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WO2024098130A1 - Method for producing microcarriers, said microcarriers and use of said microcarriers - Google Patents

Method for producing microcarriers, said microcarriers and use of said microcarriers Download PDF

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Publication number
WO2024098130A1
WO2024098130A1 PCT/BR2023/050382 BR2023050382W WO2024098130A1 WO 2024098130 A1 WO2024098130 A1 WO 2024098130A1 BR 2023050382 W BR2023050382 W BR 2023050382W WO 2024098130 A1 WO2024098130 A1 WO 2024098130A1
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WIPO (PCT)
Prior art keywords
microcarriers
present
process according
fat
production
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PCT/BR2023/050382
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French (fr)
Portuguese (pt)
Inventor
Bibiana FRANZEN MATTE
Raíssa CANOVA
Luiza BRAND
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Cellva Ingredients Ltda
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Cellva Ingredients Ltda
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Publication of WO2024098130A1 publication Critical patent/WO2024098130A1/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L13/00Meat products; Meat meal; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B33ADDITIVE MANUFACTURING TECHNOLOGY
    • B33YADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
    • B33Y70/00Materials specially adapted for additive manufacturing
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12NMICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N5/00Undifferentiated human, animal or plant cells, e.g. cell lines; Tissues; Cultivation or maintenance thereof; Culture media therefor
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J5/00Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers
    • C09J5/02Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers involving pretreatment of the surfaces to be joined

Definitions

  • the present invention refers to the Biotechnology technological sector and concerns the production process of microcarriers particularly suitable for alternative production of cultured meat and fat.
  • the objective of the present invention is to provide technology to enable the production of meat and fat equivalent to animal products. This reduces animal slaughter, which is currently a critical factor in our society. [002].
  • the present invention relates to microcarriers and their application in the production of cultured meat and fat. BASICS OF THE INVENTION [003].
  • mammalian cells e.g.: fat culture
  • mammalian cells e.g.: bovine, porcine
  • proliferate a highly controlled extracorporeal system that provides the cells with all the ingredients necessary for this.
  • adipose (or fatty) cells which biologically have the capacity to store excess energy, when properly stimulated, in large fat vesicles within its cytoplasm. All this starting from a small initial cultivation.
  • the final product is very similar to fatty tissue originating from animal slaughter, as this tissue is mainly composed of the same cells that were now produced in an industrial setup, and can therefore meet the organoleptic characteristics necessary to replace the use of fat originating from animal slaughter.
  • the three-dimensional (3D) organization of cells produced in culture may be highly relevant.
  • This document describes edible microcarriers formed from cross-linked pectin, such as pectin-thiopropionylamide (PTP) and RGD-containing polypeptide, such as thiolated cardosin A.
  • PTP pectin-thiopropionylamide
  • RGD-containing polypeptide such as thiolated cardosin A.
  • Document CN113684177A describes a composite microcarrier for the manufacture of cell cultured meat. This composite microcarrier comprises microcarrier beads with a network-like structure of polysaccharide, aldehyde acid and protein. [0010].
  • Document CN114317394A discloses an edible and dissolvable microcarrier for three-dimensional cell culture.
  • the polysaccharide microcarrier is edible, soluble, with good biocompatibility and cell adhesion, capable of supporting cell adhesion, growth and proliferation, and can be used for rapid large-scale cell production and reducing the cost of cell culture meat products, especially used in the field of cell culture meat, and wide in application prospect.
  • Document WO2020149791 discloses methods for forming and producing renewable primary cell lines of muscle and/or fat, immortalized cell lines and stem cell lines from shrimp, prawn, crab, crayfish and/or lobster species and the cell lines as well as human and animal meat products produced from them. [0012]. Therefore, there is no equivalent solution in the state of the art to the one presented here in the present invention that combines technical differences, economic advantages, safety and reliability.
  • microcarriers that allow cell expansion in bioprocesses.
  • microcarriers that are edible.
  • microcarriers with a manufacturing cost that does not increase the price of the final product.
  • microcarriers that do not affect the taste and quality of the final product.
  • microcarriers suitable for the production of cultured animal fat are yet another objective of the present invention.
  • microcarriers that can contribute to the nutritional properties of the final product.
  • microcarriers that promote the adherence of cells of animal origin to quickly enter a differentiation stage.
  • microcarriers with good biocompatibility, adhesion and cell proliferation.
