosol-generating substrate manufacturing device according to an embodiment of the present application, in which a mixed material and an extruded substrate are shown at the same time;
  • FIG5 is a cross-sectional view of the manufacturing equipment shown in FIG4;
  • FIG6 is a schematic structural diagram of a first extrusion die of an embodiment of the present application.
  • FIG7 is a schematic diagram of the structure of a second extrusion die according to an embodiment of the present application, and also shows an extruded matrix
  • FIG8 is a schematic structural diagram of a third extrusion die according to an embodiment of the present application, in which an extrusion matrix and an adapter are shown at the same time;
  • FIG9 is a schematic structural diagram of a vacuum drying device according to an embodiment of the present application, and also shows an extruded matrix
  • FIG10 is a schematic structural diagram of a hardening device according to an embodiment of the present application, in which an extrusion die and an extrusion matrix are shown;
  • FIG11 is a cross-sectional view of the hardening device shown in FIG10 ;
  • FIG12 is a schematic structural diagram of another hardening device according to an embodiment of the present application, which also shows an extruded matrix
  • FIG13 is a cross-sectional view of a first extruded matrix according to an embodiment of the present application.
  • FIG14 is a schematic diagram of the structure of a second extruded matrix according to an embodiment of the present application.
  • FIG15 is a schematic diagram of the structure of a third extruded matrix according to an embodiment of the present application.
  • FIG16 is a flow chart of a first manufacturing method according to an embodiment of the present application.
  • FIG17 is a flow chart of a second manufacturing method according to an embodiment of the present application.
  • FIG18 is a flow chart of a third manufacturing method according to an embodiment of the present application.
  • FIG. 19 is a flow chart of a fourth manufacturing method according to an embodiment of the present application.
  • An embodiment of the present application provides a method for manufacturing an aerosol-generating substrate.
  • the aerosol-generating substrate is used in conjunction with an electronic atomization device having a heating component.
  • the heating component heats and atomizes the aerosol-generating substrate to generate an aerosol for users to inhale or for use in medicine, beauty, etc.
  • the method for manufacturing the aerosol generating substrate comprises the following steps:
  • Step S10 Extruding the mixed material at room temperature to form an extrusion matrix
  • extrusion molding refers to a processing method in which the material is added to the extruder, and the material is pushed forward by the screw through the action between the barrel and the screw of the extruder, and continuously passes through the extrusion die at the outlet of the extruder to form various cross-section products or semi-finished products.
  • the material formed by extrusion molding is in the form of strips.
  • the mixed material is a material used to manufacture an aerosol-generating matrix.
  • the mixed material is a mixture of a solid material and a liquid material, that is, the mixed material contains a certain amount of water.
  • the extrusion temperature i.e. the temperature inside the barrel of the extruder
  • the extrusion temperature below 10°C is defined as low temperature
  • the extrusion temperature above 90°C is defined as high temperature
  • the room-temperature extrusion molding of the mixed material described in the implementation of the present application may refer to extrusion molding of the mixed material within an extrusion temperature range of 10° C. to 90° C.
  • Temperature affects the fluidity of the mixed material in the extruder and the smoothness of the outer surface of the extruded matrix.
  • the extrusion temperature is lower than 10°C, the fluidity of the mixed material is poor, the production speed of the extruder is slow, the efficiency is low, and the torque provided by the extruder at this temperature is high, which affects the service life of the extruder.
  • the extrusion temperature is higher than 90°C, the mixed material flows fast and the pressure of the mixed material at the extruder outlet is relatively low, which is not conducive to the molding of the mixed material. As a result, the yield rate will decrease. In addition, at this temperature, the energy consumption of the extruder is high and the production cost increases.
  • the mixed material When the extrusion temperature is 10°C to 90°C, the mixed material has good fluidity, which is conducive to the molding of the mixed material, can ensure the stability of the rheological properties of the mixed material, and the endogenous components of the extruded extrusion matrix are stable. In addition, at this temperature, the torque provided by the extruder is low, the energy consumption of the extruder is low, and the service life of the extruder is increased while reducing the production cost.
  • the extrusion temperature of room temperature extrusion molding can be 35° C. to 70° C. (including 35° C. and 70° C.).
  • Step S20 performing negative pressure drying on the extruded matrix in a vacuum environment.
  • negative pressure drying The main purpose of negative pressure drying is to evaporate the water in the extruded matrix. If the extruded matrix contains a large amount of volatile lubricant, negative pressure drying can also remove the volatile lubricant.
  • step S20 may be the last step of the manufacturing method, that is, the dried extruded matrix is the finished product of the aerosol generating matrix.
  • Step S20 may not be the last step of the manufacturing method, which is equivalent to the dried extruded matrix being only a semi-finished product of the aerosol generating matrix.
  • step S20 other processing may be performed, including but not limited to slitting, packaging, etc.
  • the vacuum environment can reduce the boiling point of water (i.e., the boiling point of water is lower than the boiling point of 100°C under normal pressure), so that the water in the extruded matrix can evaporate at low temperature (i.e., water evaporates below 100°C).
  • negative pressure drying can slow down the overflow of water from the extruded matrix, so that the extruded matrix can maintain the reserved skeleton after the water overflows, thereby forming pores.
  • the pores are the channels for the aerosol-generating matrix to release aerosols and aromas during the heating process. Therefore, negative pressure drying can increase the porosity of the aerosol-generating matrix, and thus improve the release efficiency of aerosols and aromas.
  • the temperature of the vacuum environment may be greater than 20°C and less than 100°C.
  • the temperature of the vacuum environment refers to the ambient temperature within the device that provides the vacuum environment.
  • the temperature of the vacuum environment When the temperature of the vacuum environment is lower than or equal to 20°C, it takes a long time to dry the extruded matrix, the production efficiency is low, and the production cost is high.
  • the temperature of the vacuum environment is higher than or equal to 100°C, the extruded matrix Thermosensitive aroma components are easily volatilized by heat.
  • the temperature when the temperature is higher than or equal to 100°C, the extruded matrix reaches its softening point, and the support of the outer wall of the extruded matrix decreases. Under the influence of vacuum negative pressure, the overall structure is prone to shrinkage, which causes the pores on the skeleton to shrink and deform after the water inside the extruded matrix overflows, and the porosity decreases. As a result, the channel for the aerosol-generating matrix to release aerosols and aromas is blocked, affecting the overall release efficiency.
  • the temperature of the vacuum environment may be 30° C. to 60° C. (inclusive).
  • the hardness of the extruded matrix after negative pressure drying may be 40HB to 300HB (including 40HB and 300HB). More preferably, the hardness of the extruded matrix after negative pressure drying may be 80HB to 250HB (including 80HB and 250HB).
  • the manufacturing device 100 mainly includes an extruder 110 and a vacuum drying device 120 .
  • the extruder 110 is used to perform room temperature extrusion molding on the mixed material 200 ′ so that the mixed material 200 ′ forms an extruded matrix 200 .
  • the extruder 110 can be a single-screw extruder or a twin-screw extruder.
  • a twin-screw extruder is preferably used because, compared with a single-screw extruder, a twin-screw extruder can further homogenize the mixed material 200′ during the conveying process of the mixed material 200′, thereby improving product stability, and the extrusion efficiency of a twin-screw extruder is higher than that of a single-screw extruder.
  • the vacuum drying device 120 is used to dry the extruded matrix 200 under negative pressure.
  • the ambient temperature in the vacuum drying device 120 is the temperature of the vacuum environment mentioned above.
  • the vacuum drying device 120 may include a housing 121, a vacuum pump 122, a heating system (not shown) and an electrical instrument control system (not shown), wherein at least one partition 123 is provided in the housing 121, and a material tray 124 may be placed on the partition 123.
  • the material tray 124 may be taken out, the extruded matrix 200 may be placed in the material tray 124, and then the material tray 124 may be placed on the partition 123 in the housing 121.
  • the vacuum pump 122 is used to form a vacuum in the housing 121, and the partition 123 is heated by the heating system to provide heat for the extruded matrix 200.
  • the manufacturing method of the aerosol generating matrix of the embodiment of the present application mainly involves extruding the mixed material at room temperature, and then drying the extruded matrix under negative pressure in a vacuum environment. It can ensure the stability of the rheological properties of the slurry and the stability of the endogenous components of the extruded matrix, while negative pressure drying can ensure that the shrinkage of the extruded matrix is small and the drying time is short, which is convenient for continuous production.
  • the combination of room temperature extrusion molding and negative pressure drying can not only achieve uniform and stable aerosol generation matrix, uniform internal pore distribution, and high processability of aerosol generation matrix, but also realize continuous production of aerosol generation matrix with high production efficiency and low manufacturing cost.
  • the mixed materials of the embodiment of the present application may include plant raw materials, auxiliary raw materials, smoke-generating agent raw materials, adhesive raw materials and flavor raw materials.
  • Plant raw materials are used to generate aerosols when heated.
  • Auxiliary raw materials are used to provide skeleton support for plant raw materials.
  • Smoke-generating agent raw materials are used to generate smoke when heated.
  • Adhesive raw materials are used to bond various raw material components.
  • Flavor raw materials are used to provide characteristic aromas. In this way, plant raw materials and smoke-generating agent raw materials can ensure the amount of aerosol generated, while flavor raw materials can increase the release of aroma during the inhalation process and enhance user experience.
  • Auxiliary raw materials can not only improve the fluidity of the mixed materials, but also make the aerosol generation matrix porous to facilitate the extraction and flow of aerosols. Adhesive raw materials ensure that plant raw materials and auxiliary raw materials constitute a stable mixture to avoid loose structure.
  • the plant raw material can be one or more combinations of powders formed after crushing tobacco raw materials, tobacco leaf fragments, tobacco stems, tobacco dust, and flavor plants.
  • Plant raw materials are the core source of flavor. Endogenous substances in plant raw materials can produce physiological satisfaction for users. Endogenous substances such as alkaloids enter the human blood and promote the pituitary gland to produce dopamine, thereby obtaining physiological satisfaction.
  • the auxiliary raw material can be one or more combinations of inorganic fillers, lubricants, and emulsifiers.
  • the inorganic filler includes one or more combinations of heavy calcium carbonate, light calcium carbonate, zeolite, attapulgite, talc, and diatomaceous earth.
  • the inorganic filler can provide a skeleton support for the plant raw material.
  • the inorganic filler also has micropores, which can increase the porosity of the aerosol generating matrix, thereby increasing the aerosol release rate.
  • Lubricants include one or more combinations of candelilla wax, carnauba wax, shellac, sunflower wax, rice bran, beeswax, stearic acid, and palmitic acid. Lubricants can increase the fluidity of plant raw material powders, reduce the friction between plant raw material powders, make the overall density of plant raw material powder distribution more uniform, and reduce the pressure required for the extrusion molding process, and reduce the wear of the die.
  • Emulsifiers include one or more combinations of polyglycerol fatty acid esters, Tween-80, and polyvinyl alcohol. Emulsifiers can to a certain extent Slow down the loss of flavor substances during storage, increase the stability of flavor substances, and improve the sensory quality of the product.
  • the smoke-generating agent raw material may include: a monohydric alcohol (such as menthol); a polyhydric alcohol (such as propylene glycol, glycerol, triethylene glycol, 1,3-butylene glycol and tetraethylene glycol); an ester of a polyhydric alcohol (such as triacetin, triethyl citrate, a mixture of diacetin esters, triethyl citrate, benzyl benzoate, glyceryl tributyrate); a monocarboxylic acid; a dicarboxylic acid; a polycarboxylic acid (such as lauric acid, myristic acid) or an aliphatic ester of a polycarboxylic acid (such as dimethyl dodecanedioate, dimethyl tetradecanedioate, erythritol, 1,3-butylene glycol, tetraethylene glycol, triethyl citrate, propylene carbonate,
  • the adhesive raw material is in close contact with the component raw material interface by wetting, generating intermolecular attraction, thereby playing the role of bonding the component raw materials, such as powders, liquids, etc.
  • the adhesive raw material can be a natural plant extract, a non-ionized modified viscous polysaccharide, including one or more combinations of tamarind polysaccharides, guar gum, and modified cellulose (such as carboxymethyl cellulose).
  • the adhesive is used to bond the particles together, which is not easy to loosen. In addition, it improves the water resistance of the aerosol generating matrix and is harmless to the human body.
  • the flavor raw material is used to provide a characteristic aroma, such as a solid or liquid substance of hay aroma, roasted sweet aroma, and nicotine.
  • the flavor raw material may include one or more combinations of tobacco or other plants, flavor plant extracts, extracts, essential oils, and absolute oils; the flavor raw material may include one or more combinations of monomer flavor substances, such as megastigmatriene, neophytadiene, geraniol, nerol, and the like.
  • the plant raw material in 100 parts by weight of the mixture, can be 30 to 90 parts, the auxiliary raw material can be 1 to 15 parts, the smoke agent raw material can be 5 to 30 parts, the adhesive raw material can be 1 to 10 parts, and the flavor raw material can be 1 to 15 parts.
  • the extruded matrix 200 with different structures can be extruded.
  • the extruded matrix 200 with the air channel 200 a can be extruded.
  • the number of air passages 200a may be one or more.
  • the air passages 200a may be as shown in FIG.
  • the straight airway can be a spiral airway as shown in Figure 14, or a combination of a straight airway and a spiral airway.
  • the straight airway is an airway extending along a straight line, or in other words, the extending direction of the straight airway is a straight line.
  • the spiral airway is an airway in which at least part of the area along the extension direction is in a curved shape with a curvature not equal to zero.
  • the spiral airway may have a structure in which there are both a curved segment with a curvature not equal to zero and a straight segment with a curvature of zero, or may have only a curved segment with a curvature not equal to zero and no straight segment with a curvature of zero.
  • the spiral airway does not need to extend along a straight line.
  • the air channel 200a can be located inside the extruded matrix 200 as shown in Figures 13 and 14, or it can be located on the outer wall of the extruded matrix 200. When the number of air channels 200a is multiple, a portion of the air channels 200a can be located inside the extruded matrix 200, and another portion of the air channels 200a can be located on the outer wall of the extruded matrix 200 as shown in Figure 15.
  • the shape of the cross section of the air channel 200a located inside the extruded matrix 200 is not limited.
  • the shape of the cross section can be circular, polygonal (including but not limited to triangle, square, prism, etc.), elliptical, racetrack-shaped or irregular, etc., wherein irregular refers to other symmetrical or asymmetrical shapes other than the shapes listed above.
  • the cross-sectional shape of the air channel 200a located on the outer side wall of the extruded matrix 200 can be semicircular, semi-elliptical, polygonal or irregular, wherein irregular refers to other symmetrical or asymmetrical shapes other than the shapes listed above.
  • the air channel 200a is used to increase the surface area of the aerosol generating substrate (the side wall of the air channel 200a is equivalent to a part of the surface of the aerosol generating substrate), so that the heat acting on the aerosol generating substrate can enter the interior of the aerosol generating substrate from the surface of the aerosol generating substrate to improve the heating efficiency.
  • some aerosol generating matrices have naturally formed micropores inside.
  • the gaps between particles constitute micropores.
  • the airway 200a described in the present application is different from the micropores.
  • the airway 200a described in the present application is a hole in the macroscopic sense, while the micropores are holes in the microscopic sense.
  • the cross-sectional area and length of the airway 200a are much larger than those of the micropores.
  • the airway 200a is mainly processed. Therefore, the cross-sectional area and length of the airway 200a can be changed according to the design requirements, while the size of the micropores is determined by the size of the particles.
  • the cross-sectional area and length of the micropores are determined by the gap between them, and the dimensions of the micropores are naturally formed by the extrusion process.
  • the extrusion pressure of room temperature extrusion molding may be 0.5 bar to 300 bar (inclusive).
  • the extrusion pressure described in the embodiments of the present application refers to the extrusion pressure of the extrusion die located at the outlet of the extruder.
  • the extrusion pressure will affect the molding shape, surface smoothness, yield rate, and production rate of the extruded matrix.
  • the extrusion pressure is lower than 0.5 bar, the molding rate of the extruded matrix is low, and the product defect rate increases, which in turn leads to a slow production rate and increased production costs.
  • the extrusion pressure is higher than 300 bar, the transmission structure load of the extruder is high (the torque required is high), which leads to a decrease in the service life of the extruder. Therefore, controlling the extrusion pressure within the range of 0.5 bar to 300 bar can not only improve the molding rate of the extruded matrix, but also extend the service life of the extruder.
  • the extrusion pressure of room temperature extrusion molding can be 20 bar to 80 bar (including 20 bar and 80 bar).
  • the extrusion method of room temperature extrusion molding can be horizontal extrusion.
  • Horizontal extrusion means that the extrusion die at the extruder outlet is arranged horizontally, and the extruded matrix is extruded in the horizontal direction (such as the extruder 110 shown in Figures 2 and 3), or in other words, the extrusion direction of the extruded matrix is parallel to the horizontal plane.
  • the die of the extrusion die rotates while the extruded matrix does not rotate, and the extruded matrix extruded by the rotating die directly enters the conveying device (such as the first conveying device 140 in Figures 2 and 3). Since the rotation of the die will cause a certain stress to be generated in the extruded matrix, horizontal extrusion can reduce the direct release of the stress of the extruded matrix (the generated stress can be eliminated by heating). Therefore, horizontal extrusion can improve the yield rate of the aerosol-generating matrix with a spiral airway.
  • the extrusion method of room temperature extrusion molding can also be vertical extrusion.
  • Vertical extrusion means that the extrusion die at the extruder outlet is set downward, and the extruded matrix is extruded along the direction of gravity (such as the extruder 110 shown in Figures 4 and 5), or in other words, the extrusion direction of the extruded matrix is parallel to the water.
  • the plane is vertical.
  • the manufacturing equipment 100 may be provided with a third conveying device 170 , and the extruded matrix 200 directly enters the third conveying device 170 after being extruded from the extruder 110 .
  • vertical extrusion can improve the yield rate and reduce the investment cost of the extruder. It can also reduce the floor space of the extruder.
  • the extrusion method of room temperature extrusion molding can also be inclined extrusion.
  • Inclined extrusion means that the extrusion die at the extruder outlet is inclined, and the angle between the extrusion direction of the extruded matrix and the horizontal plane is greater than 0° and less than 90°.
  • Inclined extrusion can not only reduce the extrusion pressure of the mixed material, but also facilitate the space design of other equipment.
  • the extrusion die 113 can be a single-mold single-mouth die, that is, there is one bottom die 1131 (the bottom die 1131 is not shown in Figure 6, and the bottom die 1131 in Figure 7 can be referred to) at the outlet of the extruder 110, and the discharge end of the bottom die 1131 has a mouth die 1132. After the mixed material 200′ passes through the mouth die 1132, an extruded matrix 200 with an air channel 200a can be formed.
  • the extrusion die 113 may also be a single-mode multi-port die, that is, there is one bottom die 1131 at the outlet of the extruder 110, and the discharge end of the bottom die 1131 has multiple port dies 1132. After the mixed material 200 ′ passes through the multiple port dies 1132, multiple extruded matrices 200 are simultaneously formed.
