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WO2024155184A3 - Solid extraction process - Google Patents

Solid extraction process Download PDF

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Publication number
WO2024155184A3
WO2024155184A3 PCT/NL2024/050019 NL2024050019W WO2024155184A3 WO 2024155184 A3 WO2024155184 A3 WO 2024155184A3 NL 2024050019 W NL2024050019 W NL 2024050019W WO 2024155184 A3 WO2024155184 A3 WO 2024155184A3
Authority
WO
WIPO (PCT)
Prior art keywords
providing
extraction
liquid
extraction process
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/NL2024/050019
Other languages
French (fr)
Other versions
WO2024155184A2 (en
Inventor
Carlos Iván CABRERA-RODRÍGUEZ
Francisco CAPARRÓS SALVADOR
Luuk ROOK
Joana Patricia CORREIA LEIRÓS
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Greencovery BV
Original Assignee
Greencovery BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Greencovery BV filed Critical Greencovery BV
Priority to EP24701758.5A priority Critical patent/EP4651961A2/en
Publication of WO2024155184A2 publication Critical patent/WO2024155184A2/en
Publication of WO2024155184A3 publication Critical patent/WO2024155184A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0288—Applications, solvents
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/001—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from waste materials, e.g. kitchen waste
    • A23J1/004—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from waste materials, e.g. kitchen waste from waste products of dairy plant
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/006—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from vegetable materials
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/009—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from unicellular algae
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/14—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00—Working-up of proteins for foodstuffs
    • A23J3/04—Animal proteins
    • A23J3/08—Dairy proteins
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00—Working-up of proteins for foodstuffs
    • A23J3/20—Proteins from microorganisms or unicellular algae
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00—Working-up of proteins for foodstuffs
    • A23J3/22—Working-up of proteins for foodstuffs by texturising
    • A23J3/28—Working-up of proteins for foodstuffs by texturising using coagulation from or in a bath, e.g. spun fibres
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00—Working-up of proteins for foodstuffs
    • A23J3/30—Working-up of proteins for foodstuffs by hydrolysis
    • A23J3/32—Working-up of proteins for foodstuffs by hydrolysis using chemical agents
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00—Working-up of proteins for foodstuffs
    • A23J3/30—Working-up of proteins for foodstuffs by hydrolysis
    • A23J3/32—Working-up of proteins for foodstuffs by hydrolysis using chemical agents
    • A23J3/325—Working-up of proteins for foodstuffs by hydrolysis using chemical agents of casein
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20—Synthetic spices, flavouring agents or condiments
    • A23L27/206—Dairy flavours
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L35/00—Foods or foodstuffs not provided for in groups A23L5/00 - A23L33/00; Preparation or treatment thereof
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
    • A23L5/23—Removal of unwanted matter, e.g. deodorisation or detoxification by extraction with solvents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0207—Control systems
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/028—Flow sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0292—Treatment of the solvent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
    • B01D9/0054—Use of anti-solvent

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Cell Biology (AREA)
  • Microbiology (AREA)
  • Zoology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Automation & Control Theory (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The invention provides a method for converting a solid mixture (200) into a non- dissolved part (310), a precipitated part (320) and a supernatant part (330), the method comprising: an extraction stage (10) comprising dissolving at least part of the solid mixture (200) in an extraction liquid (400), thereby providing a liquid mixture (500) and the non- dissolved part (310), wherein the extraction liquid (400) comprises (a) an organic extraction material (410) selected from the group consisting of acetone and alcohols, (b) at least 0.01 M of OH-, (c) at least 0.01 M of a cation (430) selected from the group comprising Na+, K+, Ca2+, Mg2+ and NH4+, and (d) water (700); a first separation stage (20) comprising separating the liquid mixture (500) from the non-dissolved part (310); and a precipitation stage (30) comprising providing CO2 (600) to the liquid mixture (500), thereby providing the precipitated part (320) and the supernatant part (330).
PCT/NL2024/050019 2023-01-17 2024-01-16 Solid extraction process Ceased WO2024155184A2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP24701758.5A EP4651961A2 (en) 2023-01-17 2024-01-16 Solid extraction process