  • technologies applicable to the production of meat and fat to replace animal slaughter [0022].
  • microcarriers that allow cell differentiation, such as muscle and fat.
  • the present invention achieves these and other objectives through a microcarrier production process that comprises: - selection of appropriate vegetable regions; - decellularization of said vegetables and production of microcarriers; - chemical and thermal processing of microcarriers; - arrangement of microcarriers for adhesion of cells capable of adhesion. [0024].
  • the present invention achieves these and other objectives through microcarriers obtained from the above process. [0025].
  • the present invention achieves these and other objectives through the use of said microcarriers to produce material similar to meat and fat of animal origin. DETAILED DESCRIPTION OF THE DRAWINGS [0026].
  • the present invention is better detailed through the attached figures: [0027].
  • Figure 1 is an image of the final result of the microcarrier object of the present invention; [0028].
  • Figure 2 is a first preferred embodiment of use/application of the object of the present invention; [0029].
  • Figure 3 is a second preferred embodiment of use/application of the object of the present invention; [0030].
  • Figure 4 is a graph that illustrates the results of DNA quantification after a certain period in cultivation. DETAILED DESCRIPTION OF THE INVENTION [0031].
  • the present invention relates to a microcarrier production process comprising: - selection of appropriate vegetable regions; - decellularization of said vegetables and production of microcarriers; - chemical and thermal processing of microcarriers; - arrangement of microcarriers for adhesion of cells capable of adhesion. [0032].
  • the microcarrier production process comprises: - selection of appropriate vegetable regions; - decellularization of said vegetables and preparation of microcarriers; - chemical and thermal processing of microcarriers; - arrangement of microcarriers for adhesion of cells capable of adhesion.
  • the microcarriers prepared through the above process are indicated for production in bioreactors of meat or fat similar to products of animal origin. [0034].
  • a microcarrier or microtransporter is a support matrix that allows the growth of adherent cells in bioreactors. Instead of on a flat surface, cells are grown on the surface of microcarriers so that each particle carries several hundred cells, and therefore the expansion capacity can be multiplied several times.
  • microcarrier technology provides a simple way to scale up cultural systems for industrial production of cell- or protein-based therapies, or for research purposes.
  • the advantages of applying microcarrier technology in the biotechnology industry include (a) ease of scaling, (b) ability to precisely control cell growth conditions in bioreactors even with remote control, (c) significant reduction in space required for manufacturing operation , (d) relevant reduction in technical work and (e) a more natural environment for cell culture that promotes differentiation. [0036].
  • vegetables In order to develop microcarriers that allow cell expansion in bioprocesses and that are edible, it was decided to use vegetables. In a preferred embodiment, it was decided to use broccoli florets due to their appearance similar to a microcarrier, which simplifies the process and is a relevant technical advantage. [0037].
  • Vegetables can be used to prepare microcarriers such as spinach, lettuce, cauliflower, peas, kale and other vegetables with similar characteristics. [0038].
  • appropriate vegetable regions are used.
  • the selection of vegetables is carried out according to size (less than 500um) and rounded shape. [0039].
  • the vegetables undergo a decellularization technique and are then decellularized.
  • Decellularization consists of a technique that involves removing cells from a tissue or organ, leaving only the structure that surrounds them, this being the extracellular matrix. [0040]. This process involves exposing living tissues to a sequence of detergents to remove intracellular components, leaving behind the extracellular matrix intact.
  • the detergent will be selected from combinations of ionic detergents and non-ionic detergents, whether or not including disinfectants.
  • ionic detergents cetyltrimethylammonium bromide
  • non-ionic detergents such as octyl phenol ethoxylate (Triton®-x-100) and digitonin.
  • Detergents can be combined with the use of disinfectants.
  • detergents between 2% and 16% are used, preferably in the following concentration ranges: between 2 and 4%; between 4.1 and 6%; between 6.1% and 8%; between 8.1 and 10%; between 10.1 and 12%, between 12.1% and 14%, between 14.1 and 16%. [0042].
  • This step takes place at a temperature that varies between 2°C and 34°C, preferably being one of the following temperature ranges: between 2°C and 6°C; between 6.1°C and 10°C; between 10.1°C and 14°C; between 14°C and 18°C; between 18°C and 22°C; between 22°C and 26°C; between 26°C and 30°C; between 30°C and 34°C.
  • a refrigerator and oven are used to reach said temperatures.