  • a single-mode multi-port die may be selected, which can improve production efficiency and is more suitable for mass production.
  • the extrusion die 113 can also be a multi-mode multi-port die, that is, the adapter 116 at the outlet of the extruder 110 is connected to a plurality of bottom dies 1131, and the discharge end of each bottom die 1131 is provided with a plurality of port dies 1132. After the mixed material 200 ′ passes through the port dies 1132 on each bottom die 1131, a plurality of extruded matrices 200 are simultaneously formed.
  • a multi-mode multi-port die can also be selected, which can improve production efficiency and is more suitable for mass production.
  • the absolute pressure of the vacuum environment may be 0 kPa to 101.325 kPa (including 0 kPa and 101.325 kPa).
  • the absolute pressure of the vacuum environment may be 4 kPa to 20 kPa (including 4 kPa and 20 kPa).
  • the water content of the extruded matrix after negative pressure drying may be 3% to 20% (inclusive) of the total weight of the extruded matrix.
  • step S20 is not the last step of the manufacturing method
  • the dried extruded matrix is fragile in the subsequent processing process, which not only leads to a high defect rate in subsequent production, but also increases production costs.
  • the smoke water content of the aerosol-generating matrix during the heating and suction process is high, and the smoke temperature is not easy to reduce, which easily causes the user to have a "hot mouth” phenomenon during the suction process, reducing the user's suction experience. Therefore, controlling the water content in the dried extruded matrix within the range of 3% to 20% of the total weight of the extruded matrix can effectively improve the user's suction experience. In addition, for the extruded matrix that is processed by it after drying, the defect rate of subsequent production can also be reduced.
  • the water content of the extruded matrix after negative pressure drying may be 4% to 13% (including 4% and 13%) of the total weight of the extruded matrix.
  • the extruded matrix may be dried under negative pressure by at least one of microwave heating, resistance heating and infrared heating.
  • Microwave heating refers to the use of the energy characteristics of microwaves to heat materials.
  • Resistance heating refers to the use of the thermal effect of electric current passing through a resistor to heat the material.
  • Infrared heating refers to the use of infrared radiation heat transfer to heat materials.
  • microwave heating resistance heating and infrared heating
  • a combination of any two of them can be used, or all three of them can be used.
  • Microwave heating, resistance heating and infrared heating can keep the temperature of the vacuum environment at the required temperature more stably.
  • the temperature of the vacuum environment can be maintained in the range of greater than 20°C and less than 100°C, thereby better increasing the internal temperature of the extruded matrix and stimulating the vibration of water molecules inside the extruded matrix.
  • heating method is not limited to microwave heating, resistance heating and infrared heating. In other embodiments, other heating methods can also be used as long as the extruded matrix can be dried under negative pressure.
  • the manufacturing method may further include: cutting the extruded matrix into set lengths.
  • the length of the extruded matrix extruded by room temperature extrusion molding is usually relatively long, so the extruded matrix can be cut into required lengths according to different usage scenarios.
  • the manufacturing equipment 100 is provided with a slitting device 150 having a slitting tool (not shown), and the extruded matrix 200 is slitting by the slitting tool.
  • slitting there are many ways of slitting.
  • physical contact slitting in which the slitting tool contacts the extruded matrix can be used. That is, the slitting tool directly contacts the extruded matrix.
  • Physical contact slitting includes but is not limited to rotary hob cutting, cutting disc cutting, wire cutting, roller cutting, extrusion and the like.
  • non-physical contact slitting between the slitting tool and the extruded matrix can also be used, that is, the slitting tool itself has no physical contact with the extruded matrix.
  • Non-physical contact slitting includes but is not limited to laser cutting, plasma cutting, air knife, water knife and the like.
  • the extruded matrix can be cut into set lengths before the extruded matrix is subjected to negative pressure drying. In other words, the extruded matrix is first cut into set lengths and then subjected to negative pressure drying.
  • the extruded matrix may be pre-cut before the extruded matrix is subjected to negative pressure drying, and the pre-cut extruded matrix may be cut into set lengths after the extruded matrix is subjected to negative pressure drying.
  • Pre-slitting is equivalent to the initial slitting of the extruded matrix, and the length of the extruded matrix after pre-slitting is longer than the set length.
  • two cutting devices 150 can be provided.
  • the first cutting device 150 is provided along the material of the vacuum drying device 120. Upstream of the conveying direction, the second slitting device 150 is arranged downstream of the vacuum drying device 120 along the material conveying direction.
  • the first slitting device 150 is used to pre-slit the extruded matrix 200
  • the second slitting device 150 is used to slit the extruded matrix 200 after negative pressure drying into set lengths.
  • Figures 2 and 3 please refer to Figures 2 and 3.
  • the manufacturing equipment 100 can also be provided with a second conveying device 160 between the vacuum drying device 120 and the second slitting device 150.
  • the extruded matrix 200 that has completed negative pressure drying in the vacuum drying device 120 is conveyed to the second slitting device 150 by the second conveying device 160 for slitting.
  • the texture of the extruded matrix extruded by room temperature extrusion molding is usually relatively soft. Therefore, before the extruded matrix is subjected to negative pressure drying, pre-slitting of the extruded matrix is equivalent to slitting the soft body of the extruded matrix.
  • the cutting of the pre-cut extruded matrix is equivalent to cutting of the extruded matrix with a relatively hard texture.
  • the pre-slitting-negative pressure drying-slitting method can improve the consistency of the longitudinal dimension (i.e., the dimension along the extrusion direction) of the extruded matrix after cutting, thereby improving the slitting yield.
  • the extruded matrix can also be shaped after the pre-cut.
  • a jig may be used to circumferentially align the extruded matrix, and then the shaped extruded matrix may be dried under negative pressure.
  • a jig may be used to calibrate the circumference and straightness of the extruded matrix.
  • the extruded matrix can also be cut into set lengths after the extruded matrix is dried under negative pressure. That is, the extruded matrix is first dried under negative pressure and then cut into set lengths. Compared with the manufacturing method with pre-cutting, this embodiment actually omits the pre-cutting step.
  • Only one slitting device 150 may be provided downstream of the vacuum drying device 120 along the material conveying direction, while no slitting device 150 may be provided upstream of the vacuum drying device 120 along the material conveying direction. No slitting is performed on the extruded matrix 200 before the negative pressure drying. After the extruded matrix 200 is subjected to negative pressure drying, the slitting device 150 is used to cut the extruded matrix 200 into set lengths.
  • the texture of the extruded matrix extruded by room temperature extrusion molding is usually relatively soft. Therefore, the extruded matrix is first subjected to negative pressure drying and then cut to prevent the cutting before negative pressure drying from causing slight deformation to the extruded matrix with lower hardness.
  • a jig can also be used to calibrate the circumference and straightness of the extruded matrix before slitting.
  • the extruded matrix of a set length can be directly extruded by room temperature extrusion molding.
  • the extruded matrix can naturally detach under the action of its own gravity when it reaches or approaches the set length, thereby reducing the subsequent slitting steps and further reducing the production cost.
  • the manufacturing method before the extruded matrix is subjected to negative pressure drying, the manufacturing method further comprises: cooling and hardening the extruded matrix.
  • the extruded matrix can be cooled and hardened before negative pressure drying to increase the hardness of the extruded matrix.
  • the hardness of the extruded matrix extruded by room temperature extrusion molding before cooling and hardening may be 0HB to 100HB (including 0HB and 100HB), and after cooling and hardening, the hardness of the extruded matrix may be 1HB to 200HB (including 1HB and 200HB).
  • the hardness of the extruded matrix extruded by room temperature extrusion molding before cooling and hardening can be 1HB to 60HB (including 1HB and 60HB), and after cooling and hardening, the hardness of the extruded matrix can be 40HB to 120HB (including 40HB and 120HB).
  • the temperature of the extruded matrix before cooling and hardening may be 0°C to 40°C (including 0°C and 40°C), and the temperature of the extruded matrix after cooling and hardening may be -50°C to 5°C (including -50°C and 5°C).
  • the extruded matrix may be slit into set lengths after the extruded matrix is cooled and hardened.
  • the manufacturing equipment 100 can be provided with a hardening device 130 and two slitting devices 150.
  • the hardening device 130 is arranged between the extruder 110 and the vacuum drying device 120, so as to cool and harden the extruded matrix 200 before negative pressure drying.
  • One of the two slitting devices 150 is arranged between the hardening device 130 and the vacuum drying device 120, so as to pre-slit the extruded matrix 200 after cooling and hardening before negative pressure drying.
  • the other of the two slitting devices 150 is arranged downstream of the vacuum drying device 120 along the material conveying direction, so as to cut the extruded matrix 200 after negative pressure drying into set lengths.
  • the manufacturing equipment 100 may also only set the slitting device 150 between the hardening device 130 and the vacuum drying device 120, and no slitting device 150 is set downstream of the vacuum drying device 120 along the material conveying direction.
  • the slitting device 150 set between the hardening device 130 and the vacuum drying device 120 is used to cut the cooled and hardened extruded matrix 200 into set lengths before negative pressure drying. That is to say, after the extruded matrix 200 is cooled and hardened, it can be directly cut into set lengths without pre-cutting.
  • the extruded matrix Since the hardness of the extruded matrix increases after cooling and hardening, the extruded matrix is easier to cut after cooling and hardening, and the extruded matrix after cutting will not be deformed, and the cut surface is more neat and complete.
  • the cooling and hardening may be placing the extruded matrix in a low-temperature environment for cooling, wherein the temperature of the low-temperature environment is lower than the hardening temperature of the extruded matrix.
  • the temperature of the low-temperature environment refers to the ambient temperature within a device that provides the low-temperature environment.
  • the extruded matrix can be transferred to a low-temperature environment with a relatively low temperature for cooling.
  • the temperature in the low-temperature environment needs to be lower than the hardening temperature of the extruded matrix.
  • the temperature in the low-temperature environment is lower than the hardening temperature of the extruded matrix
  • the temperature of the low-temperature environment can be -270°C to 60°C (including -270°C and 60°C).
  • the temperature of the low temperature environment may be -100°C to 40°C (inclusive).
  • the cooling and hardening may also be performed by cooling the extruded matrix using a refrigerant.
  • the refrigerant may be in the form of a liquid, such as liquid nitrogen or liquefied air, or a gas or a solid.
  • the extruded substrate may be directly heat exchanged with a refrigerant.
  • Direct heat exchange refers to heat exchange between heat exchange media through direct contact. That is, the extruded matrix is in direct contact with the refrigerant.
  • the hardening device 130 can be provided with a refrigerant supplier (not shown) and a container 131 having a receiving chamber 131a, the receiving chamber 131a having a transmission channel 131c running through opposite sides of the container 131 and a liquid inlet 131b connected to the receiving chamber 131a, the extruded matrix 200 extruded from the extruder 110 enters the receiving chamber 131a through the transmission channel 131c, the refrigerant supplier injects the liquid refrigerant into the liquid inlet 131b, the refrigerant enters the receiving chamber 131a through the liquid inlet 131b and contacts with the extruded matrix 200 in the receiving chamber 131a for heat exchange.
  • a first conveying device 140 having multiple guide grooves 140a can be provided outside the die mouth of the extrusion die 113.
  • the first conveying device 140 passes through the conveying channel 131c to guide each extrusion matrix 200 through the conveying channel 131c into the accommodating cavity 131a for cooling and hardening.
  • the advantage of direct heat exchange between the extruded matrix and the refrigerant is that the surface of the hardened heat exchange medium can be cooled more quickly so that the extruded matrix can maintain the stability of the shape, thereby facilitating continuous production and improving production efficiency.
  • the extruded matrix can also be indirectly heat exchanged with the refrigerant.
  • the hardening device 130 may include a cooling tube 132, and the cooling tube 132 includes an inner tube 1321 and an outer tube 1322.
  • a liquid storage chamber 132a for storing the refrigerant is formed between the inner tube 1321 and the outer tube 1322.
  • the inner tube 1321 has a heat exchange channel 1321a extending therethrough.
  • the extruded matrix 200 extruded from the extruder 110 enters the heat exchange channel 1321a and contacts the inner tube 1321 for heat exchange.
  • the inner tube 1321 that absorbs the heat of the extruded matrix 200 then exchanges heat with the refrigerant, which is equivalent to indirect heat exchange between the extruded matrix 200 and the refrigerant through the inner tube 1321. Heat exchange.
  • the inner surface of the inner tube 1321 forming the heat exchange channel 1321a is generally a smooth surface.
  • the roughness of the inner surface of the inner tube 1321 can be Ra1.2 ⁇ m ⁇ Ra0.08 ⁇ m (including Ra1.2 ⁇ m and Ra0.08 ⁇ m). The friction between the smooth inner surface and the outer surface of the extruded matrix 200 is small, and will not cause deformation of the extruded matrix 200.
  • the advantage of indirect heat exchange between the extruded matrix and the refrigerant is that it can effectively avoid problems such as expansion deformation, cracking, etc. that may occur when the extruded matrix directly contacts the refrigerant.
  • cooling and hardening step there may be no cooling and hardening step.
  • a manufacturing method after the extruded matrix is extruded, before the negative pressure drying, only slitting may be performed without cooling and hardening.
  • the cooling and hardening step may be omitted.
  • the components of the mixed material include solid material and liquid material.
  • the manufacturing method may further include: dividing the solid material and the liquid material into two modules and feeding them separately.
  • Solid material refers to solid material
  • liquid material refers to liquid material. That is to say, part of the components in the mixed material are solid, and part of the components are liquid.
  • the solid material and the liquid material are mixed to form a mixed material.
  • the mixed material formed after the solid material and the liquid material are mixed is in a uniform form and can no longer be divided into solid material and liquid material.
  • the solid materials such as plant raw materials, auxiliary raw materials and adhesive raw materials and the liquid materials such as smoke agent raw materials and flavor raw materials can be added into the barrel of the extruder respectively, so that the solid materials and the liquid materials are mixed in the barrel of the extruder.
  • the advantage of dividing the solid material and liquid material into two modules for feeding separately is that it can reduce the pre-treatment cost of the mixed material, ensure the continuity of the production process, and improve the consistency and uniformity of the product while improving production efficiency.
  • dividing the solid material and the liquid material into two modules for feeding separately may include the following steps: adding the solid material; when the solid material moves along the material conveying direction to the liquid material adding position, adding the liquid material to the solid material.
  • solid material is first added to the extruder. After the solid material enters the barrel of the extruder, it will move along the material conveying direction toward the direction of the extrusion die. When the solid material moves along the material conveying direction to the liquid material adding position, liquid material is added to the extruder to mix the liquid material and the solid material in the barrel of the extruder.
  • the feeding amount and feeding speed can be determined according to the production speed of the extruder and the ratio of each raw material in the mixed material.
  • a solid material feeding port 114 and a liquid material feeding port 115 connected to the barrel 111 of the extruder 110 may be provided on the extruder 110 , and the liquid material feeding port 115 is located downstream of the solid material feeding port 114 along the material conveying direction.
  • the number of the solid material feeding ports 114 may be one or more. When a plurality of solid material feeding ports 114 are provided, each solid material feeding port 114 may be used to add the same solid material or different solid materials.
  • the number of the liquid material feeding ports 115 may be one or more. When multiple liquid material feeding ports 115 are provided, each liquid material feeding port 115 may be used to add the same liquid material or different liquid materials.
  • the extruder mainly relies on the rotation of the screw to convey the mixed material, and the screw and the inner wall of the extruder barrel are not completely sealed, that is, there is a gap between the screw and the inner wall of the extruder barrel. If the liquid material is added first, the liquid material will easily leak from the gap. Therefore, adding the solid material first, and then adding the liquid material when the solid material moves along the material conveying direction to the liquid material adding position, can better avoid liquid leakage.
  • the mixed material may not be fed separately as a solid material and a liquid material.
  • the solid material and the liquid material may be mixed first to form a mixed material (referred to as mixed slurry feeding), and then the mixed material is added to the barrel of the extruder.
  • the advantage of mixed slurry feeding is that the mixed material has better consistency, which can ensure the uniformity and stability of the product.
  • the feed port (using mixed slurry feeding)
  • a screw 112 may be further provided at the feeding port to further homogenize the mixed slurry.
  • the manufacturing method may further include: wrapping a packaging layer on the outer surface of the extruded matrix.
  • the packaging layer includes but is not limited to medium consumables such as cigarette paper, paper tubes, and tin foil.
  • medium consumables such as cigarette paper, paper tubes, and tin foil.
  • the extruded matrix wrapped with the packaging layer is equivalent to the finished product of the aerosol generating matrix.
  • the extruded matrix wrapped with the packaging layer may also be combined with other functional segments, such as a cooling segment, a filtering segment, etc., to form an aerosol generating product.
  • the manufacturing method may further include: sealing and packaging the extruded matrix.
  • the extruded matrix can be directly sealed and packaged, for example, the extruded matrix can be encapsulated in a blister packaging container.
  • the sealed and packaged extruded matrix is also equivalent to a finished product of the aerosol-generating matrix.
  • the sealed and packaged extruded matrix can be directly used on the electronic atomization device after removing the packaging.
  • the manufacturing method of the first embodiment mainly includes the following steps:
  • Step S01a feeding
  • Step S02a extrusion molding at room temperature
  • Step S03a cooling and hardening
  • Step S04a cutting
  • Step S05a negative pressure drying
  • Step S06a Packaging.
  • the manufacturing method of the second embodiment mainly includes the following steps:
  • Step S01b feeding
  • Step S02b extrusion molding at room temperature
  • Step S03b cutting
  • Step S04b negative pressure drying
  • Step S05b Packaging.
  • the manufacturing method of the second embodiment does not have a cooling and hardening step.
  • the manufacturing method of the third embodiment mainly includes the following steps:
  • Step S01c feeding
  • Step S02c extrusion molding at room temperature
  • Step S03c pre-cutting
  • Step S04c negative pressure drying
  • Step S05c cutting
  • Step S06c Packaging.
  • the manufacturing method of the third embodiment does not have a cooling and hardening step, and the slitting in the third embodiment includes pre-slitting before negative pressure drying and slitting after negative pressure drying.
  • the manufacturing method of the fourth embodiment mainly includes the following steps:
  • Step S01d feeding
  • Step S02d extrusion molding at room temperature
  • Step S03d negative pressure drying
  • Step S04d Packaging.
  • the manufacturing method of the fourth embodiment does not have the steps of cooling, hardening and slitting.
  • the reference terms "in one embodiment”, “in some embodiments”, “in other embodiments”, “in yet other embodiments”, or “exemplary” etc. mean that the specific features, structures, materials or characteristics described in conjunction with the embodiment or example are included in at least one embodiment of the present application. or examples.
  • the schematic representations of the above terms do not necessarily refer to the same embodiment or example.
  • the specific features, structures, materials or characteristics described can be combined in any one or more embodiments or examples in a suitable manner.
  • those skilled in the art can combine different embodiments or examples described in this application and the features of different embodiments or examples without contradiction.