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NL2033973 2023-01-17
NL2033973A NL2033973B1 (en) 2023-01-17 2023-01-17 Solid extraction process

Publications (2)

Publication Number Publication Date
WO2024155184A2 WO2024155184A2 (en) 2024-07-25
WO2024155184A3 true WO2024155184A3 (en) 2024-09-06

Family

ID=85381447

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/NL2024/050019 Ceased WO2024155184A2 (en) 2023-01-17 2024-01-16 Solid extraction process

Country Status (3)

Country Link
EP (1) EP4651961A2 (en)
NL (1) NL2033973B1 (en)
WO (1) WO2024155184A2 (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5828246A (en) * 1981-08-10 1983-02-19 Mitsubishi Acetate Co Ltd Preparation of stevioside
US10113214B2 (en) * 2012-07-05 2018-10-30 Aisin Seiki Kabushiki Kaisha Alkali metal and/or alkali earth metal extraction method
WO2018204061A1 (en) * 2017-05-02 2018-11-08 Cellulose Sciences International, Inc. Treatment of brown stock

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
HUE033952T2 (en) 2008-05-16 2018-01-29 Siebte Pmi Verwaltungs Gmbh Oilseed protein concentrates and processes for the production thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5828246A (en) * 1981-08-10 1983-02-19 Mitsubishi Acetate Co Ltd Preparation of stevioside
US10113214B2 (en) * 2012-07-05 2018-10-30 Aisin Seiki Kabushiki Kaisha Alkali metal and/or alkali earth metal extraction method
WO2018204061A1 (en) * 2017-05-02 2018-11-08 Cellulose Sciences International, Inc. Treatment of brown stock

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
ANDERSEN L T ET AL: "Study of taste-active compounds in the water-soluble extract of mature Cheddar cheese", INTERNATIONAL DAIRY JOURNAL, ELSEVIER APPLIED SCIENCE, BARKING, GB, vol. 20, no. 8, 1 August 2010 (2010-08-01), pages 528 - 536, XP027061288, ISSN: 0958-6946, [retrieved on 20100306] *
ENGEL E ET AL: "DETERMINATION OF TASTE-ACTIVE COMPOUNDS OF A BITTER CAMEMBERT CHEESE BY OMISSION TESTS", JOURNAL OF DAIRY RESEARCH, CAMBRIDGE UNIVERSITY PRESS, CAMBRIDGE, GB, vol. 68, no. 4, 1 November 2001 (2001-11-01), pages 675 - 688, XP009069054, ISSN: 0022-0299, DOI: 10.1017/S0022029901005209 *
RDUDOT-ALGARON F ET AL: "Isolation of y-Glutamyl Peptides from Comte Cheese", JOURNAL OF DAIRY RESEARCH, 1 January 1994 (1994-01-01), pages 1161 - 1166, XP093185324 *
SALLES C ET AL: "Evaluation of taste compounds in water-soluble extract of goat cheeses", FOOD CHEMISTRY, vol. 68, no. 4, 1 March 2000 (2000-03-01), NL, pages 429 - 435, XP093185315, ISSN: 0308-8146, DOI: 10.1016/S0308-8146(99)00213-7 *
TABORDA GONZALO ET AL: "Taste and flavor of artisan and industrial Manchego cheese as influenced by the water-soluble extract compounds", EUROPEAN FOOD RESEARCH AND TECHNOLOGY, vol. 227, no. 2, 16 October 2007 (2007-10-16), Berlin/Heidelberg, pages 323 - 330, XP093185321, ISSN: 1438-2377, Retrieved from the Internet <URL:http://link.springer.com/article/10.1007/s00217-007-0769-7/fulltext.html> DOI: 10.1007/s00217-007-0769-7 *

Also Published As

Publication number Publication date
WO2024155184A2 (en) 2024-07-25
EP4651961A2 (en) 2025-11-26
NL2033973B1 (en) 2024-07-26

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