  • exchanges also occur, preferably between 5 and 8 exchanges; between 9 and 12 exchanges; between 13 and 16 exchanges; between 17 and 20 exchanges; under agitation of the mixture reached 0 rpm to 200 rpm; 200rpm to 400rpm; 400rpm to 600rpm; 600rpm to 800rpm preferably using a magnetic stirrer.
  • a thermal and chemical procedure is carried out. This procedure allows the improvement of cell adhesion.
  • Chemical processing involves the use of different concentrations of inorganic salt solution that contains cation and anion.
  • inorganic salt such as potassium periodate is used in concentrations ranging from 0.004 mg/ml to 14 mg/ml, preferably between 0.004 mg/ml to 0.04 mg/ml; from 0.04 mg/ml to 0.4 mg/ml; from 0.4 mg/ml to 4 mg/ml; from 4 mg/ml to 14 mg/ml of salt in H20 solution at a temperature ranging between 35°C and 65°C, preferably 35°C to 45°C, 46°C to 55°C and 56°C at 65°C temperatures are reached using an oven in a period of time that varies between 20 and 40 minutes per cycle; between 40 and 80 minutes per cycle; between 80 and 120 minutes per cycle; between 120 and 160 minutes per cycle.
  • the number of cycles varies between 2 to 4 cycles of salt exposure; 3 to 5 cycles of salt exposure; 4 to 6 cycles of salt exposure.
  • cells of animal origin are added to assess cell viability for at least 7 days, preferably for a period that varies between 7 and 35 days.
  • DNA extraction is performed to evaluate the quality of the decellularization step as well as maintaining the viability of the cells during this period when in contact with the microcarriers of the present invention.
  • test protocol was developed: [0049].
  • FIG. 1 illustrates the final result of the microcarrier object of the present invention, which clearly illustrates the application of the decellularization technique to an appropriate region of the selected vegetable.
  • Figure 2 illustrates the result of applying the present invention to a caramel food mixture.
  • Figure 3 illustrates the result of applying the present invention to a meat product (sausage).
  • Figure 4 illustrates the result of DNA quantification. [0054]. Analyzing figure 4, it can be seen that there was a satisfactory result after the decellularization of the vegetable.
  • This graph illustrates that the process of the present invention offers significant results in terms of the number of cells adhered to the microcarrier, proving what is proposed. It was observed that the quantification of DNA, which is related to the number of cells, was higher in the CA + MCdp group compared to the CA + MCd group. [0057]. Considering the results achieved, it can be understood that there is potential for cell proliferation in the microcarriers of present invention for a longer period of time. [0058].
  • the present invention presents numerous technical and economic advantages when compared to the state of the art, some of which are listed below: ⁇ The microcarriers of the present invention allow cell expansion in bioprocesses; ⁇ The microcarriers of the present invention are edible; ⁇ The microcarriers of the present invention have a manufacturing cost that does not increase the price of the final product; ⁇ The microcarriers of the present invention do not affect the flavor and quality of the final product; ⁇ The microcarriers of the present invention are indicated for the production of cultured animal fat; ⁇ The microcarriers of the present invention can contribute to the nutritional properties of the final product; ⁇ The microcarriers of the present invention promote the adherence of cells of animal origin to quickly enter a differentiation stage; ⁇ The microcarriers of the present invention have good biocompatibility and allow cell adhesion and proliferation; ⁇ The microcarriers of the present invention are applicable to the production of meat and fat to replace animal slaughter; ⁇ The microcarriers of the present invention allow cell differentiation, such as in muscle and fat

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  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Biotechnology (AREA)
  • Genetics & Genomics (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
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  • Nutrition Science (AREA)
  • Wood Science & Technology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Food Science & Technology (AREA)
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Abstract

The present invention relates to a method for producing microcarriers which are particularly suitable for the alternative production of cultured meat and fat. The aim of the present invention is to provide technology to facilitate the production of meat and fat that are equivalent to the animal products, thereby reducing animal slaughter, which is currently a critical issue in our society. The present invention further relates to the microcarriers and the use thereof in the production of cultured meat and fat.