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Abstract

An aerosol generating matrix manufacturing method, comprising: performing room temperature extrusion molding on a mixed material, to cause the mixed material to form an extruded matrix; performing negative pressure drying on the extruded matrix in a vacuum environment. The manufacturing method combines room temperature extrusion molding with negative pressure drying, which can not only achieve a uniform and stable aerosol generating matrix having uniform internal pore distribution and high processability, but also achieve continuous production of the aerosol generating matrix with high production efficiency and low manufacturing costs. In addition, an aerosol generating matrix manufacturing device is ​​provided.

Description

一种气溶胶生成基质的制造方法及制造设备A method and device for manufacturing an aerosol-generating substrate

相关申请的交叉引用CROSS-REFERENCE TO RELATED APPLICATIONS

本申请基于申请号为202310684825.9,申请日为2023年06月09日的中国专利申请提出,并要求该中国专利申请的优先权,该中国专利申请的全部内容在此引入本申请作为参考。This application is based on the Chinese patent application with application number 202310684825.9 and application date June 9, 2023, and claims the priority of the Chinese patent application. The entire content of the Chinese patent application is hereby introduced into this application as a reference.

技术领域Technical Field

本申请涉及发烟制品技术领域,特别是涉及一种气溶胶生成基质的制造方法及制造设备。The present application relates to the technical field of smoking products, and in particular to a method and equipment for manufacturing an aerosol generating substrate.

背景技术Background Art

发烟制品包括通过点燃的方式形成气溶胶的发烟制品以及通过加热而不燃烧的方式形成气溶胶的发烟制品,其中,在一个典型的加热而不燃烧的发烟制品中,其包含烟草或其他植物原料、香味原料或/及雾化剂等可在加热时挥发以产生气溶胶的气溶胶生成基质,气溶胶生成基质利用外部热源加热,使其刚好加热到足以散发出香味的程度,气溶胶生成基质不会燃烧,而是通过负载雾化剂,使用时通过加热释放雾化剂,以形成烟雾。Smoking articles include smoking articles that form aerosols by ignition and smoking articles that form aerosols by heating without burning. In a typical smoking article that heats without burning, it contains an aerosol-generating substrate such as tobacco or other plant materials, flavor materials and/or atomizers that can volatilize when heated to produce an aerosol. The aerosol-generating substrate is heated by an external heat source so that it is heated just enough to emit a fragrance. The aerosol-generating substrate does not burn, but instead loads the atomizer and releases the atomizer by heating when used to form smoke.

气溶胶生成基质气溶胶生成基质主要有颗粒型、传统烟丝型和薄片型三种,但是,相关技术中,气溶胶生成基质的制造方法复杂,设备投资高、生产效率低且对环境污染大。Aerosol generating substrates There are three main types of aerosol generating substrates: particle type, traditional tobacco type and sheet type. However, in the related art, the manufacturing method of the aerosol generating substrate is complicated, the equipment investment is high, the production efficiency is low and the environmental pollution is great.

发明内容Summary of the invention

有鉴于此,本申请实施例期望提供一种生产效率较高,且成本较低的气溶胶生成基质的制造方法及制造设备。In view of this, the embodiments of the present application hope to provide a method and a manufacturing device for an aerosol generating substrate with high production efficiency and low cost.

为达到上述目的,本申请实施例提供了一种气溶胶生成基质的制造方法,所述制造方法包括: To achieve the above object, the present application provides a method for manufacturing an aerosol generating substrate, the manufacturing method comprising:

对混合物料进行常温挤出成型,以使所述混合物料形成挤出基质;Extruding the mixed material at room temperature to form an extrusion matrix;

在真空环境中对所述挤出基质进行负压干燥。The extruded matrix is dried under negative pressure in a vacuum environment.

一种实施方式中,所述常温挤出成型的挤出温度为10℃~90℃。In one embodiment, the extrusion temperature of the room temperature extrusion molding is 10°C to 90°C.

一种实施方式中,所述真空环境的温度大于20℃且小于100℃。In one embodiment, the temperature of the vacuum environment is greater than 20°C and less than 100°C.

一种实施方式中,所述真空环境的绝对压力为0kpa~101.325kpa。In one implementation, the absolute pressure of the vacuum environment is 0 kPa to 101.325 kPa.

一种实施方式中,所述常温挤出成型的挤出压力为0.5bar~300bar。In one embodiment, the extrusion pressure of the room temperature extrusion molding is 0.5 bar to 300 bar.

一种实施方式中,所述挤出温度为35℃~70℃。In one embodiment, the extrusion temperature is 35°C to 70°C.

一种实施方式中,所述绝对压力为4kpa~20kpa。In one embodiment, the absolute pressure is 4 kPa to 20 kPa.

一种实施方式中,所述挤出压力为20bar~80bar。In one embodiment, the extrusion pressure is 20 bar to 80 bar.

一种实施方式中,所述常温挤出成型的挤出方式为水平挤出、垂直挤出和倾斜挤出中的一种。In one embodiment, the extrusion method of the room temperature extrusion molding is one of horizontal extrusion, vertical extrusion and inclined extrusion.

一种实施方式中,对所述挤出基质进行负压干燥,包括:In one embodiment, the extruded matrix is subjected to negative pressure drying, comprising:

采用微波加热、电阻加热和红外加热中的至少一种加热方式对所述挤出基质进行负压干燥。The extruded matrix is dried under negative pressure by using at least one heating method selected from microwave heating, resistance heating and infrared heating.

一种实施方式中,所述制造方法还包括:将所述挤出基质分切成设定长度。In one embodiment, the manufacturing method further comprises: slitting the extruded matrix into set lengths.

一种实施方式中,所述将所述挤出基质分切成设定长度,包括:在对所述挤出基质进行所述负压干燥之前,将所述挤出基质分切成所述设定长度。In one embodiment, the cutting the extruded matrix into the set length comprises: before the extruded matrix is subjected to the negative pressure drying, the cutting the extruded matrix into the set length.

一种实施方式中,所述将所述挤出基质分切成设定长度,包括:在对所述挤出基质进行所述负压干燥之前,对所述挤出基质进行预分切,在对所述挤出基质进行所述负压干燥之后,将预分切的所述挤出基质分切成所述设定长度。In one embodiment, the cutting of the extruded matrix into set lengths comprises: pre-cutting the extruded matrix before the negative pressure drying of the extruded matrix, and cutting the pre-cut extruded matrix into the set lengths after the negative pressure drying of the extruded matrix.

一种实施方式中,分切的方式为分切工具与所述挤出基质接触的物理接触式分切。In one embodiment, the slitting is performed by physical contact slitting in which a slitting tool contacts the extruded matrix.

一种实施方式中,分切的方式为分切工具与所述挤出基质间隔的非物理接触式分切。In one embodiment, the slitting is performed by non-physical contact slitting between a slitting tool and the extruded matrix.

一种实施方式中,在对所述挤出基质进行所述负压干燥之前,所述制造方法还包括:对所述挤出基质进行冷却硬化。In one embodiment, before the negative pressure drying of the extruded matrix, the manufacturing method further comprises: cooling and hardening the extruded matrix.

一种实施方式中,所述对所述挤出基质进行冷却硬化,包括: In one embodiment, the cooling and hardening of the extruded matrix comprises:

将所述挤出基质置入低温环境中进行冷却,其中,所述低温环境的温度低于所述挤出基质的硬化温度。The extruded matrix is placed in a low temperature environment for cooling, wherein the temperature of the low temperature environment is lower than the hardening temperature of the extruded matrix.

一种实施方式中,所述硬化温度为-100℃~60℃,所述低温环境的温度为-270℃~60℃。In one embodiment, the hardening temperature is -100°C to 60°C, and the temperature of the low temperature environment is -270°C to 60°C.

一种实施方式中,所述对所述挤出基质进行冷却硬化,包括:将所述挤出基质与冷媒进行直接换热。In one embodiment, the cooling and hardening of the extruded matrix comprises: directly exchanging heat between the extruded matrix and a refrigerant.

一种实施方式中,所述对所述挤出基质进行冷却硬化,包括:将所述挤出基质与冷媒进行间接换热。In one embodiment, the cooling and hardening of the extruded matrix comprises: indirectly exchanging heat between the extruded matrix and a refrigerant.

一种实施方式中,在对所述挤出基质进行硬化处理之后,所述制造方法还包括:将所述挤出基质分切成设定长度。In one embodiment, after the extruded matrix is hardened, the manufacturing method further comprises: cutting the extruded matrix into set lengths.

一种实施方式中,经过所述冷却硬化之后的所述挤出基质的硬度为1HB~200HB。In one embodiment, the hardness of the extruded matrix after cooling and hardening is 1HB to 200HB.

一种实施方式中,经过所述冷却硬化之后的所述挤出基质的温度为-50℃~5℃。In one embodiment, the temperature of the extruded matrix after cooling and hardening is -50°C to 5°C.

一种实施方式中,经过所述负压干燥后的所述挤出基质的硬度为40HB~300HB。In one embodiment, the hardness of the extruded matrix after the negative pressure drying is 40HB to 300HB.

一种实施方式中,经过所述负压干燥后的所述挤出基质中的含水量为所述挤出基质的总重量的3%~20%。In one embodiment, the water content of the extruded matrix after the negative pressure drying is 3% to 20% of the total weight of the extruded matrix.

一种实施方式中,所述混合物料的组分包括固料和液料,在对混合物料进行常温挤出成型之前,所述制造方法还包括:In one embodiment, the components of the mixed material include a solid material and a liquid material. Before the mixed material is subjected to room temperature extrusion molding, the manufacturing method further includes:

将所述固料和所述液料分成两个模块分别进行喂料。The solid material and the liquid material are divided into two modules for feeding respectively.

一种实施方式中,所述将所述固料和所述液料分成两个模块分别进行喂料,包括:In one embodiment, the solid material and the liquid material are divided into two modules for feeding respectively, comprising:

添加所述固料;adding the solid material;

当所述固料沿物料输送方向移动至所述液料的添加位置,向所述固料中添加所述液料。When the solid material moves along the material conveying direction to the adding position of the liquid material, the liquid material is added to the solid material.

一种实施方式中,在对所述挤出基质进行负压干燥之后,所述制造方法还 包括:在所述挤出基质的外表面包裹包装层。In one embodiment, after the extruded matrix is subjected to negative pressure drying, the manufacturing method further comprises: The method comprises: wrapping a packaging layer on the outer surface of the extruded matrix.

一种实施方式中,在对所述挤出基质进行负压干燥之后,所述制造方法还包括:对所述挤出基质进行密封包装。In one embodiment, after the extruded matrix is dried under negative pressure, the manufacturing method further comprises: sealing and packaging the extruded matrix.

一种实施方式中,在100重量份的所述混合物料中,植物原料为30份~90份,助剂原料为1~15份,发烟剂原料为5份~30份,粘合剂原料为1份~10份,香料原料为1~15份。In one embodiment, in 100 parts by weight of the mixed material, the plant raw material is 30 to 90 parts, the auxiliary raw material is 1 to 15 parts, the smoke agent raw material is 5 to 30 parts, the adhesive raw material is 1 to 10 parts, and the fragrance raw material is 1 to 15 parts.

本申请实施例提供了一种气溶胶生成基质的制造设备,包括:The present application embodiment provides a manufacturing device for an aerosol generating substrate, comprising:

挤出机,所述挤出机用于对混合物料进行常温挤出成型,以使所述混合物料形成挤出基质;An extruder, the extruder is used to perform room temperature extrusion molding on the mixed material so that the mixed material forms an extrusion matrix;

真空干燥装置,所述真空干燥装置用于对所述挤出基质进行负压干燥。A vacuum drying device is used to perform negative pressure drying on the extruded matrix.

一种实施方式中,所述挤出机的挤出模具为具有一个底模,且所述底模的出料端具有一个口模的单模单口模具。In one embodiment, the extrusion die of the extruder is a single-die single-mouth die having a bottom die, and a mouth die at the discharge end of the bottom die.

一种实施方式中,所述挤出机的挤出模具为具有一个底模,且所述底模的出料端具有多个口模的单模多口模具。In one embodiment, the extrusion die of the extruder is a single-die multi-die having a bottom die, and a discharge end of the bottom die having a plurality of die openings.

一种实施方式中,所述挤出机的挤出模具为具有多个底模,且各所述底模的出料端分别具有多个口模的模多口模具。In one embodiment, the extrusion die of the extruder is a multi-opening die having a plurality of bottom dies, and the discharge end of each bottom die has a plurality of opening dies.

一种实施方式中,所述制造设备还包括硬化装置和两个分切装置;In one embodiment, the manufacturing apparatus further comprises a hardening device and two slitting devices;

所述硬化装置设置在所述挤出机和所述真空干燥装置之间,以用于在进行所述负压干燥之前对所述挤出基质进行冷却硬化;The hardening device is disposed between the extruder and the vacuum drying device to cool and harden the extruded matrix before the negative pressure drying;

两个所述分切装置的其中之一设置在所述硬化装置与所述真空干燥装置之间,以用于在进行所述负压干燥之前,对经过所述冷却硬化的所述挤出基质进行预分切;两个所述分切装置的其中另一设置在所述真空干燥装置沿物料输送方向的下游,以用于将经过所述负压干燥的所述挤出基质分切成设定长度。One of the two slitting devices is arranged between the hardening device and the vacuum drying device, so as to pre-slit the extruded matrix that has undergone the cooling and hardening before the negative pressure drying; the other of the two slitting devices is arranged downstream of the vacuum drying device along the material conveying direction, so as to cut the extruded matrix that has undergone the negative pressure drying into set lengths.

一种实施方式中,所述制造设备还包括硬化装置和分切装置;In one embodiment, the manufacturing equipment further comprises a hardening device and a slitting device;

所述硬化装置设置在所述挤出机和所述真空干燥装置之间,以用于在进行所述负压干燥之前对所述挤出基质进行冷却硬化;The hardening device is disposed between the extruder and the vacuum drying device to cool and harden the extruded matrix before the negative pressure drying;

所述分切装置设置在所述硬化装置与所述真空干燥装置之间,以用于在进 行所述负压干燥之前,将经过所述冷却硬化的所述挤出基质分切成设定长度。The slitting device is arranged between the hardening device and the vacuum drying device to Before performing the negative pressure drying, the extruded matrix that has been cooled and hardened is cut into set lengths.

本申请实施例提供了一种气溶胶生成基质的制造方法及制造设备,该制造方法主要是对混合物料进行常温挤出成型,再在真空环境中对挤出基质进行负压干燥。常温挤出成型可以保证浆料流变特性稳定,且挤出的挤出基质的内源性成分稳定,而负压干燥可以确保挤出基质的收缩率小,干燥时间短,便于实现连续化生产。常温挤出成型与负压干燥搭配使用,不仅可以实现气溶胶生成基质均一稳定、内部孔隙分布均匀,气溶胶生成基质的可加工性高,还可以实现气溶胶生成基质的连续化生产,生产效率高,制造成本低。The embodiment of the present application provides a method and equipment for manufacturing an aerosol generating matrix, the manufacturing method mainly involves extrusion molding the mixed material at room temperature, and then negative pressure drying the extruded matrix in a vacuum environment. Room temperature extrusion molding can ensure the stability of the rheological properties of the slurry, and the endogenous components of the extruded extruded matrix are stable, while negative pressure drying can ensure that the shrinkage rate of the extruded matrix is small and the drying time is short, which is convenient for realizing continuous production. The combination of room temperature extrusion molding and negative pressure drying can not only realize the uniformity and stability of the aerosol generating matrix, the uniform distribution of internal pores, and the high processability of the aerosol generating matrix, but also realize the continuous production of the aerosol generating matrix, with high production efficiency and low manufacturing cost.

附图说明BRIEF DESCRIPTION OF THE DRAWINGS

图1为本申请实施例的一种气溶胶生成基质的制造方法的方法示意图;FIG1 is a schematic diagram of a method for manufacturing an aerosol generating substrate according to an embodiment of the present application;

图2为本申请实施例的一种气溶胶生成基质的制造设备的结构示意图,图中同时示出了混合物料和挤出基质;FIG2 is a schematic structural diagram of an aerosol generating substrate manufacturing device according to an embodiment of the present application, wherein a mixed material and an extruded substrate are shown at the same time;

图3为图2所示的制造设备的剖视图;FIG3 is a cross-sectional view of the manufacturing equipment shown in FIG2 ;

图4为本申请实施例的另一种气溶胶生成基质的制造设备的结构示意图,图中同时示出了混合物料和挤出基质;FIG4 is a schematic structural diagram of another aerosol-generating substrate manufacturing device according to an embodiment of the present application, in which a mixed material and an extruded substrate are shown at the same time;

图5为图4所示的制造设备的剖视图;FIG5 is a cross-sectional view of the manufacturing equipment shown in FIG4;

图6为本申请实施例的第一种挤出模具的口模的结构示意图;FIG6 is a schematic structural diagram of a first extrusion die of an embodiment of the present application;

图7为本申请实施例的第二种挤出模具的结构示意图,图中同时示出了挤出基质;FIG7 is a schematic diagram of the structure of a second extrusion die according to an embodiment of the present application, and also shows an extruded matrix;

图8为本申请实施例的第三种挤出模具的结构示意图,图中同时示出了挤出基质和转接头;FIG8 is a schematic structural diagram of a third extrusion die according to an embodiment of the present application, in which an extrusion matrix and an adapter are shown at the same time;

图9为本申请实施例的一种真空干燥装置的结构示意图,图中同时示出了挤出基质;FIG9 is a schematic structural diagram of a vacuum drying device according to an embodiment of the present application, and also shows an extruded matrix;

图10为本申请实施例的一种硬化装置的结构示意图,图中同时示出了挤出模具和挤出基质;FIG10 is a schematic structural diagram of a hardening device according to an embodiment of the present application, in which an extrusion die and an extrusion matrix are shown;

图11为图10所示的硬化装置的剖视图; FIG11 is a cross-sectional view of the hardening device shown in FIG10 ;

图12为本申请实施例的另一种硬化装置的结构示意图,图中同时示出了挤出基质;FIG12 is a schematic structural diagram of another hardening device according to an embodiment of the present application, which also shows an extruded matrix;

图13为本申请实施例的第一种挤出基质的剖视图;FIG13 is a cross-sectional view of a first extruded matrix according to an embodiment of the present application;

图14为本申请实施例的第二种挤出基质的结构示意图;FIG14 is a schematic diagram of the structure of a second extruded matrix according to an embodiment of the present application;

图15为本申请实施例的第三种挤出基质的结构示意图;FIG15 is a schematic diagram of the structure of a third extruded matrix according to an embodiment of the present application;

图16为本申请实施例的第一种制造方法的流程图;FIG16 is a flow chart of a first manufacturing method according to an embodiment of the present application;

图17为本申请实施例的第二种制造方法的流程图;FIG17 is a flow chart of a second manufacturing method according to an embodiment of the present application;

图18为本申请实施例的第三种制造方法的流程图;FIG18 is a flow chart of a third manufacturing method according to an embodiment of the present application;

图19为本申请实施例的第四种制造方法的流程图。FIG. 19 is a flow chart of a fourth manufacturing method according to an embodiment of the present application.

具体实施方式DETAILED DESCRIPTION

本申请一实施例提供了一种气溶胶生成基质的制造方法。气溶胶生成基质用于与具有加热组件的电子雾化装置配合使用,具体地,加热组件对气溶胶生成基质进行加热雾化,以产生供用户吸食或者用于医药、美容等的气溶胶。An embodiment of the present application provides a method for manufacturing an aerosol-generating substrate. The aerosol-generating substrate is used in conjunction with an electronic atomization device having a heating component. Specifically, the heating component heats and atomizes the aerosol-generating substrate to generate an aerosol for users to inhale or for use in medicine, beauty, etc.

请参阅图1,该气溶胶生成基质的制造方法包括以下步骤:Referring to FIG. 1 , the method for manufacturing the aerosol generating substrate comprises the following steps:

步骤S10:对混合物料进行常温挤出成型,以使混合物料形成挤出基质;Step S10: Extruding the mixed material at room temperature to form an extrusion matrix;

具体地,挤出成型是指将物料加入到挤出机中,物料通过挤出机的料筒和螺杆间的作用,被螺杆向前推送,连续通过挤出机出口处的挤出模具而制成各种截面制品或半制品的一种加工方法。挤出成型形成的物料呈条状。Specifically, extrusion molding refers to a processing method in which the material is added to the extruder, and the material is pushed forward by the screw through the action between the barrel and the screw of the extruder, and continuously passes through the extrusion die at the outlet of the extruder to form various cross-section products or semi-finished products. The material formed by extrusion molding is in the form of strips.

混合物料是用于制造气溶胶生成基质的物料,混合物料是固料和液料的混合物,也就是说,混合物料中含有一定的水分。The mixed material is a material used to manufacture an aerosol-generating matrix. The mixed material is a mixture of a solid material and a liquid material, that is, the mixed material contains a certain amount of water.

在挤出成型领域,挤出温度(即挤出机的料筒内的温度)在10℃~90℃之间(包含10℃和90℃)定义为常温,挤出温度在10℃以下定义为低温,挤出温度在90℃以上定义为高温。In the field of extrusion molding, the extrusion temperature (i.e. the temperature inside the barrel of the extruder) between 10°C and 90°C (including 10°C and 90°C) is defined as room temperature, the extrusion temperature below 10°C is defined as low temperature, and the extrusion temperature above 90°C is defined as high temperature.

示例性地,本申请实施所述的对混合物料进行常温挤出成型可以是指在10℃~90℃的挤出温度范围内对混合物料进行挤出成型。Illustratively, the room-temperature extrusion molding of the mixed material described in the implementation of the present application may refer to extrusion molding of the mixed material within an extrusion temperature range of 10° C. to 90° C.

温度会影响混合物料在挤出机中的流动性及挤出基质外表面的光滑性。当 挤出温度低于10℃时,混合物料流动性差,挤出机的生产速度慢,效率低,且在该温度下挤出机所提供的扭矩较高,影响挤出机的使用寿命。Temperature affects the fluidity of the mixed material in the extruder and the smoothness of the outer surface of the extruded matrix. When the extrusion temperature is lower than 10°C, the fluidity of the mixed material is poor, the production speed of the extruder is slow, the efficiency is low, and the torque provided by the extruder at this temperature is high, which affects the service life of the extruder.

当挤出温度高于90℃时,混合物料流动快,混合物料在挤出机出口处的压力较小,不利于混合物料成型,由此,会导致良品率下降,另外,在该温度下,挤出机的能耗较高,生产成本增加。When the extrusion temperature is higher than 90°C, the mixed material flows fast and the pressure of the mixed material at the extruder outlet is relatively low, which is not conducive to the molding of the mixed material. As a result, the yield rate will decrease. In addition, at this temperature, the energy consumption of the extruder is high and the production cost increases.

当挤出温度为10℃~90℃时,混合物料流动性较好,有利于混合物料成型,能够保证混合物料流变特性稳定,且挤出的挤出基质的内源性成分稳定。另外,在该温度下,挤出机所提供的扭矩较低,挤出机的能耗较低,在提高挤出机的使用寿命的同时,也可以降低生产成本。When the extrusion temperature is 10°C to 90°C, the mixed material has good fluidity, which is conducive to the molding of the mixed material, can ensure the stability of the rheological properties of the mixed material, and the endogenous components of the extruded extrusion matrix are stable. In addition, at this temperature, the torque provided by the extruder is low, the energy consumption of the extruder is low, and the service life of the extruder is increased while reducing the production cost.

较优选地,常温挤出成型的挤出温度可以为35℃~70℃(包含35℃和70℃)。More preferably, the extrusion temperature of room temperature extrusion molding can be 35° C. to 70° C. (including 35° C. and 70° C.).

步骤S20:在真空环境中对挤出基质进行负压干燥。Step S20: performing negative pressure drying on the extruded matrix in a vacuum environment.

负压干燥的主要目的是使挤出基质中的水分蒸发,如果挤出基质含有较多的易挥发的润滑剂,则负压干燥还可以去除易挥发的润滑剂。The main purpose of negative pressure drying is to evaporate the water in the extruded matrix. If the extruded matrix contains a large amount of volatile lubricant, negative pressure drying can also remove the volatile lubricant.

需要说明的是,步骤S20可以是制造方法的最后一步,也就是说,干燥后的挤出基质就是气溶胶生成基质的成品。步骤S20也可以不是制造方法的最后一步,相当于干燥后的挤出基质只是气溶胶生成基质的半成品,在步骤S20之后,还可以有其它的处理,这些处理包括但不限于分切、包装等。It should be noted that step S20 may be the last step of the manufacturing method, that is, the dried extruded matrix is the finished product of the aerosol generating matrix. Step S20 may not be the last step of the manufacturing method, which is equivalent to the dried extruded matrix being only a semi-finished product of the aerosol generating matrix. After step S20, other processing may be performed, including but not limited to slitting, packaging, etc.

真空环境可以降低水的沸点(即水的沸点低于常压下的100℃的沸点),以使挤出基质中的水分能够在低温状态下蒸发(即水在100℃以下蒸发)。另外,负压干燥可以减缓水分从挤出基质中溢出,使挤出基质能够在水分溢出后保持预留的骨架,从而形成孔隙。孔隙是气溶胶生成基质在加热过程中释放气溶胶和香气的通道,因此,负压干燥可以提高气溶胶生成基质的孔隙率,进而可以提高气溶胶和香气的释放效率。The vacuum environment can reduce the boiling point of water (i.e., the boiling point of water is lower than the boiling point of 100°C under normal pressure), so that the water in the extruded matrix can evaporate at low temperature (i.e., water evaporates below 100°C). In addition, negative pressure drying can slow down the overflow of water from the extruded matrix, so that the extruded matrix can maintain the reserved skeleton after the water overflows, thereby forming pores. The pores are the channels for the aerosol-generating matrix to release aerosols and aromas during the heating process. Therefore, negative pressure drying can increase the porosity of the aerosol-generating matrix, and thus improve the release efficiency of aerosols and aromas.

示例性地,真空环境的温度可以大于20℃且小于100℃。Illustratively, the temperature of the vacuum environment may be greater than 20°C and less than 100°C.

真空环境的温度是指提供真空环境的装置内的环境温度。The temperature of the vacuum environment refers to the ambient temperature within the device that provides the vacuum environment.

当真空环境的温度低于或等于20℃时,烘干挤出基质所需的时间长,生产效率低,生产成本高。当真空环境的温度高于或等于100℃时,挤出基质中的 热敏性香气成分易受热挥发,同时,温度高于或等于100℃时,挤出基质达到软化点,挤出基质外壁的支持性下降,在真空负压的影响下,整体结构易发生收缩,从而导致挤出基质内部水分溢出后,骨架上的孔隙易收缩变形,孔隙率下降,由此,会导致气溶胶生成基质释放气溶胶和香气的通道受阻,影响整体释放效率。When the temperature of the vacuum environment is lower than or equal to 20°C, it takes a long time to dry the extruded matrix, the production efficiency is low, and the production cost is high. When the temperature of the vacuum environment is higher than or equal to 100°C, the extruded matrix Thermosensitive aroma components are easily volatilized by heat. At the same time, when the temperature is higher than or equal to 100°C, the extruded matrix reaches its softening point, and the support of the outer wall of the extruded matrix decreases. Under the influence of vacuum negative pressure, the overall structure is prone to shrinkage, which causes the pores on the skeleton to shrink and deform after the water inside the extruded matrix overflows, and the porosity decreases. As a result, the channel for the aerosol-generating matrix to release aerosols and aromas is blocked, affecting the overall release efficiency.

较优选地,真空环境的温度可以为30℃~60℃(包含30℃和60℃)。More preferably, the temperature of the vacuum environment may be 30° C. to 60° C. (inclusive).

另外,经过负压干燥后的挤出基质的硬度可以为40HB~300HB(包含40HB和300HB),较优选地,经过负压干燥后的挤出基质的硬度可以为80HB~250HB(包含80HB和250HB)。In addition, the hardness of the extruded matrix after negative pressure drying may be 40HB to 300HB (including 40HB and 300HB). More preferably, the hardness of the extruded matrix after negative pressure drying may be 80HB to 250HB (including 80HB and 250HB).

本申请另一实施例还提供了一种气溶胶生成基质的制造设备100,请参阅图2至图5,该制造设备100主要包括挤出机110和真空干燥装置120。Another embodiment of the present application further provides a manufacturing device 100 for an aerosol generating substrate. Please refer to FIGS. 2 to 5 . The manufacturing device 100 mainly includes an extruder 110 and a vacuum drying device 120 .

挤出机110用于对混合物料200′进行常温挤出成型,以使混合物料200′形成挤出基质200。The extruder 110 is used to perform room temperature extrusion molding on the mixed material 200 ′ so that the mixed material 200 ′ forms an extruded matrix 200 .

挤出机110可以是单螺杆挤出机,也可以是双螺杆挤出机,优选采用双螺杆挤出机,因为与单螺杆挤出机相比,双螺杆挤出机可在混合物料200′的输送过程对混合物料200′进行进一步均质,可提升产品稳定性,且双螺杆挤出机的挤出效率高于单螺杆挤出机。The extruder 110 can be a single-screw extruder or a twin-screw extruder. A twin-screw extruder is preferably used because, compared with a single-screw extruder, a twin-screw extruder can further homogenize the mixed material 200′ during the conveying process of the mixed material 200′, thereby improving product stability, and the extrusion efficiency of a twin-screw extruder is higher than that of a single-screw extruder.

真空干燥装置120用于对挤出基质200进行负压干燥。The vacuum drying device 120 is used to dry the extruded matrix 200 under negative pressure.

真空干燥装置120内的环境温度就是前面所述的真空环境的温度。The ambient temperature in the vacuum drying device 120 is the temperature of the vacuum environment mentioned above.

示例性地,请参阅图2至图4、图9,真空干燥装置120可以包括箱体121、真空泵122、加热系统(图未示出)和电器仪表控制系统(图未示出),其中,箱体121内设置有至少一个隔板123,隔板123上可放置料盘124,当需要对挤出基质200进行负压干燥时,可将料盘124取出,将挤出基质200放置在料盘124中,再将料盘124放置于箱体121内的隔板123上。真空泵122用于使箱体121内形成真空,隔板123通过被加热系统加热,为挤出基质200提供热量。Exemplarily, referring to FIGS. 2 to 4 and 9, the vacuum drying device 120 may include a housing 121, a vacuum pump 122, a heating system (not shown) and an electrical instrument control system (not shown), wherein at least one partition 123 is provided in the housing 121, and a material tray 124 may be placed on the partition 123. When the extruded matrix 200 needs to be negatively dried, the material tray 124 may be taken out, the extruded matrix 200 may be placed in the material tray 124, and then the material tray 124 may be placed on the partition 123 in the housing 121. The vacuum pump 122 is used to form a vacuum in the housing 121, and the partition 123 is heated by the heating system to provide heat for the extruded matrix 200.

也就是说,本申请实施例的气溶胶生成基质的制造方法主要是对混合物料进行常温挤出成型,再在真空环境中对挤出基质进行负压干燥。常温挤出成型 可以保证浆料流变特性稳定,且挤出的挤出基质的内源性成分稳定,而负压干燥可以确保挤出基质的收缩率小,干燥时间短,便于实现连续化生产。常温挤出成型与负压干燥搭配使用,不仅可以实现气溶胶生成基质均一稳定、内部孔隙分布均匀,气溶胶生成基质的可加工性高,还可以实现气溶胶生成基质的连续化生产,生产效率高,制造成本低。That is to say, the manufacturing method of the aerosol generating matrix of the embodiment of the present application mainly involves extruding the mixed material at room temperature, and then drying the extruded matrix under negative pressure in a vacuum environment. It can ensure the stability of the rheological properties of the slurry and the stability of the endogenous components of the extruded matrix, while negative pressure drying can ensure that the shrinkage of the extruded matrix is small and the drying time is short, which is convenient for continuous production. The combination of room temperature extrusion molding and negative pressure drying can not only achieve uniform and stable aerosol generation matrix, uniform internal pore distribution, and high processability of aerosol generation matrix, but also realize continuous production of aerosol generation matrix with high production efficiency and low manufacturing cost.

本申请实施例的混合物料可以包括植物原料、助剂原料、发烟剂原料、粘合剂原料和香料原料。The mixed materials of the embodiment of the present application may include plant raw materials, auxiliary raw materials, smoke-generating agent raw materials, adhesive raw materials and flavor raw materials.

植物原料用于在加热时产生气溶胶。助剂原料用于为植物原料提供骨架支撑。发烟剂原料用于在加热时产生烟雾。粘合剂原料用于粘结各原料组分。香料原料用于提供特征香气。如此,植物原料和发烟剂原料能够保证气溶胶生成量,而香料原料能够提升抽吸过程中的香气的释放,提升用户体验。助剂原料不仅能够提高混合物料的流动性,还使得气溶胶生成基质呈多孔结构,以便于气溶胶的提取和流动。粘合剂原料保证植物原料和助剂原料等构成稳定地混合物,避免结构松散。Plant raw materials are used to generate aerosols when heated. Auxiliary raw materials are used to provide skeleton support for plant raw materials. Smoke-generating agent raw materials are used to generate smoke when heated. Adhesive raw materials are used to bond various raw material components. Flavor raw materials are used to provide characteristic aromas. In this way, plant raw materials and smoke-generating agent raw materials can ensure the amount of aerosol generated, while flavor raw materials can increase the release of aroma during the inhalation process and enhance user experience. Auxiliary raw materials can not only improve the fluidity of the mixed materials, but also make the aerosol generation matrix porous to facilitate the extraction and flow of aerosols. Adhesive raw materials ensure that plant raw materials and auxiliary raw materials constitute a stable mixture to avoid loose structure.

示例性地,植物原料可以为烟叶原料、烟叶碎片、烟梗、烟末、香味植物等经破碎处理后形成的粉末中一种或多种组合。植物原料为香味的核心来源,植物原料中的内源物质可以给用户产生生理满足感,内源物质例如生物碱进入人体血液,促进脑垂体产生多巴胺,从而获得生理满足感。Exemplarily, the plant raw material can be one or more combinations of powders formed after crushing tobacco raw materials, tobacco leaf fragments, tobacco stems, tobacco dust, and flavor plants. Plant raw materials are the core source of flavor. Endogenous substances in plant raw materials can produce physiological satisfaction for users. Endogenous substances such as alkaloids enter the human blood and promote the pituitary gland to produce dopamine, thereby obtaining physiological satisfaction.