Description

Relatório Descritivo de Patente de Invenção para “PROCESSO DE PREPARAÇÃO DE MICROCARREADORES, DITOS MICROCARREADORES E USO DOS DITOS MICROCARREADORES” CAMPO DA INVENÇÃO [001]. A presente invenção refere-se ao setor tecnológico de Biotecnologia e diz respeito a processo de produção de microcarreadores particularmente indicados para produção alternativa de carne e gordura cultivadas. O objetivo da presente invenção é proporcionar tecnologia para viabilizar produção de carne e gordura equivalentes aos produtos animais. Assim, reduz-se o abate animal que atualmente é um fator crítico presente em nossa sociedade. [002]. Ainda, a presente invenção refere-se aos microcarreadores e sua aplicação na produção de carne e gordura cultivadas. FUNDAMENTOS DA INVENÇÃO [003]. A produção de carne e gordura por cultivo de células de mamíferos (ex.: cultura de gordura) é uma das formas que a nova indústria de alimentos tem para atender as mais recentes demandas do consumidor, em especial para a substituição de proteína e gordura oriunda de abate animal. Ela se baseia na capacidade de células e tecidos, no caso concreto principalmente de células de mamíferos (ex.: bovino, suíno) de se multiplicarem (ex.: proliferar) e maturarem em um sistema extracorpóreo altamente controlado que fornece às células todas os ingredientes necessários para tal. [004]. Ao final do processo produtivo, espera-se obter uma grande quantidade de células de interesse, no caso células adiposas (ou gordurosas), que biologicamente possuem a capacidade de armazenar o excesso energético, quando devidamente estimuladas, em grandes vesículas de gordura dentro do seu citoplasma. Tudo isso partindo de um cultivo inicial pequeno. [005]. Desta forma, o produto final muito se assemelha ao tecido gorduroso oriundo de abate animal, visto que este tecido é composto majoritariamente pelas mesmas células que foram produzidas agora em setup industrial, podendo então atender as características organolépticas necessárias para substituir o uso de gordura oriunda de abate animal. [006]. A depender do que se espera do produto final, por questões organolépticas, a organização tridimensional (3D) das células produzidas no cultivo pode ter alta relevância. Para isso, tecnologias já existentes (microcarreadores, microencapsulamento, etc) podem ser empregadas ou desenvolvidas utilizando técnicas de engenharia tecidual com o material bruto cultivado (ex.: bioimpressão 3D, semeadura em arcabouços comestíveis, etc.). [007]. Destacamos abaixo alguns ensinamentos do estado da técnica que se referem a presente matéria: [008]. O documento US2015079238 descreve microcarreadores comestíveis, incluindo beads de microcarreadores, microesferas e microesponjas, apropriados para uso em um biorreator para células de cultura que podem ser usadas para formar um produto de carne comestível. Este documento descreve microcarreadores comestíveis formados de pectina reticulada, como pectina-tiopropionilamida (PTP) e polipeptídeo contendo RGD, como cardosina tiolada A. [009]. Já o documento CN113684177A descreve um microcarreador compósito para a fabricação de carne de cultura de células. Este microcarreador composto compreende esferas de microcarreador com uma estrutura em forma de rede de polissacarídeo, ácido aldeído e proteína. [0010]. O documento CN114317394A divulga um microcarreador comestível e dissolúvel para cultura de células tridimensionais. O microcarreador de polissacarídeo é comestível, solúvel, com boa biocompatibilidade e adesão celular, capaz de suportar adesão, crescimento e proliferação de células, podendo ser utilizado para produção rápida de células em larga escala e redução do custo de produtos cárneos de cultura celular, especialmente utilizados em o campo da carne de cultura de células, e ampla na perspectiva de aplicação. [0011]. O documento WO2020149791 revela métodos para a formação e produção de linhas de células primárias renováveis de músculo e/ou gordura, linhas de células imortalizadas e linhas de células-tronco de espécies de camarão, camarão, caranguejo, lagostim e/ou lagosta e as próprias linhas de células bem como produtos de carne de consumo humano e animal produzidos a partir deles. [0012]. Portanto, não existe no estado da técnica solução equivalente à apresentada aqui na presente invenção que alia diferenciais técnicos, vantagens