示例性地,助剂原料可以为无机填料、润滑剂、乳化剂中一种或多种组合。其中,无机填料包括重质碳酸钙、轻质碳酸钙、沸石、凹凸棒石、滑石粉、硅藻土中一种或多种组合。无机填料可以为植物原料提供骨架支撑作用,同时无机填料还具有微孔,可以提高气溶胶生成基质的孔隙率,从而提高气溶胶释放率。润滑剂包括小烛树蜡、巴西棕榈蜡、虫胶、向日葵蜡、米糠、蜂蜡、硬脂酸、软脂酸中一种或多种组合。润滑剂可以增加植物原料粉末的流动性,减少植物原料粉末相互间的摩擦力,可使植物原料粉末分布的整体密度较为均匀,也能降低用于挤压成型过程中所需的压力,降低口模的磨损。乳化剂包括聚甘油脂肪酸酯、吐温-80、聚乙烯醇中一种或多种组合。乳化剂在一定程度上能够 减缓香味物质在储存过程中的损失,增加香味物质的稳定性,提高产品的感官品质。Exemplarily, the auxiliary raw material can be one or more combinations of inorganic fillers, lubricants, and emulsifiers. Among them, the inorganic filler includes one or more combinations of heavy calcium carbonate, light calcium carbonate, zeolite, attapulgite, talc, and diatomaceous earth. The inorganic filler can provide a skeleton support for the plant raw material. At the same time, the inorganic filler also has micropores, which can increase the porosity of the aerosol generating matrix, thereby increasing the aerosol release rate. Lubricants include one or more combinations of candelilla wax, carnauba wax, shellac, sunflower wax, rice bran, beeswax, stearic acid, and palmitic acid. Lubricants can increase the fluidity of plant raw material powders, reduce the friction between plant raw material powders, make the overall density of plant raw material powder distribution more uniform, and reduce the pressure required for the extrusion molding process, and reduce the wear of the die. Emulsifiers include one or more combinations of polyglycerol fatty acid esters, Tween-80, and polyvinyl alcohol. Emulsifiers can to a certain extent Slow down the loss of flavor substances during storage, increase the stability of flavor substances, and improve the sensory quality of the product.

示例性地,发烟剂原料可以包括:一元醇(如薄荷醇);多元醇(如丙二醇、丙三醇、三乙二醇、1,3-丁二醇和四乙二醇);多元醇的酯(如三乙酸甘油酯、柠檬酸三乙酯、二乙酸甘油酯混合物、柠檬酸三乙酯、苯甲酸苯甲酯、甘油三丁酸酯);单羧酸;二元羧酸;多元羧酸(如月桂酸、肉豆蔻酸)或多元羧酸的脂肪族酯(如十二烷二酸二甲酯、十四烷二酸二甲酯、赤藻糖醇、1,3-丁二醇、四乙二醇、柠檬酸三乙酯、碳酸亚丙酯、月桂酸乙酯、特瑞克汀(Triactin)、内消旋赤藻糖醇、二乙酸甘油酯混合物、辛二酸二乙酯、柠檬酸三乙酯、苯甲酸苯甲酯、苯基乙酸苯甲酯、香草酸乙酯、甘油三丁酸酯、乙酸月桂酯)中一种或多种组合。Exemplarily, the smoke-generating agent raw material may include: a monohydric alcohol (such as menthol); a polyhydric alcohol (such as propylene glycol, glycerol, triethylene glycol, 1,3-butylene glycol and tetraethylene glycol); an ester of a polyhydric alcohol (such as triacetin, triethyl citrate, a mixture of diacetin esters, triethyl citrate, benzyl benzoate, glyceryl tributyrate); a monocarboxylic acid; a dicarboxylic acid; a polycarboxylic acid (such as lauric acid, myristic acid) or an aliphatic ester of a polycarboxylic acid (such as dimethyl dodecanedioate, dimethyl tetradecanedioate, erythritol, 1,3-butylene glycol, tetraethylene glycol, triethyl citrate, propylene carbonate, ethyl laurate, Triactin, meso-erythritol, a mixture of diacetin esters, diethyl suberate, triethyl citrate, benzyl benzoate, benzyl phenylacetate, ethyl vanillate, glyceryl tributyrate, lauryl acetate) in one or more combinations.

示例性地,粘合剂原料通过与组分原料界面润湿而紧密接触,产生分子间的吸引力,从而起到粘结组分原料,例如粉体、液体等的作用。粘合剂原料可以为天然植物提取、非离子化改性粘性多糖,包括罗望子多糖、瓜尔胶、改性纤维素(如羧甲基纤维素)中的一种或多种组合。粘合剂用于将颗粒粘接在一起,不易松散,此外提高了气溶胶生成基质的耐水性,对人体无害。Exemplarily, the adhesive raw material is in close contact with the component raw material interface by wetting, generating intermolecular attraction, thereby playing the role of bonding the component raw materials, such as powders, liquids, etc. The adhesive raw material can be a natural plant extract, a non-ionized modified viscous polysaccharide, including one or more combinations of tamarind polysaccharides, guar gum, and modified cellulose (such as carboxymethyl cellulose). The adhesive is used to bond the particles together, which is not easy to loosen. In addition, it improves the water resistance of the aerosol generating matrix and is harmless to the human body.

示例性地,香料原料用于提供特征香气,如干草香、烤甜香、烟碱的固体或液体物质。香料原料可以包括烟草或其他植物、香味植物提取物、浸膏、精油、净油中的一种或多种组合;香料原料可以包括单体香味物质,例如巨豆三烯酮、新植二烯、香叶醇、橙花醇等中的一种或多种组合。Exemplarily, the flavor raw material is used to provide a characteristic aroma, such as a solid or liquid substance of hay aroma, roasted sweet aroma, and nicotine. The flavor raw material may include one or more combinations of tobacco or other plants, flavor plant extracts, extracts, essential oils, and absolute oils; the flavor raw material may include one or more combinations of monomer flavor substances, such as megastigmatriene, neophytadiene, geraniol, nerol, and the like.

示例性地,在100重量份的混合物料中,植物原料可以为30份~90份,助剂原料可以为1~15份,发烟剂原料可以为5份~30份,粘合剂原料可以为1份~10份,香料原料可以为1~15份。For example, in 100 parts by weight of the mixture, the plant raw material can be 30 to 90 parts, the auxiliary raw material can be 1 to 15 parts, the smoke agent raw material can be 5 to 30 parts, the adhesive raw material can be 1 to 10 parts, and the flavor raw material can be 1 to 15 parts.

根据设置在挤出机出口处的挤出模具的结构形式的不同,可以挤出不同结构形式的挤出基质200,比如,请参阅图13至图15,可以挤出具有气道200a的挤出基质200。According to the different structures of the extrusion die disposed at the outlet of the extruder, the extruded matrix 200 with different structures can be extruded. For example, referring to FIGS. 13 to 15 , the extruded matrix 200 with the air channel 200 a can be extruded.

气道200a的数量可以是一个,也可以是多个。气道200a可以是图13所示 的直通气道,也可以图14所示的是螺旋气道,还可以是直通气道和螺旋气道的组合。直通气道是沿直线延伸的气道,或者说,直通气道的延伸方向为直线。The number of air passages 200a may be one or more. The air passages 200a may be as shown in FIG. The straight airway can be a spiral airway as shown in Figure 14, or a combination of a straight airway and a spiral airway. The straight airway is an airway extending along a straight line, or in other words, the extending direction of the straight airway is a straight line.

螺旋气道是沿延伸方向的至少部分区域呈曲率不为0的曲线形的气道,比如,沿螺旋气道的延伸方向,螺旋气道可以是既有曲率不为0的曲线段,又有曲率为0的直线段的结构形式,也可以是只有曲率不为0的曲线段,而没有曲率为0的直线段的结构形式。也就是说,从螺旋气道沿延伸方向的起点至终点,螺旋气道只要不是沿直线延伸即可。The spiral airway is an airway in which at least part of the area along the extension direction is in a curved shape with a curvature not equal to zero. For example, along the extension direction of the spiral airway, the spiral airway may have a structure in which there are both a curved segment with a curvature not equal to zero and a straight segment with a curvature of zero, or may have only a curved segment with a curvature not equal to zero and no straight segment with a curvature of zero. In other words, from the starting point to the end point of the spiral airway along the extension direction, the spiral airway does not need to extend along a straight line.

气道200a可以如图13和图14所示的位于挤出基质200的内部,也可以位于挤出基质200的外侧壁上,当气道200a的数量为多个时,还可以如图15所示的一部分气道200a位于挤出基质200的内部,另一部分气道200a位于挤出基质200的外侧壁上。The air channel 200a can be located inside the extruded matrix 200 as shown in Figures 13 and 14, or it can be located on the outer wall of the extruded matrix 200. When the number of air channels 200a is multiple, a portion of the air channels 200a can be located inside the extruded matrix 200, and another portion of the air channels 200a can be located on the outer wall of the extruded matrix 200 as shown in Figure 15.

位于挤出基质200内部的气道200a的横截面的形状不做限制,比如,横截面的形状可以是圆形、多边形(包括但不限于三角形、方形、棱形等),椭圆形、跑道形或异形等,其中,异形是指前面所列举的形状之外的其它对称或非对称的形状。The shape of the cross section of the air channel 200a located inside the extruded matrix 200 is not limited. For example, the shape of the cross section can be circular, polygonal (including but not limited to triangle, square, prism, etc.), elliptical, racetrack-shaped or irregular, etc., wherein irregular refers to other symmetrical or asymmetrical shapes other than the shapes listed above.

位于挤出基质200的外侧壁上的气道200a横截面的形状可以是半圆形,半椭圆形、多边形或异形等,其中,异形是指前面所列举的形状之外的其它对称或非对称的形状。The cross-sectional shape of the air channel 200a located on the outer side wall of the extruded matrix 200 can be semicircular, semi-elliptical, polygonal or irregular, wherein irregular refers to other symmetrical or asymmetrical shapes other than the shapes listed above.

气道200a用于增大气溶胶生成基质的表面积(气道200a的侧壁相当于是气溶胶生成基质的一部分表面),使作用到气溶胶生成基质的热量能够从气溶胶生成基质的表面进入气溶胶生成基质内部,以提高加热效率。The air channel 200a is used to increase the surface area of the aerosol generating substrate (the side wall of the air channel 200a is equivalent to a part of the surface of the aerosol generating substrate), so that the heat acting on the aerosol generating substrate can enter the interior of the aerosol generating substrate from the surface of the aerosol generating substrate to improve the heating efficiency.

需要说明的是,相关技术中,有一些气溶胶生成基质的内部存在自然形成的微孔,比如,对于颗粒结合体的气溶胶生成基质,颗粒与颗粒之间的间隙构成微孔,但是,本申请所述的气道200a与微孔不同,本申请所述的气道200a属于宏观意义上的孔,微孔属于微观意义上的孔,气道200a的横截面积以及长度等尺寸比微孔大的多。气道200a主要依靠加工而成,因此,气道200a的横截面积以及长度等尺寸可以根据设计要求而改变,而微孔的尺寸由颗粒与颗粒 之间的间隙决定,微孔的横截面积以及长度等尺寸通过挤出工艺的方式自然形成。It should be noted that in the related art, some aerosol generating matrices have naturally formed micropores inside. For example, for the aerosol generating matrix of a particle combination, the gaps between particles constitute micropores. However, the airway 200a described in the present application is different from the micropores. The airway 200a described in the present application is a hole in the macroscopic sense, while the micropores are holes in the microscopic sense. The cross-sectional area and length of the airway 200a are much larger than those of the micropores. The airway 200a is mainly processed. Therefore, the cross-sectional area and length of the airway 200a can be changed according to the design requirements, while the size of the micropores is determined by the size of the particles. The cross-sectional area and length of the micropores are determined by the gap between them, and the dimensions of the micropores are naturally formed by the extrusion process.

一实施例中,常温挤出成型的挤出压力可以为0.5bar~300bar(包含0.5bar和300bar)。In one embodiment, the extrusion pressure of room temperature extrusion molding may be 0.5 bar to 300 bar (inclusive).

本申请实施例所述的挤出压力是指位于挤出机出口处的挤出模具的挤出压力。The extrusion pressure described in the embodiments of the present application refers to the extrusion pressure of the extrusion die located at the outlet of the extruder.

挤出压力对挤出基质的成型形状、表面光滑度、良品率、生产速率都会有影响。当挤出压力低于0.5bar时,挤出基质的成型率低,产品不良率升高,进而导致生产速率减慢,生产成本提升,当挤出压力高于300bar时,挤出机的传动结构负载高(所需提供的扭矩高),从而导致挤出机的使用寿命降低。因此,将挤出压力控制在0.5bar~300bar的范围内,既可以提高挤出基质的成型率,又可以延长挤出机的使用寿命。The extrusion pressure will affect the molding shape, surface smoothness, yield rate, and production rate of the extruded matrix. When the extrusion pressure is lower than 0.5 bar, the molding rate of the extruded matrix is low, and the product defect rate increases, which in turn leads to a slow production rate and increased production costs. When the extrusion pressure is higher than 300 bar, the transmission structure load of the extruder is high (the torque required is high), which leads to a decrease in the service life of the extruder. Therefore, controlling the extrusion pressure within the range of 0.5 bar to 300 bar can not only improve the molding rate of the extruded matrix, but also extend the service life of the extruder.

较优选地,常温挤出成型的挤出压力可以为20bar~80bar(包含20bar和80bar)。Preferably, the extrusion pressure of room temperature extrusion molding can be 20 bar to 80 bar (including 20 bar and 80 bar).

一实施例中,常温挤出成型的挤出方式可以为水平挤出。In one embodiment, the extrusion method of room temperature extrusion molding can be horizontal extrusion.

水平挤出是指挤出机出口处的挤出模具水平设置,挤出基质在水平方向被挤出(比如图2和图3所示的挤出机110),或者说,挤出基质的挤出方向与水平面平行。Horizontal extrusion means that the extrusion die at the extruder outlet is arranged horizontally, and the extruded matrix is extruded in the horizontal direction (such as the extruder 110 shown in Figures 2 and 3), or in other words, the extrusion direction of the extruded matrix is parallel to the horizontal plane.

对于形成螺旋气道的挤出基质,挤出基质在通过挤出机出口处的挤出模具时,挤出模具的口模旋转而挤出基质不旋转,被旋转的口模挤出的挤出基质直接进入输送装置(比如图2和图3中的第一输送装置140),由于口模旋转会使挤出基质产生一定的应力,而水平挤出可以减少挤出基质的应力的直接释放(所产生的应力可通过加热进行消除),因此,水平挤出可以提升具有螺旋气道的气溶胶生成基质的良品率。For the extruded matrix forming a spiral airway, when the extruded matrix passes through the extrusion die at the outlet of the extruder, the die of the extrusion die rotates while the extruded matrix does not rotate, and the extruded matrix extruded by the rotating die directly enters the conveying device (such as the first conveying device 140 in Figures 2 and 3). Since the rotation of the die will cause a certain stress to be generated in the extruded matrix, horizontal extrusion can reduce the direct release of the stress of the extruded matrix (the generated stress can be eliminated by heating). Therefore, horizontal extrusion can improve the yield rate of the aerosol-generating matrix with a spiral airway.

一实施例中,常温挤出成型的挤出方式也可以为垂直挤出。In one embodiment, the extrusion method of room temperature extrusion molding can also be vertical extrusion.

垂直挤出是指挤出机出口处的挤出模具朝下设置,挤出基质沿重力方向被挤出(比如图4和图5所示的挤出机110),或者说,挤出基质的挤出方向与水 平面垂直。Vertical extrusion means that the extrusion die at the extruder outlet is set downward, and the extruded matrix is extruded along the direction of gravity (such as the extruder 110 shown in Figures 4 and 5), or in other words, the extrusion direction of the extruded matrix is parallel to the water. The plane is vertical.

示例性地,请参阅图4和图5,制造设备100可以设置第三输送装置170,挤出基质200从挤出机110中挤出后,直接进入第三输送装置170。Exemplarily, referring to FIG. 4 and FIG. 5 , the manufacturing equipment 100 may be provided with a third conveying device 170 , and the extruded matrix 200 directly enters the third conveying device 170 after being extruded from the extruder 110 .

对于形成直通气道的挤出基质,垂直挤出可以提升良品率,并且降低挤出机的投入成本,另外还可以减少挤出机的占地面积For extruded substrates with straight airways, vertical extrusion can improve the yield rate and reduce the investment cost of the extruder. It can also reduce the floor space of the extruder.

一实施例中,常温挤出成型的挤出方式还可以为倾斜挤出。In one embodiment, the extrusion method of room temperature extrusion molding can also be inclined extrusion.

倾斜挤出是指挤出机出口处的挤出模具倾斜设置,挤出基质的挤出方向与水平面之间的夹角大于0°,且小于90°。Inclined extrusion means that the extrusion die at the extruder outlet is inclined, and the angle between the extrusion direction of the extruded matrix and the horizontal plane is greater than 0° and less than 90°.

倾斜挤出不仅可以减小混合物料的挤出压力,还可以方便其它设备的空间设计。Inclined extrusion can not only reduce the extrusion pressure of the mixed material, but also facilitate the space design of other equipment.

一实施例中,请参阅图6,挤出模具113可以是单模单口模具,即挤出机110出口处的底模1131(图6中未示出底模1131,可参考图7的底模1131)为一个,该底模1131的出料端具有一个口模1132,混合物料200′通过该口模1132后可以形成具有气道200a的挤出基质200。In one embodiment, please refer to Figure 6, the extrusion die 113 can be a single-mold single-mouth die, that is, there is one bottom die 1131 (the bottom die 1131 is not shown in Figure 6, and the bottom die 1131 in Figure 7 can be referred to) at the outlet of the extruder 110, and the discharge end of the bottom die 1131 has a mouth die 1132. After the mixed material 200′ passes through the mouth die 1132, an extruded matrix 200 with an air channel 200a can be formed.

一实施例中,请参阅图7,挤出模具113也可以是单模多口模具,即挤出机110出口处的底模1131为一个,该底模1131的出料端具有多个口模1132,混合物料200′通过多个口模1132后,同时形成多个挤出基质200。当挤出机110的螺杆112的尺寸相对较大时,可选用单模多口模具,如此可提高生产效率,更适用于批量化生产。In one embodiment, please refer to FIG. 7 , the extrusion die 113 may also be a single-mode multi-port die, that is, there is one bottom die 1131 at the outlet of the extruder 110, and the discharge end of the bottom die 1131 has multiple port dies 1132. After the mixed material 200 ′ passes through the multiple port dies 1132, multiple extruded matrices 200 are simultaneously formed. When the size of the screw 112 of the extruder 110 is relatively large, a single-mode multi-port die may be selected, which can improve production efficiency and is more suitable for mass production.