econômicas, segurança e confiabilidade. OBJETIVOS DA INVENÇÃO [0013]. Assim, é um objetivo da presente invenção proporcionar microcarreadores que permitam a expansão celular em bioprocessos. [0014]. É outro dos objetivos da presente invenção proporcionar microcarreadores que sejam comestíveis. [0015]. É outro dos objetivos da presente invenção proporcionar microcarreadores com custo de fabricação que não onere o preço do produto final. [0016]. É ainda outro dos objetivos da presente invenção proporcionar microcarreadores que não afetem o sabor e qualidade do produto final. [0017]. É ainda outro dos objetivos da presente invenção proporcionar microcarreadores indicado para produção de gordura animal cultivada. [0018]. É também outro dos objetivos da presente invenção proporcionar microcarreadores que possam contribuir nas propriedades nutricionais do produto final. [0019]. É também outro dos objetivos da presente invenção proporcionar microcarreadores que promovam a aderência de células de origem animal para entrarem rapidamente em um estágio de diferenciação. [0020]. É ainda outro dos objetivos da presente invenção proporcionar microcarreadores , com boa biocompatibilidade, adesão e proliferação celular. [0021]. É também outro dos objetivos da presente invenção proporcionar tecnologias aplicáveis a produção de carne e gordura em substituição ao abate animal. [0022]. É ainda outro dos objetivos da presente invenção proporcionar microcarreadores que permitem a diferenciação em celular, como em músculo e gordura. SUMÁRIO DA INVENÇÃO [0023]. A presente invenção atinge esses e outros objetivos por meio de processo de produção de microcarreadores que compreende: - seleção de regiões apropriadas de hortaliças; - descelularização das ditas hortaliças e confecção dos microcarreadores; - processamento químico e térmico dos microcarreadores; - disposição dos microcarreadores para aderência de células aptas para adesão. [0024]. A presente invenção atinge esses e outros objetivos por meio de microcarreadores obtidos a partir do processo acima. [0025]. Ainda, a presente invenção atinge esses e outros objetivos por meio de uso dos ditos microcarreadores para produção de material similar a carne e gordura de origem animal. DESCRIÇÃO DETALHADA DOS DESENHOS [0026]. A presente invenção é mais bem detalhada por meio das figuras apensas: [0027]. Figura 1 é uma imagem do resultado final do microcarreador objeto da presente invenção; [0028]. Figura 2 é uma primeira concretização preferida de uso/aplicação do objeto da presente invenção; [0029]. Figura 3 é uma segunda concretização preferida de uso/aplicação do objeto da presente invenção; [0030]. Figura 4 é um gráfico que ilustra resultado da quantificação de DNA após determinado período em cultivo. DESCRIÇÃO DETALHADA DA INVENÇÃO [0031]. A presente invenção se refere a um processo de produção de microcarreadores que compreende: - seleção de regiões apropriadas de hortaliças; - descelularização das ditas hortaliças e confecção dos microcarreadores; - processamento químico e térmico dos microcarreadores; - disposição dos microcarreadores para aderência de células aptas para adesão. [0032]. Em uma concretização preferida da presente invenção, o processo de produção de microcarreadores compreende: - seleção de regiões apropriadas de hortaliças; - descelularização das ditas hortaliças e confecção dos microcarreadores; - processamento químico e térmico dos microcarreadores; - disposição dos microcarreadores para aderência de células aptas para adesão. [0033]. Os microcarreadores preparados por meio do processo acima são indicados para produção em biorreatores de carne ou gordura similares aos produtos de origem animal. [0034]. Um microcarreador ou microtransportador é uma matriz de suporte que permite o crescimento de células aderentes em biorreatores. Em vez de em uma superfície plana, as células são cultivadas na superfície de microcarreadores para que cada partícula carregue várias centenas de células, e, portanto, a capacidade de expansão pode ser multiplicada várias vezes. Ele fornece uma maneira simples de escalar sistemas culturais para a produção industrial de terapias baseadas em células ou proteínas, ou para fins de pesquisa. [0035]. As vantagens da aplicação da tecnologia de microcarreador na indústria biotecnológica incluem (a) facilidade de escala, (b) capacidade de