一实施例中,请参阅图8,挤出模具113还可以是多模多口模具,即挤出机110出口处的转接头116连接有多个底模1131,每个底模1131的出料端均设有多个口模1132,混合物料200′通过各个底模1131上的口模1132后,同时形成多个挤出基质200。当挤出机110的螺杆112的尺寸相对较大时,也可以选用多模多口模具,如此可提高生产效率,更适用于批量化生产。In one embodiment, please refer to FIG8 , the extrusion die 113 can also be a multi-mode multi-port die, that is, the adapter 116 at the outlet of the extruder 110 is connected to a plurality of bottom dies 1131, and the discharge end of each bottom die 1131 is provided with a plurality of port dies 1132. After the mixed material 200 ′ passes through the port dies 1132 on each bottom die 1131, a plurality of extruded matrices 200 are simultaneously formed. When the size of the screw 112 of the extruder 110 is relatively large, a multi-mode multi-port die can also be selected, which can improve production efficiency and is more suitable for mass production.

一实施例中,真空环境的绝对压力可以为0kpa~101.325kpa(包含0kpa和101.325kpa)。In one embodiment, the absolute pressure of the vacuum environment may be 0 kPa to 101.325 kPa (including 0 kPa and 101.325 kPa).

绝对压力与水的沸点有正相关关系,即绝对压力越低,则水的沸点越低。 因此,通过控制绝对压力,可以控制挤出基质中水分的沸点,以使干燥后的挤出基质中的含水量能够控制在合适的范围内。There is a positive correlation between absolute pressure and the boiling point of water, that is, the lower the absolute pressure, the lower the boiling point of water. Therefore, by controlling the absolute pressure, the boiling point of the water in the extruded matrix can be controlled so that the water content in the dried extruded matrix can be controlled within a suitable range.

另外,将真空环境的绝对压力设置在0kpa~101.325kpa的范围内,不仅可以有效减少挤出基质中的的水分,还可以尽可能地保留原料中的香气成分及有效物质(例如植物碱、发烟剂等),进而可以保证产品质量。In addition, setting the absolute pressure of the vacuum environment within the range of 0 kPa to 101.325 kPa can not only effectively reduce the moisture in the extruded matrix, but also retain the aroma components and effective substances (such as alkaloids, smoke agents, etc.) in the raw materials as much as possible, thereby ensuring product quality.

较优选地,真空环境的绝对压力可以为4kpa~20kpa(包含4kpa和20kpa)。Preferably, the absolute pressure of the vacuum environment may be 4 kPa to 20 kPa (including 4 kPa and 20 kPa).

一实施例中,经过负压干燥后的挤出基质中的含水量可以为挤出基质的总重量的3%~20%(包含3%和20%)。In one embodiment, the water content of the extruded matrix after negative pressure drying may be 3% to 20% (inclusive) of the total weight of the extruded matrix.

当挤出基质中的含水量低于3%时,在用户的抽吸过程中,气溶胶生成基质所产生的杂气较高,降低用户的抽吸体验,另外,如果干燥后的挤出基质在后续还有其它的处理(即步骤S20不是制造方法的最后一步),则干燥后的挤出基质在后续的处理过程中易碎,由此,不仅会导致后续生产的不良率较高,增加生产成本。当挤出基质中的含水量高于20%时,气溶胶生成基质在加热抽吸过程中的烟气含水量较高,烟气温度不易降低,易使用户在抽吸过程中产生“烫嘴”现象,降低用户的抽吸体验。因此,将干燥后的挤出基质中的含水量控制在挤出基质的总重量的3%~20%的范围内,可以有效地提高用户的抽吸体验,另外,对于干燥后还有它处理的挤出基质,也可以降低后续生产的不良率。When the water content in the extruded matrix is lower than 3%, during the user's suction process, the impurities generated by the aerosol-generating matrix are high, which reduces the user's suction experience. In addition, if the dried extruded matrix is subsequently processed by other methods (i.e., step S20 is not the last step of the manufacturing method), the dried extruded matrix is fragile in the subsequent processing process, which not only leads to a high defect rate in subsequent production, but also increases production costs. When the water content in the extruded matrix is higher than 20%, the smoke water content of the aerosol-generating matrix during the heating and suction process is high, and the smoke temperature is not easy to reduce, which easily causes the user to have a "hot mouth" phenomenon during the suction process, reducing the user's suction experience. Therefore, controlling the water content in the dried extruded matrix within the range of 3% to 20% of the total weight of the extruded matrix can effectively improve the user's suction experience. In addition, for the extruded matrix that is processed by it after drying, the defect rate of subsequent production can also be reduced.

较优选地,经过负压干燥后的挤出基质中的含水量可以为挤出基质的总重量的4%~13%(包含4%和13%)。Preferably, the water content of the extruded matrix after negative pressure drying may be 4% to 13% (including 4% and 13%) of the total weight of the extruded matrix.

一实施例中,可以采用微波加热、电阻加热和红外加热中的至少一种加热方式对挤出基质进行负压干燥。In one embodiment, the extruded matrix may be dried under negative pressure by at least one of microwave heating, resistance heating and infrared heating.

微波加热(Microwave heating)是指利用微波的能量特征对物料进行加热。Microwave heating refers to the use of the energy characteristics of microwaves to heat materials.

电阻加热是指利用电流通过电阻体的热效应对物料进行加热。Resistance heating refers to the use of the thermal effect of electric current passing through a resistor to heat the material.

红外加热是指利用红外线的辐射传热对物料进行加热。Infrared heating refers to the use of infrared radiation heat transfer to heat materials.

根据需要,可以只采用微波加热、电阻加热和红外加热中的一种加热方式,也可以采用微波加热、电阻加热和红外加热中任意两种加热方式的组合,还可以采用微波加热、电阻加热和红外加热这三种加热方式。 According to needs, only one of microwave heating, resistance heating and infrared heating can be used, or a combination of any two of them can be used, or all three of them can be used.

微波加热、电阻加热和红外加热可以使真空环境的温度能够较稳定地保持在所需要的温度,比如真空环境的温度可以保持在大于20℃且小于100℃的范围内,从而可以较好地提高挤出基质的内部温度,激发挤出基质内部的水分子震动。Microwave heating, resistance heating and infrared heating can keep the temperature of the vacuum environment at the required temperature more stably. For example, the temperature of the vacuum environment can be maintained in the range of greater than 20°C and less than 100°C, thereby better increasing the internal temperature of the extruded matrix and stimulating the vibration of water molecules inside the extruded matrix.

需要说明是的,加热方式并不限于微波加热、电阻加热和红外加热,在另一些实施例中,也可以采用其它的加热方式,只要能够对挤出基质进行负压干燥即可。It should be noted that the heating method is not limited to microwave heating, resistance heating and infrared heating. In other embodiments, other heating methods can also be used as long as the extruded matrix can be dried under negative pressure.

一实施例中,所述制造方法还可以包括:将挤出基质分切成设定长度。In one embodiment, the manufacturing method may further include: cutting the extruded matrix into set lengths.

通过常温挤出成型挤出的挤出基质的长度通常相对较长,因此,可以根据不同的使用场景,将挤出基质分切成所需的长度。The length of the extruded matrix extruded by room temperature extrusion molding is usually relatively long, so the extruded matrix can be cut into required lengths according to different usage scenarios.

请参阅图2至图5,制造设备100设置有具有分切工具(图未示出)的分切装置150,挤出基质200通过分切工具完成分切。2 to 5 , the manufacturing equipment 100 is provided with a slitting device 150 having a slitting tool (not shown), and the extruded matrix 200 is slitting by the slitting tool.

分切的方式可以有多种,比如,一实施例中,可以采用分切工具与挤出基质接触的物理接触式分切,也就是说,分切工具直接与挤出基质接触,物理接触式分切包括但不限于旋转滚刀切割、切割片切割、线切割、辊切、挤压等方式。There are many ways of slitting. For example, in one embodiment, physical contact slitting in which the slitting tool contacts the extruded matrix can be used. That is, the slitting tool directly contacts the extruded matrix. Physical contact slitting includes but is not limited to rotary hob cutting, cutting disc cutting, wire cutting, roller cutting, extrusion and the like.

另一实施例中,也可以采用分切工具与挤出基质间隔的非物理接触式分切,也就是说,分切工具本身与挤出基质没有物理上的接触,非物理接触式分切包括但不限于激光切割、等离子切割、空气刀、水刀等方式。In another embodiment, non-physical contact slitting between the slitting tool and the extruded matrix can also be used, that is, the slitting tool itself has no physical contact with the extruded matrix. Non-physical contact slitting includes but is not limited to laser cutting, plasma cutting, air knife, water knife and the like.

一实施例中,可以在对挤出基质进行负压干燥之前,将挤出基质分切成设定长度。也就是说,先将挤出基质分切成设定长度,再对分切后进行负压干燥。In one embodiment, the extruded matrix can be cut into set lengths before the extruded matrix is subjected to negative pressure drying. In other words, the extruded matrix is first cut into set lengths and then subjected to negative pressure drying.

一实施例中,也可以在对挤出基质进行负压干燥之前,对挤出基质进行预分切,在对挤出基质进行负压干燥之后,将预分切的挤出基质分切成设定长度。In one embodiment, the extruded matrix may be pre-cut before the extruded matrix is subjected to negative pressure drying, and the pre-cut extruded matrix may be cut into set lengths after the extruded matrix is subjected to negative pressure drying.

预分切相当于是对挤出基质先进行初次分切,经过预分切的挤出基质的长度比设定长度更长。Pre-slitting is equivalent to the initial slitting of the extruded matrix, and the length of the extruded matrix after pre-slitting is longer than the set length.

示例性地,请参阅图2和图3,对于需要进行预分切的制造设备100,可以设置两个分切装置150,第一个分切装置150设置在真空干燥装置120沿物料 输送方向的上游,第二个分切装置150设置在真空干燥装置120沿物料输送方向的下游,第一个分切装置150用于对挤出基质200进行预分切,第二个分切装置150用于将经过负压干燥之后的挤出基质200分切成设定长度。为了便于在挤出基质200进行负压干燥之后对挤出基质200进行分切,请参阅图2和图3,制造设备100还可以在真空干燥装置120和第二个分切装置150之间设置第二输送装置160,在真空干燥装置120中完成负压干燥的挤出基质200通过第二输送装置160输送至第二个分切装置150处进行分切。For example, referring to FIG. 2 and FIG. 3 , for a manufacturing device 100 that needs to be pre-cut, two cutting devices 150 can be provided. The first cutting device 150 is provided along the material of the vacuum drying device 120. Upstream of the conveying direction, the second slitting device 150 is arranged downstream of the vacuum drying device 120 along the material conveying direction. The first slitting device 150 is used to pre-slit the extruded matrix 200, and the second slitting device 150 is used to slit the extruded matrix 200 after negative pressure drying into set lengths. In order to facilitate slitting the extruded matrix 200 after negative pressure drying, please refer to Figures 2 and 3. The manufacturing equipment 100 can also be provided with a second conveying device 160 between the vacuum drying device 120 and the second slitting device 150. The extruded matrix 200 that has completed negative pressure drying in the vacuum drying device 120 is conveyed to the second slitting device 150 by the second conveying device 160 for slitting.

通过常温挤出成型挤出的挤出基质的质地通常相对较软,因此,在挤出基质进行负压干燥之前,对挤出基质进行的预分切相当于是对挤出基质的软体进行分切。The texture of the extruded matrix extruded by room temperature extrusion molding is usually relatively soft. Therefore, before the extruded matrix is subjected to negative pressure drying, pre-slitting of the extruded matrix is equivalent to slitting the soft body of the extruded matrix.

预分切的挤出基质经过负压干燥之后,挤出基质中的水分脱除,挤出基质硬化,因此,在负压干燥之后,对预分切的挤出基质进行的分切相当于是对质地相对较硬的挤出基质进行分切。After the pre-cut extruded matrix is dried under negative pressure, the moisture in the extruded matrix is removed and the extruded matrix hardens. Therefore, after the negative pressure drying, the cutting of the pre-cut extruded matrix is equivalent to cutting of the extruded matrix with a relatively hard texture.

在挤出基质进行负压干燥的过程中,挤出基质的体积会发生收缩,因此,采用预分切—负压干燥—分切的方式可以提高切割后的挤出基质的纵向尺寸(即沿挤出方向上的尺寸)的一致性,进而可以提高分切的良品率。During the negative pressure drying process of the extruded matrix, the volume of the extruded matrix will shrink. Therefore, the pre-slitting-negative pressure drying-slitting method can improve the consistency of the longitudinal dimension (i.e., the dimension along the extrusion direction) of the extruded matrix after cutting, thereby improving the slitting yield.

另外,对于需要进行预分切的挤出基质,还可以在预分切之后对挤出基质进行校形。In addition, for an extruded matrix that needs to be pre-cut, the extruded matrix can also be shaped after the pre-cut.

示例性地,挤出基质经过预分切之后,可以先采用治具对挤出基质进行圆周校形,再对校形后的挤出基质进行负压干燥。For example, after the extruded matrix is pre-cut, a jig may be used to circumferentially align the extruded matrix, and then the shaped extruded matrix may be dried under negative pressure.

示例性地,也可以在挤出基质经过负压干燥之后,且在将挤出基质分切成设定长度之前采用治具对挤出基质进行圆周和直线度校形。For example, after the extruded matrix is dried under negative pressure and before the extruded matrix is cut into set lengths, a jig may be used to calibrate the circumference and straightness of the extruded matrix.

一实施例中,也可以在对挤出基质进行负压干燥之后,将挤出基质分切成设定长度。也就是说,先对挤出基质进行负压干燥,再将挤出基质分切成设定长度,与具有预分切的制造方法相比,该实施例实际上就是省略了预分切的步骤。In one embodiment, the extruded matrix can also be cut into set lengths after the extruded matrix is dried under negative pressure. That is, the extruded matrix is first dried under negative pressure and then cut into set lengths. Compared with the manufacturing method with pre-cutting, this embodiment actually omits the pre-cutting step.

示例性地,以图2所示的制造设备100为例,对于本实施例的制造方法, 可以只在真空干燥装置120沿物料输送方向的下游设置一个分切装置150,而真空干燥装置120沿物料输送方向的上游不设置分切装置150,挤出基质200进行负压干燥之前不进行任何分切,在对挤出基质200进行负压干燥之后,再利用分切装置150将挤出基质200分切成设定长度。For example, taking the manufacturing device 100 shown in FIG. 2 as an example, for the manufacturing method of this embodiment, Only one slitting device 150 may be provided downstream of the vacuum drying device 120 along the material conveying direction, while no slitting device 150 may be provided upstream of the vacuum drying device 120 along the material conveying direction. No slitting is performed on the extruded matrix 200 before the negative pressure drying. After the extruded matrix 200 is subjected to negative pressure drying, the slitting device 150 is used to cut the extruded matrix 200 into set lengths.

通过常温挤出成型挤出的挤出基质的质地通常相对较软,因此,先将挤出基质进行负压干燥,再对挤出基质进行分切,可以防止负压干燥前的分切对硬度较小的挤出基质造成微小变形。The texture of the extruded matrix extruded by room temperature extrusion molding is usually relatively soft. Therefore, the extruded matrix is first subjected to negative pressure drying and then cut to prevent the cutting before negative pressure drying from causing slight deformation to the extruded matrix with lower hardness.

需要说明的是,对于没有预分切的任意一种分切方式,也可以在分切之前采用治具对挤出基质进行圆周和直线度校形。It should be noted that, for any slitting method without pre-slitting, a jig can also be used to calibrate the circumference and straightness of the extruded matrix before slitting.

在一些实施例中,也可以没有分切的步骤,也就是说,可以通过常温挤出成型直接挤出设定长度的挤出基质,比如,当挤出基质通过垂直挤出的方式挤出之后,挤出基质可以在达到或接近设定长度时,在自身重力作用下自然脱离,从而可以减少后续的分切步骤,进而可以降低生产成本。In some embodiments, there may be no slitting step, that is, the extruded matrix of a set length can be directly extruded by room temperature extrusion molding. For example, after the extruded matrix is extruded by vertical extrusion, the extruded matrix can naturally detach under the action of its own gravity when it reaches or approaches the set length, thereby reducing the subsequent slitting steps and further reducing the production cost.

一实施例中,在对挤出基质进行负压干燥之前,制造方法还包括:对挤出基质进行冷却硬化。In one embodiment, before the extruded matrix is subjected to negative pressure drying, the manufacturing method further comprises: cooling and hardening the extruded matrix.

由于通过常温挤出成型挤出的挤出基质的质地通常相对较软,因此,为了便于后续的处理,可以在进行负压干燥之前,对挤出基质进行冷却硬化,以提高挤出基质的硬度。Since the texture of the extruded matrix extruded by room temperature extrusion molding is usually relatively soft, in order to facilitate subsequent processing, the extruded matrix can be cooled and hardened before negative pressure drying to increase the hardness of the extruded matrix.

在进行冷却硬化之后,挤出基质的硬度提高,挤出基质的温度也会降低。After cooling and hardening, the hardness of the extruded matrix increases and the temperature of the extruded matrix decreases.

示例性地,通过常温挤出成型挤出的挤出基质在进行冷却硬化之前的硬度可以为0HB~100HB(包含0HB和100HB),经过冷却硬化之后,挤出基质的硬度可以为1HB~200HB(包含1HB和200HB)。For example, the hardness of the extruded matrix extruded by room temperature extrusion molding before cooling and hardening may be 0HB to 100HB (including 0HB and 100HB), and after cooling and hardening, the hardness of the extruded matrix may be 1HB to 200HB (including 1HB and 200HB).

较优选地,通过常温挤出成型挤出的挤出基质在进行冷却硬化之前的硬度可以为1HB~60HB(包含1HB和60HB),经过冷却硬化之后,挤出基质的硬度可以为40HB~120HB(包含40HB和120HB)。Preferably, the hardness of the extruded matrix extruded by room temperature extrusion molding before cooling and hardening can be 1HB to 60HB (including 1HB and 60HB), and after cooling and hardening, the hardness of the extruded matrix can be 40HB to 120HB (including 40HB and 120HB).