controle preciso das condições de crescimento celular em biorreatores mesmo com controle remoto, (c) redução significativa do espaço necessário para operação de fabricação, (d) redução relevante no trabalho técnico e (e) um ambiente mais natural para a cultura celular que promove diferenciação. [0036]. De modo a desenvolver microcarreadores que permitam a expansão celular em bioprocessos e que sejam comestíveis, foi decidido pelo uso de hortaliças. Em uma concretização preferida, decidiu-se pelo uso de floretes de brócolis devido a seu aspecto semelhante a um microcarreador o que simplifica o processo sendo uma vantagem técnica relevante. [0037]. Em concretizações alternativas da presente invenção, outras hortaliças podem ser usadas para preparação os microcarreadores como espinafre, alface, couve-flor, ervilha, couve e demais vegetais com características similares a estes. [0038]. Para a presente invenção, são utilizadas regiões apropriadas de hortaliças. Em concretizações preferidas, a seleção das hortaliças é realizada de acordo com tamanho (menor que 500um) e formato arredondado. [0039]. Na sequência, as hortaliças passam por técnica de descelularização sendo então descelularizadas. Descelularização consiste em uma técnica que envolve a remoção das células de um tecido ou órgão, deixando apenas a estrutura que as envolve sendo esta a matriz extracelular. [0040]. Esse processo envolve a exposição de tecidos vivos a uma sequência de detergentes para remover componentes intracelulares, deixando para trás a matriz extracelular intacta. Ainda, as paredes celulares vegetais, após sofrerem descelularização vegetal, são compostas principalmente de celulose, pectina e hemicelulose. Logo, são benéficas nutricionalmente na maioria das dietas. [0041]. O detergente ser selecionado dentre combinações entre detergentes iônicos e detergentes não-iônicos compreendendo ou não desinfetantes. Exemplos de detergentes que podem ser usados neste processo, mas não limitados a estes são: uso combinado de detergentes iônicos (brometo de cetriltrimetilamônio) e não-iônicos como octil fenol etoxilato (Triton®-x-100) e digitonina. Os detergentes podem ser combinados com uso de desinfetantes. Preferencialmente, utiliza-se detergentes entre 2% e 16%, sendo preferencialmente nas seguintes faixas de concentração: entre 2 e 4%; entre 4,1 e 6%; entre 6,1% e 8%; entre 8,1 e 10%; entre 10,1 e 12%, entre 12,1% e 14%, entre 14,1 e 16%. [0042]. Esta etapa ocorre em temperatura que varia entre 2°C e 34°C, sendo preferencialmente uma das seguintes faixas de temperatura: entre 2°C e 6°C; entre 6,1°C e 10°C; entre 10,1°C e 14°C; entre 14°C e 18°C; entre 18°C e 22°C; entre 22°C e 26°C; entre 26°C e 30°C; entre 30°C e 34°C. preferencialmente, neste caso, utiliza-se geladeira e estufa para alcançar as ditas temperaturas. [0043]. Nesta etapa, também ocorrem as trocas, preferencialmente sendo, entre 5 e 8 trocas; entre 9 e 12 trocas; entre 13 e 16 trocas; entre 17 e 20 trocas; sob agitação da mistura alcançada ocorre 0 rpm a 200rpm; 200rpm a 400rpm; 400rpm a 600rpm; 600rpm a 800rpm preferencialmente com uso de agitador magnético. [0044]. Na sequência da preparação dos microcarreadores, é realizado procedimento térmico e químico. Esse procedimento permite o melhoramento da adesão celular. [0045]. O processamento químico envolve o uso de diferentes concentrações de solução de sal inorgânico que contém cátion e ânion. Em conjunto, são realizados ciclos de temperaturas com os microcarreadores embebidos em solução em período de tempo determinado. [0046]. Em concretizações preferidas, utiliza-se sal inorgânico como periodato de potássio em concentrações que variam entre 0,004 mg/ml a 14 mg/ml, sendo preferencialmente entre 0,004 mg/ml a 0,04 mg/ml; de 0,04 mg/ml a 0,4 mg/ml; de 0,4 mg/ml a 4 mg/ml; de 4 mg/ml a 14 mg/ml de sal em solução de H20 sob temperatura que varia entre 35°C e 65°C, sendo preferencialmente 35°C a 45°C, 46°C a 55°C e 56°C a 65°C temperaturas estas alcançadas por meio de estufa em período de tempo que varia entre 20 e 40 minutos por ciclo; entre 40 e 80 minutos por ciclo; entre 80 e 120 minutos por ciclo; entre 120 e 160 minutos por ciclo. Preferencialmente, o número de ciclos varia entre 2 a 4 ciclos de exposição ao sal; 3 a 5 ciclos de exposição ao sal; 4 a 6 ciclos de exposição ao sal. [0047]. Na sequência, são adicionadas