示例性地,挤出基质进行冷却硬化之前的温度可以为0℃~40℃(包含0℃和40℃),经过冷却硬化之后,挤出基质的温度可以为-50℃~5℃(包含-50℃和 5℃)。For example, the temperature of the extruded matrix before cooling and hardening may be 0°C to 40°C (including 0°C and 40°C), and the temperature of the extruded matrix after cooling and hardening may be -50°C to 5°C (including -50°C and 5℃).

对于具有分切步骤的制造方法,可以在对挤出基质进行冷却硬化之后再将挤出基质分切成设定长度。For the manufacturing method having the slitting step, the extruded matrix may be slit into set lengths after the extruded matrix is cooled and hardened.

示例性地,请参阅图2和图3,制造设备100可以设置硬化装置130和两个分切装置150。硬化装置130设置在挤出机110和真空干燥装置120之间,以用于在进行负压干燥之前对挤出基质200进行冷却硬化。两个分切装置150的其中之一设置在硬化装置130与真空干燥装置120之间,以用于在进行负压干燥之前,对经过冷却硬化的挤出基质200进行预分切。两个分切装置150的其中另一设置在真空干燥装置120沿物料输送方向的下游,以用于将经过负压干燥的挤出基质200分切成设定长度。Exemplarily, referring to Fig. 2 and Fig. 3, the manufacturing equipment 100 can be provided with a hardening device 130 and two slitting devices 150. The hardening device 130 is arranged between the extruder 110 and the vacuum drying device 120, so as to cool and harden the extruded matrix 200 before negative pressure drying. One of the two slitting devices 150 is arranged between the hardening device 130 and the vacuum drying device 120, so as to pre-slit the extruded matrix 200 after cooling and hardening before negative pressure drying. The other of the two slitting devices 150 is arranged downstream of the vacuum drying device 120 along the material conveying direction, so as to cut the extruded matrix 200 after negative pressure drying into set lengths.

示例性地,请参阅图4和图5,制造设备100也可以只在硬化装置130和真空干燥装置120之间设置分切装置150,真空干燥装置120沿物料输送方向的下游不设置分切装置150,设置在硬化装置130与真空干燥装置120之间的分切装置150用于在进行负压干燥之前,将经过冷却硬化的挤出基质200分切成设定长度,也就是说,挤出基质200经过冷却硬化之后,可以直接分切成设定长度,而不需要进行预分切。For example, referring to Figures 4 and 5, the manufacturing equipment 100 may also only set the slitting device 150 between the hardening device 130 and the vacuum drying device 120, and no slitting device 150 is set downstream of the vacuum drying device 120 along the material conveying direction. The slitting device 150 set between the hardening device 130 and the vacuum drying device 120 is used to cut the cooled and hardened extruded matrix 200 into set lengths before negative pressure drying. That is to say, after the extruded matrix 200 is cooled and hardened, it can be directly cut into set lengths without pre-cutting.

由于挤出基质进行冷却硬化之后,挤出基质的硬度会提高,因此,挤出基质进行冷却硬化之后,挤出基质更易于分切,且分切后的挤出基质不会产生形变,切割面更加整齐、完整。Since the hardness of the extruded matrix increases after cooling and hardening, the extruded matrix is easier to cut after cooling and hardening, and the extruded matrix after cutting will not be deformed, and the cut surface is more neat and complete.

一实施例中,冷却硬化可以是将挤出基质置入低温环境中进行冷却,其中,低温环境的温度低于挤出基质的硬化温度。In one embodiment, the cooling and hardening may be placing the extruded matrix in a low-temperature environment for cooling, wherein the temperature of the low-temperature environment is lower than the hardening temperature of the extruded matrix.

低温环境的温度是指提供低温环境的装置内的环境温度。The temperature of the low-temperature environment refers to the ambient temperature within a device that provides the low-temperature environment.

也就是说,可以将挤出基质传送至温度较低的低温环境中进行冷却,为了满足硬化要求,低温环境中的温度需要低于挤出基质的硬化温度。That is, the extruded matrix can be transferred to a low-temperature environment with a relatively low temperature for cooling. In order to meet the hardening requirements, the temperature in the low-temperature environment needs to be lower than the hardening temperature of the extruded matrix.

示例性地,在满足低温环境中的温度低于挤出基质的硬化温度的前提下,如果挤出基质的硬化温度为-100℃~60℃(包含-100℃和60℃),则低温环境的温度可以为-270℃~60℃(包含-270℃和60℃)。 Exemplarily, under the premise that the temperature in the low-temperature environment is lower than the hardening temperature of the extruded matrix, if the hardening temperature of the extruded matrix is -100°C to 60°C (including -100°C and 60°C), the temperature of the low-temperature environment can be -270°C to 60°C (including -270°C and 60°C).

较优选地,如果挤出基质的硬化温度为-30℃~40℃(包含-30℃和40℃),则低温环境的温度可以为-100℃~40℃(包含-100℃和40℃)。More preferably, if the hardening temperature of the extruded matrix is -30°C to 40°C (inclusive), the temperature of the low temperature environment may be -100°C to 40°C (inclusive).

一实施例中,冷却硬化也可以是利用冷媒对挤出基质进行冷却。冷媒的形态可以是液体,比如液氮或液化空气,也可以是气体或固体。In one embodiment, the cooling and hardening may also be performed by cooling the extruded matrix using a refrigerant. The refrigerant may be in the form of a liquid, such as liquid nitrogen or liquefied air, or a gas or a solid.

示例性地,可以将挤出基质与冷媒进行直接换热。For example, the extruded substrate may be directly heat exchanged with a refrigerant.

直接换热是指换热介质之间通过直接接触进行热交换。也就是说,挤出基质与冷媒直接接触。比如,请参阅图10和图11,硬化装置130可以设置冷媒供应器(图未示出)和具有容纳腔131a的容器131,容纳腔131a具有贯穿容器131相对两侧的传送通道131c以及与容纳腔131a连通的进液槽131b,从挤出机110中挤出的挤出基质200通过该传送通道131c进入容纳腔131a,冷媒供应器将液态的冷媒注入进液槽131b,冷媒通过进液槽131b进入容纳腔131a内并与容纳腔131a内的挤出基质200接触进行换热。Direct heat exchange refers to heat exchange between heat exchange media through direct contact. That is, the extruded matrix is in direct contact with the refrigerant. For example, referring to Figures 10 and 11, the hardening device 130 can be provided with a refrigerant supplier (not shown) and a container 131 having a receiving chamber 131a, the receiving chamber 131a having a transmission channel 131c running through opposite sides of the container 131 and a liquid inlet 131b connected to the receiving chamber 131a, the extruded matrix 200 extruded from the extruder 110 enters the receiving chamber 131a through the transmission channel 131c, the refrigerant supplier injects the liquid refrigerant into the liquid inlet 131b, the refrigerant enters the receiving chamber 131a through the liquid inlet 131b and contacts with the extruded matrix 200 in the receiving chamber 131a for heat exchange.

另外,请参阅图10和图11,当挤出模具113可以同时挤出多个挤出基质200时,由于刚挤出的挤出基质200的硬度较低,为了防止多个挤出基质200黏在一起,可以在挤出模具113的模口外设置具有多个导槽140a的第一输送装置140,第一输送装置140穿过传送通道131c,以分别引导各个挤出基质200通过传送通道131c进入容纳腔131a内进行冷却硬化。In addition, please refer to Figures 10 and 11. When the extrusion die 113 can extrude multiple extrusion matrices 200 at the same time, since the hardness of the extrusion matrix 200 just extruded is relatively low, in order to prevent the multiple extrusion matrices 200 from sticking together, a first conveying device 140 having multiple guide grooves 140a can be provided outside the die mouth of the extrusion die 113. The first conveying device 140 passes through the conveying channel 131c to guide each extrusion matrix 200 through the conveying channel 131c into the accommodating cavity 131a for cooling and hardening.

挤出基质与冷媒进行直接换热的好处在于,可以较快速地冷却硬化换热介质的表面,以使挤出基质能够保持形态的稳定性,进而可以便于连续化生产,提高生产效率。示例性地,也可以将挤出基质与冷媒进行间接换热。The advantage of direct heat exchange between the extruded matrix and the refrigerant is that the surface of the hardened heat exchange medium can be cooled more quickly so that the extruded matrix can maintain the stability of the shape, thereby facilitating continuous production and improving production efficiency. For example, the extruded matrix can also be indirectly heat exchanged with the refrigerant.

间接换热是指换热介质之间在进行热交换的过程中不直接接触。也就是说,挤出基质与冷媒不会直接接触,而是通过中间件进行间接换热。比如,请参阅图12,硬化装置130可以包括冷却管132,冷却管132包括内管1321和外管1322,内管1321和外管1322之间形成用于储存冷媒的储液腔132a,内管1321具有贯穿的换热通道1321a,从挤出机110挤出的挤出基质200进入换热通道1321a并与内管1321接触进行热交换,吸收了挤出基质200的热量的内管1321再与冷媒进行热交换,相当于挤出基质200与冷媒之间通过内管1321进行间接 换热。Indirect heat exchange means that the heat exchange media are not in direct contact with each other during the heat exchange process. That is to say, the extruded matrix and the refrigerant will not be in direct contact, but will be indirectly heat exchanged through an intermediate piece. For example, referring to FIG. 12 , the hardening device 130 may include a cooling tube 132, and the cooling tube 132 includes an inner tube 1321 and an outer tube 1322. A liquid storage chamber 132a for storing the refrigerant is formed between the inner tube 1321 and the outer tube 1322. The inner tube 1321 has a heat exchange channel 1321a extending therethrough. The extruded matrix 200 extruded from the extruder 110 enters the heat exchange channel 1321a and contacts the inner tube 1321 for heat exchange. The inner tube 1321 that absorbs the heat of the extruded matrix 200 then exchanges heat with the refrigerant, which is equivalent to indirect heat exchange between the extruded matrix 200 and the refrigerant through the inner tube 1321. Heat exchange.

需要说明的是,内管1321形成换热通道1321a的内表面一般为光滑表面,比如,内管1321内表面的粗糙度可以为Ra1.2μm~Ra0.08μm(包含Ra1.2μm和Ra0.08μm),光滑的与内表面与挤出基质200的外表面之间的摩擦力较小,不会导致挤出基质200变形。It should be noted that the inner surface of the inner tube 1321 forming the heat exchange channel 1321a is generally a smooth surface. For example, the roughness of the inner surface of the inner tube 1321 can be Ra1.2μm~Ra0.08μm (including Ra1.2μm and Ra0.08μm). The friction between the smooth inner surface and the outer surface of the extruded matrix 200 is small, and will not cause deformation of the extruded matrix 200.

挤出基质与冷媒进行间接换热的好处在于,可以有效避免挤出基质直接与冷媒接触而可能出现的膨胀形变、开裂等问题。The advantage of indirect heat exchange between the extruded matrix and the refrigerant is that it can effectively avoid problems such as expansion deformation, cracking, etc. that may occur when the extruded matrix directly contacts the refrigerant.

在一些实施例中,也可以没有冷却硬化的步骤,比如,在一种制造方法中,挤出基质挤出之后,在进行负压干燥之前,可以只进行分切,而不进行冷却硬化。对于设定长度相对较短的挤出基质,通过分切产生的微量变形对后续的生产无影响,因此,可以省略冷却硬化的步骤。In some embodiments, there may be no cooling and hardening step. For example, in a manufacturing method, after the extruded matrix is extruded, before the negative pressure drying, only slitting may be performed without cooling and hardening. For an extruded matrix with a relatively short set length, the slight deformation caused by slitting has no effect on subsequent production, and therefore, the cooling and hardening step may be omitted.

一实施例中,混合物料的组分包括固料和液料,在对混合物料进行常温挤出成型之前,所述制造方法还可以包括:将固料和液料分成两个模块分别进行喂料。In one embodiment, the components of the mixed material include solid material and liquid material. Before the mixed material is subjected to room temperature extrusion molding, the manufacturing method may further include: dividing the solid material and the liquid material into two modules and feeding them separately.

固料是指固态的物料,液料是指液态的物料。也就是说,混合物料中的一部分组分为固体,一部分组分为液体,固料和液料混合后形成混合物料。Solid material refers to solid material, and liquid material refers to liquid material. That is to say, part of the components in the mixed material are solid, and part of the components are liquid. The solid material and the liquid material are mixed to form a mixed material.

需要说明的是,固料和液料混合后形成的混合物料是均一形态,不能再分为固料和液料。It should be noted that the mixed material formed after the solid material and the liquid material are mixed is in a uniform form and can no longer be divided into solid material and liquid material.

示例性地,以植物原料、助剂原料和粘合剂原料为固料,发烟剂原料和香料原料为液料为例,可以将植物原料、助剂原料和粘合剂原料等固料以及发烟剂原料和香料原料等液料分别添加至挤出机的料筒内,以使固料和液料在挤出机的料筒内进行混合。For example, taking plant raw materials, auxiliary raw materials and adhesive raw materials as solid materials and smoke agent raw materials and flavor raw materials as liquid materials, the solid materials such as plant raw materials, auxiliary raw materials and adhesive raw materials and the liquid materials such as smoke agent raw materials and flavor raw materials can be added into the barrel of the extruder respectively, so that the solid materials and the liquid materials are mixed in the barrel of the extruder.

将固料和液料分成两个模块分别进行喂料的好处在于,可以降低混合物料前处理成本,保证生产过程的连续性,在提高生产效率的同时,也可以提高产品的一致性及均匀性。The advantage of dividing the solid material and liquid material into two modules for feeding separately is that it can reduce the pre-treatment cost of the mixed material, ensure the continuity of the production process, and improve the consistency and uniformity of the product while improving production efficiency.

进一步地,将固料和液料分成两个模块分别进行喂料,可以包括以下步骤:添加固料;当固料沿物料输送方向移动至液料的添加位置,向固料中添加液料。 Furthermore, dividing the solid material and the liquid material into two modules for feeding separately may include the following steps: adding the solid material; when the solid material moves along the material conveying direction to the liquid material adding position, adding the liquid material to the solid material.

也就是说,先向挤出机中添加固料,固料进入挤出机的料筒后,会沿物料输送方向向挤出模具所在的方向移动,当固料沿物料输送方向移动至液料的添加位置时,再向挤出机中添加液料,以使液料与固料在挤出机的料筒内进行混合。That is to say, solid material is first added to the extruder. After the solid material enters the barrel of the extruder, it will move along the material conveying direction toward the direction of the extrusion die. When the solid material moves along the material conveying direction to the liquid material adding position, liquid material is added to the extruder to mix the liquid material and the solid material in the barrel of the extruder.

另外,还可以根据挤出机的生产速度、混合物料各原料的比例来确定加料量及加料速度。In addition, the feeding amount and feeding speed can be determined according to the production speed of the extruder and the ratio of each raw material in the mixed material.

示例性地,请参阅图2至图5,可以在挤出机110上设置与挤出机110的料筒111连通的固料加料口114和液料加料口115,液料加料口115位于固料加料口114沿物料输送方向的下游。Exemplarily, referring to FIG. 2 to FIG. 5 , a solid material feeding port 114 and a liquid material feeding port 115 connected to the barrel 111 of the extruder 110 may be provided on the extruder 110 , and the liquid material feeding port 115 is located downstream of the solid material feeding port 114 along the material conveying direction.

固料加料口114的数量可以是一个,也可以是多个,当设置有多个固料加料口114时,各固料加料口114可以分别添加相同的固料,也可以分别添加不同的固料。The number of the solid material feeding ports 114 may be one or more. When a plurality of solid material feeding ports 114 are provided, each solid material feeding port 114 may be used to add the same solid material or different solid materials.

同样地,液料加料口115的数量可以是一个,也可以是多个,当设置有多个液料加料口115时,各液料加料口115可以分别添加相同的液料,也可以分别添加不同的液料。Similarly, the number of the liquid material feeding ports 115 may be one or more. When multiple liquid material feeding ports 115 are provided, each liquid material feeding port 115 may be used to add the same liquid material or different liquid materials.

另外,无论是多个固料加料口114,还是多个液料加料口115,都可以设置成可拆卸的结构,以便于按需要的数量装配固料加料口114和液料加料口115。In addition, whether it is a plurality of solid material feeding ports 114 or a plurality of liquid material feeding ports 115, they can be arranged into a detachable structure so as to facilitate the assembly of the solid material feeding ports 114 and the liquid material feeding ports 115 according to the required number.

由于挤出机主要是依靠螺杆的转动来传送混合物料,而螺杆与挤出机的料筒的内壁之间不是完全密封的,也就是说,螺杆与挤出机的料筒的内壁之间具有缝隙,如果先添加液料,则液料容易从缝隙处泄漏,因此,先添加固料,且在固料沿物料输送方向移动至液料的添加位置时再添加液料,可以较好地避免液料泄漏。Since the extruder mainly relies on the rotation of the screw to convey the mixed material, and the screw and the inner wall of the extruder barrel are not completely sealed, that is, there is a gap between the screw and the inner wall of the extruder barrel. If the liquid material is added first, the liquid material will easily leak from the gap. Therefore, adding the solid material first, and then adding the liquid material when the solid material moves along the material conveying direction to the liquid material adding position, can better avoid liquid leakage.

在一些实施例中,也可以不将混合物料按固料和液料分别进行喂料,比如,可以先将固料和液料进行混合形成混合物料(简称混合浆料喂料),再将混合物料添加至挤出机的料筒内。In some embodiments, the mixed material may not be fed separately as a solid material and a liquid material. For example, the solid material and the liquid material may be mixed first to form a mixed material (referred to as mixed slurry feeding), and then the mixed material is added to the barrel of the extruder.

混合浆料喂料的好处是混合物料具有较好的一致性,可保证产品均一稳定。The advantage of mixed slurry feeding is that the mixed material has better consistency, which can ensure the uniformity and stability of the product.

另外,请参阅图3和图5,对于混合浆料喂料,加料口(采用混合浆料喂 料时,图3和图5中的固料加料口114就相当于是加料口)处还可以另外设置一个螺杆112,以对混合浆料进行进一步均质。In addition, please refer to Figures 3 and 5. For mixed slurry feeding, the feed port (using mixed slurry feeding) When the solid material feeding port 114 in FIG. 3 and FIG. 5 is equivalent to the feeding port), a screw 112 may be further provided at the feeding port to further homogenize the mixed slurry.

一实施例中,在对挤出基质进行负压干燥之后,制造方法还可以包括:在挤出基质的外表面包裹包装层。In one embodiment, after the extruded matrix is subjected to negative pressure drying, the manufacturing method may further include: wrapping a packaging layer on the outer surface of the extruded matrix.

包装层包括但不限于卷烟纸、纸管、锡箔纸等介质耗材,包裹了包装层的挤出基质就相当于是气溶胶生成基质的成品。The packaging layer includes but is not limited to medium consumables such as cigarette paper, paper tubes, and tin foil. The extruded matrix wrapped with the packaging layer is equivalent to the finished product of the aerosol generating matrix.

在一些实施方式中,包裹了包装层的挤出基质还可以与其它的功能段,比如降温段、过滤段等组合,以形成气溶胶生成制品。In some embodiments, the extruded matrix wrapped with the packaging layer may also be combined with other functional segments, such as a cooling segment, a filtering segment, etc., to form an aerosol generating product.

另一实施例中,在对挤出基质进行负压干燥之后,制造方法还可以包括:对挤出基质进行密封包装。In another embodiment, after the extruded matrix is dried under negative pressure, the manufacturing method may further include: sealing and packaging the extruded matrix.

也就是说,也可以不在挤出基质的外表面包裹包装层,而是直接将挤出基质进行密封包装,比如,可以将挤出基质封装在泡罩包装容器内。密封包装后的挤出基质也相当于是气溶胶生成基质的成品。进行密封包装的挤出基质在拆除包装后可以直接在电子雾化装置上使用。That is to say, instead of wrapping the outer surface of the extruded matrix with a packaging layer, the extruded matrix can be directly sealed and packaged, for example, the extruded matrix can be encapsulated in a blister packaging container. The sealed and packaged extruded matrix is also equivalent to a finished product of the aerosol-generating matrix. The sealed and packaged extruded matrix can be directly used on the electronic atomization device after removing the packaging.

下面通过不同的实施例分别说明本申请几种可行的制造方法。需要说明的是,以下各实施例主要是为了说明几种可行的制造方法之间的差异,各实施例中各步骤的具体方法与前面的实施例相同,在此不再赘述。The following are several feasible manufacturing methods of the present application respectively described by different embodiments. It should be noted that the following embodiments are mainly for illustrating the differences between several feasible manufacturing methods, and the specific method of each step in each embodiment is the same as that in the previous embodiment, which will not be repeated here.

实施例一Embodiment 1

请参阅图16,实施例一的制造方法主要包括以下步骤:Please refer to FIG. 16 , the manufacturing method of the first embodiment mainly includes the following steps:

步骤S01a:喂料;Step S01a: feeding;

步骤S02a:常温挤出成型;Step S02a: extrusion molding at room temperature;

步骤S03a:冷却硬化;Step S03a: cooling and hardening;

步骤S04a:分切;Step S04a: cutting;

步骤S05a:负压干燥;Step S05a: negative pressure drying;

步骤S06a:包装。Step S06a: Packaging.

实施例二Embodiment 2

请参阅图17,实施例二的制造方法主要包括以下步骤: Please refer to FIG. 17 , the manufacturing method of the second embodiment mainly includes the following steps:

步骤S01b:喂料;Step S01b: feeding;

步骤S02b:常温挤出成型;Step S02b: extrusion molding at room temperature;

步骤S03b:分切;Step S03b: cutting;

步骤S04b:负压干燥;Step S04b: negative pressure drying;

步骤S05b:包装。Step S05b: Packaging.

与实施例一的制造方法相比,实施例二的制造方法没有冷却硬化的步骤。Compared with the manufacturing method of the first embodiment, the manufacturing method of the second embodiment does not have a cooling and hardening step.

实施例三Embodiment 3

请参阅图18,实施例三的制造方法主要包括以下步骤:Please refer to FIG. 18 , the manufacturing method of the third embodiment mainly includes the following steps:

步骤S01c:喂料;Step S01c: feeding;

步骤S02c:常温挤出成型;Step S02c: extrusion molding at room temperature;

步骤S03c:预分切;Step S03c: pre-cutting;

步骤S04c:负压干燥;Step S04c: negative pressure drying;

步骤S05c:分切;Step S05c: cutting;

步骤S06c:包装。Step S06c: Packaging.

与实施例一的制造方法相比,实施例三的制造方法没有冷却硬化的步骤,且实施例三的分切包括负压干燥之前的预分切以及负压干燥之后的分切。Compared with the manufacturing method of the first embodiment, the manufacturing method of the third embodiment does not have a cooling and hardening step, and the slitting in the third embodiment includes pre-slitting before negative pressure drying and slitting after negative pressure drying.

实施例四Embodiment 4

请参阅图19,实施例四的制造方法主要包括以下步骤:Please refer to FIG. 19 , the manufacturing method of the fourth embodiment mainly includes the following steps:

步骤S01d:喂料;Step S01d: feeding;

步骤S02d:常温挤出成型;Step S02d: extrusion molding at room temperature;

步骤S03d:负压干燥;Step S03d: negative pressure drying;

步骤S04d:包装。Step S04d: Packaging.

与实施例一的制造方法相比,实施例四的制造方法没有冷却硬化和分切的步骤。Compared with the manufacturing method of the first embodiment, the manufacturing method of the fourth embodiment does not have the steps of cooling, hardening and slitting.

在本申请的描述中,参考术语“一实施例中”、“在一些实施例中”、“另一些实施例中”、“又一些实施例中”、或“示例性”等的描述意指结合该实施例或示例描述的具体特征、结构、材料或者特点包含于本申请实施例的至少一个实施例 或示例中。在本申请中,对上述术语的示意性表述不是必须针对的是相同的实施例或示例。而且,描述的具体特征、结构、材料或者特点可以在任一个或多个实施例或示例中以合适的方式结合。此外,在不相互矛盾的情况下,本领域的技术人员可以将本申请中描述的不同实施例或示例以及不同实施例或示例的特征进行结合。In the description of the present application, the reference terms "in one embodiment", "in some embodiments", "in other embodiments", "in yet other embodiments", or "exemplary" etc. mean that the specific features, structures, materials or characteristics described in conjunction with the embodiment or example are included in at least one embodiment of the present application. or examples. In this application, the schematic representations of the above terms do not necessarily refer to the same embodiment or example. Moreover, the specific features, structures, materials or characteristics described can be combined in any one or more embodiments or examples in a suitable manner. In addition, those skilled in the art can combine different embodiments or examples described in this application and the features of different embodiments or examples without contradiction.

以上所述仅为本申请的较佳实施例而已,并不用于限制本申请,对于本领域的技术人员来说,本申请可以有各种更改和变化。凡在本申请的精神和原则之内,所作的任何修改、等同替换、改进等,均包含在本申请的保护范围之内。 The above description is only a preferred embodiment of the present application and is not intended to limit the present application. For those skilled in the art, the present application may have various modifications and variations. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present application are included in the protection scope of the present application.

Claims (24)

一种气溶胶生成基质的制造方法,所述制造方法包括:A method for manufacturing an aerosol generating substrate, the method comprising: 对混合物料进行常温挤出成型,以使所述混合物料形成挤出基质;Extruding the mixed material at room temperature to form an extrusion matrix; 在真空环境中对所述挤出基质进行负压干燥。The extruded matrix is dried under negative pressure in a vacuum environment. 根据权利要求1所述的制造方法,所述常温挤出成型的挤出温度为10℃~90℃;和/或,According to the manufacturing method of claim 1, the extrusion temperature of the room temperature extrusion molding is 10°C to 90°C; and/or, 所述真空环境的温度大于20℃且小于100℃;和/或,The temperature of the vacuum environment is greater than 20° C. and less than 100° C.; and/or, 所述真空环境的绝对压力为0kpa~101.325kpa;和/或,The absolute pressure of the vacuum environment is 0 kPa to 101.325 kPa; and/or, 所述常温挤出成型的挤出压力为0.5bar~300bar。The extrusion pressure of the room temperature extrusion molding is 0.5 bar to 300 bar. 根据权利要求2所述的制造方法,所述挤出温度为35℃~70℃;和/或,The manufacturing method according to claim 2, wherein the extrusion temperature is 35°C to 70°C; and/or, 所述绝对压力为4kpa~20kpa;和/或,The absolute pressure is 4 kPa to 20 kPa; and/or, 所述挤出压力为20bar~80bar。The extrusion pressure is 20 bar to 80 bar. 根据权利要求1-3任意一项所述的制造方法,所述常温挤出成型的挤出方式为水平挤出、垂直挤出和倾斜挤出中的一种。According to the manufacturing method according to any one of claims 1 to 3, the extrusion method of the room temperature extrusion molding is one of horizontal extrusion, vertical extrusion and inclined extrusion. 根据权利要求1-3任意一项所述的制造方法,对所述挤出基质进行负压干燥,包括:According to any one of claims 1 to 3, the extruded matrix is subjected to negative pressure drying, comprising: 采用微波加热、电阻加热和红外加热中的至少一种加热方式对所述挤出基质进行负压干燥。The extruded matrix is dried under negative pressure by using at least one heating method selected from microwave heating, resistance heating and infrared heating. 根据权利要求1-3任意一项所述的制造方法,所述制造方法还包括:The manufacturing method according to any one of claims 1 to 3, further comprising: 将所述挤出基质分切成设定长度。The extruded matrix is slit into set lengths. 根据权利要求6所述的制造方法,所述将所述挤出基质分切成设定长度,包括:The manufacturing method according to claim 6, wherein the step of slitting the extruded matrix into set lengths comprises: 在对所述挤出基质进行所述负压干燥之前,将所述挤出基质分切成所 述设定长度;或,Before the extruded matrix is subjected to the negative pressure drying, the extruded matrix is cut into said set length; or, 在对所述挤出基质进行所述负压干燥之前,对所述挤出基质进行预分切,在对所述挤出基质进行所述负压干燥之后,将预分切的所述挤出基质分切成所述设定长度。Before the extruded matrix is subjected to the negative pressure drying, the extruded matrix is pre-cut, and after the extruded matrix is subjected to the negative pressure drying, the pre-cut extruded matrix is cut into the set length. 根据权利要求6所述的制造方法,分切的方式为分切工具与所述挤出基质接触的物理接触式分切;或,分切的方式为分切工具与所述挤出基质间隔的非物理接触式分切。According to the manufacturing method of claim 6, the slitting method is physical contact slitting in which the slitting tool is in contact with the extruded matrix; or, the slitting method is non-physical contact slitting in which the slitting tool is spaced from the extruded matrix. 根据权利要求1-3任意一项所述的制造方法,在对所述挤出基质进行所述负压干燥之前,所述制造方法还包括:According to any one of claims 1 to 3, before the extruded matrix is subjected to the negative pressure drying, the manufacturing method further comprises: 对所述挤出基质进行冷却硬化。The extruded matrix is cooled and hardened. 根据权利要求9所述的制造方法,所述对所述挤出基质进行冷却硬化,包括:The manufacturing method according to claim 9, wherein the step of cooling and hardening the extruded matrix comprises: 将所述挤出基质置入低温环境中进行冷却,其中,所述低温环境的温度低于所述挤出基质的硬化温度。The extruded matrix is placed in a low temperature environment for cooling, wherein the temperature of the low temperature environment is lower than the hardening temperature of the extruded matrix. 根据权利要求10所述的制造方法,所述硬化温度为-100℃~60℃,所述低温环境的温度为-270℃~60℃。According to the manufacturing method of claim 10, the hardening temperature is -100°C to 60°C, and the temperature of the low-temperature environment is -270°C to 60°C. 根据权利要求9所述的制造方法,所述对所述挤出基质进行冷却硬化,包括:The manufacturing method according to claim 9, wherein the step of cooling and hardening the extruded matrix comprises: 将所述挤出基质与冷媒进行直接换热;或,将所述挤出基质与冷媒进行间接换热。The extruded matrix is directly heat exchanged with a refrigerant; or, the extruded matrix is indirectly heat exchanged with a refrigerant. 根据权利要求9所述的制造方法,在对所述挤出基质进行硬化处理之后,所述制造方法还包括:According to the manufacturing method of claim 9, after hardening the extruded matrix, the manufacturing method further comprises: 将所述挤出基质分切成设定长度。The extruded matrix is slit into set lengths. 根据权利要求9所述的制造方法,经过所述冷却硬化之后的所述挤出基质的硬度为1HB~200HB;和/或,According to the manufacturing method of claim 9, the hardness of the extruded matrix after cooling and hardening is 1HB to 200HB; and/or, 经过所述冷却硬化之后的所述挤出基质的温度为-50℃~5℃。 The temperature of the extruded matrix after the cooling and hardening is -50°C to 5°C. 根据权利要求1-3任意一项所述的制造方法,经过所述负压干燥后的所述挤出基质的硬度为40HB~300HB。According to the manufacturing method according to any one of claims 1 to 3, the hardness of the extruded matrix after the negative pressure drying is 40HB to 300HB. 根据权利要求1-3任意一项所述的制造方法,经过所述负压干燥后的所述挤出基质中的含水量为所述挤出基质的总重量的3%~20%。According to the manufacturing method according to any one of claims 1 to 3, the water content of the extruded matrix after the negative pressure drying is 3% to 20% of the total weight of the extruded matrix. 根据权利要求1-3任意一项所述的制造方法,所述混合物料的组分包括固料和液料,在对混合物料进行常温挤出成型之前,所述制造方法还包括:According to the manufacturing method according to any one of claims 1 to 3, the components of the mixed material include a solid material and a liquid material, and before the mixed material is subjected to room temperature extrusion molding, the manufacturing method further includes: 将所述固料和所述液料分成两个模块分别进行喂料。The solid material and the liquid material are divided into two modules for feeding respectively. 根据权利要求17所述的制造方法,所述将所述固料和所述液料分成两个模块分别进行喂料,包括:According to the manufacturing method of claim 17, the step of dividing the solid material and the liquid material into two modules for feeding respectively comprises: 添加所述固料;adding the solid material; 当所述固料沿物料输送方向移动至所述液料的添加位置,向所述固料中添加所述液料。When the solid material moves along the material conveying direction to the adding position of the liquid material, the liquid material is added to the solid material. 根据权利要求1-3任意一项所述的制造方法,在对所述挤出基质进行负压干燥之后,所述制造方法还包括:According to any one of claims 1 to 3, after the extruded matrix is subjected to negative pressure drying, the manufacturing method further comprises: 在所述挤出基质的外表面包裹包装层;或,对所述挤出基质进行密封包装。A packaging layer is wrapped on the outer surface of the extruded matrix; or the extruded matrix is sealed and packaged. 根据权利要求1-3任意一项所述的制造方法,在100重量份的所述混合物料中,植物原料为30份~90份,助剂原料为1~15份,发烟剂原料为5份~30份,粘合剂原料为1份~10份,香料原料为1~15份。According to the manufacturing method according to any one of claims 1 to 3, in 100 parts by weight of the mixed material, the plant raw material is 30 to 90 parts, the auxiliary raw material is 1 to 15 parts, the smoke agent raw material is 5 to 30 parts, the adhesive raw material is 1 to 10 parts, and the fragrance raw material is 1 to 15 parts. 一种气溶胶生成基质的制造设备,包括:A manufacturing device for an aerosol generating substrate, comprising: 挤出机,所述挤出机用于对混合物料进行常温挤出成型,以使所述混合物料形成挤出基质;An extruder, the extruder is used to perform room temperature extrusion molding on the mixed material so that the mixed material forms an extrusion matrix; 真空干燥装置,所述真空干燥装置用于对所述挤出基质进行负压干燥。A vacuum drying device is used to perform negative pressure drying on the extruded matrix. 根据权利要求21所述的制造设备,所述挤出机的挤出模具为具有一个底模,且所述底模的出料端具有一个口模的单模单口模具;或, According to the manufacturing equipment according to claim 21, the extrusion die of the extruder is a single-mode single-mouth die having a bottom die, and the discharge end of the bottom die has a mouth die; or, 所述挤出机的挤出模具为具有一个底模,且所述底模的出料端具有多个口模的单模多口模具;或,The extrusion die of the extruder is a single-die multi-die having a bottom die, and a discharge end of the bottom die having a plurality of die openings; or, 所述挤出机的挤出模具为具有多个底模,且各所述底模的出料端分别具有多个口模的模多口模具。The extrusion die of the extruder is a multi-mouth die having a plurality of bottom dies, and the discharge end of each bottom die has a plurality of mouth dies. 根据权利要求21所述的制造设备,所述制造设备还包括硬化装置和两个分切装置;The manufacturing apparatus according to claim 21, further comprising a hardening device and two slitting devices; 所述硬化装置设置在所述挤出机和所述真空干燥装置之间,以用于在进行所述负压干燥之前对所述挤出基质进行冷却硬化;The hardening device is disposed between the extruder and the vacuum drying device to cool and harden the extruded matrix before the negative pressure drying; 两个所述分切装置的其中之一设置在所述硬化装置与所述真空干燥装置之间,以用于在进行所述负压干燥之前,对经过所述冷却硬化的所述挤出基质进行预分切;两个所述分切装置的其中另一设置在所述真空干燥装置沿物料输送方向的下游,以用于将经过所述负压干燥的所述挤出基质分切成设定长度。One of the two slitting devices is arranged between the hardening device and the vacuum drying device, so as to pre-slit the extruded matrix that has undergone the cooling and hardening before the negative pressure drying; the other of the two slitting devices is arranged downstream of the vacuum drying device along the material conveying direction, so as to cut the extruded matrix that has undergone the negative pressure drying into set lengths. 根据权利要求21所述的制造设备,所述制造设备还包括硬化装置和分切装置;The manufacturing equipment according to claim 21, further comprising a hardening device and a slitting device; 所述硬化装置设置在所述挤出机和所述真空干燥装置之间,以用于在进行所述负压干燥之前对所述挤出基质进行冷却硬化;The hardening device is disposed between the extruder and the vacuum drying device to cool and harden the extruded matrix before the negative pressure drying; 所述分切装置设置在所述硬化装置与所述真空干燥装置之间,以用于在进行所述负压干燥之前,将经过所述冷却硬化的所述挤出基质分切成设定长度。 The slitting device is disposed between the hardening device and the vacuum drying device, and is used to slit the extruded matrix that has been cooled and hardened into a set length before the negative pressure drying is performed.
PCT/CN2023/140421 2023-06-09 2023-12-20 Aerosol generating matrix manufacturing method and manufacturing device Pending WO2024250638A1 (en)

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