células de origem animal para avaliar viabilidade celular por pelo menos 7 dias, sendo preferencialmente por um período que varia entre 7 e 35 dias. Ao final deste período, é realizada extração de DNA para avaliar qualidade da etapa de descelularização bem como manutenção da viabilidade das células nesse período quando em contato com os microcarreadores da presente invenção. [0048]. Para que a presente invenção seja testada de modo a comprovar sua eficácia, foi desenvolvido o seguinte protocolo de teste: [0049]. (A) Protocolo de extração de DNA: a. Macerar amostra da hortaliça selecionada com uma solução tampão; b. Vortexar; c. Adicionar Proteinase K (20mg/mL) e 15 µl de SDS 10%; d. Incubar a uma temperatura de 37°C até desmanchar e concluir a digestão da amostra; e. Centrifugar por um tempo 2 min a uma rotação de 12.000 rpm; f. Transferir o sobrenadante coletado para outro tubo de reação; g. Adicionar fenol (tamponado pH 8) na proporção do volume do sobrenadante coletado; h. Homogeneizar por um período de 10 min, virando os tubos gentilmente; i. Centrifugar por um período de 5 min a rotação de 12.000 rpm, a uma temperatura de 10°C; j. Transferir o sobrenadante (fase aquosa) para um novo tubo de reação; k. Adicionar clorofórmio/álcool-isoamílico na proporção do volume de sobrenadante coletado; l. Agitar por um período de 5 min com as mãos; m. Centrifugar por um período de 5 min a uma rotação de 12.000 rpm; n. Transferir o sobrenadante para novo tubo de reação; o. Opcionalmente, adicionar NaCl até alcançar concentração final de 0,3M; p. Adicionar etanol absoluto gelado (a uma temperatura de - 20°C) na proporção de 2x o volume coletado na etapa n; q. Agitar o sistema invertendo o tubo algumas vezes; r. Incubar o sistema a temperatura de -20°C durante um período de 30 min; s. Centrifugar por um período de 30 min a uma rotação de 14.000 rpm a temperatura de 10°C; t. Descartar o etanol e adicionar 1 mL de álcool 70%; u. Centrifugar por um período de 5 min a uma rotação de 14.000 rpm a uma temperatura de 10°C; v. Descartar o sobrenadante, secar o pellet em papel toalha; w. Ressuspender o pellet em uma solução de 50 µl de TE (Tris-Edta) + 0,5 µl de RNAse A; x. Incubar a uma temperatura de 37°C durante um período de 20 min; y. Quantificação é realizada em absorbância para faixa específica de DNA (resultado em ng/ l); [0050]. A figura 1 ilustra o resultado final do microcarreador objeto da presente invenção o qual ilustra claramente a aplicação da técnica de descelularização de uma região apropriada da hortaliça selecionada. [0051]. Já, a figura 2 ilustra o resultado da aplicação da presente invenção em uma mistura alimentícia de caramelo. [0052]. A figura 3 ilustra o resultado da aplicação da presente invenção em um produto de carne (linguiça). [0053]. A figura 4 ilustra o resultado da quantificação de DNA. [0054]. Analisando a figura 4, observa-se que houve resultado satisfatório após a descelularização da hortaliça. Nos grupos contendo as células, observa-se que as células apresentaram manutenção da viabilidade com e sem a presença do microcarreador por 7 dias. [0055]. A Figura 4 apresenta os dados de quantificação de DNA dos grupos descritos acima. Abaixo, segue a legenda da figura 4: - MCdp = microcarreador descelularizado com processamento térmico e químico (presente invenção); - MCd = microcarreador descelularizado (resultado das duas primeiras etapas do processo da presente invenção); - CA + MCdp = células animais aderidas ao microcarreador da presente invenção; - CA + MCd = células animais aderidas ao microcarreador descelularizado (resultado das duas primeiras etapas do processo da presente invenção); - CA = células animais. [0056]. Esse gráfico (figura 4) ilustra que o processo da presente invenção oferece resultados significativos em termos de quantidade de células aderidas ao microcarreador comprovando o que se propõe. Observa-se que a quantificação de DNA que está relacionada a quantidade de células foi maior no grupo CA + MCdp em comparação com o grupo CA + MCd. [0057]. Considerando os resultados alcançados, pode-se entender que há potencial para proliferação das células nos microcarreadores da presente invenção por maior período de tempo. [0058]. A presente invenção apresenta inúmeras vantagens técnicas e econômicas quando comparada com o estado da arte, sendo algumas listadas abaixo: ✓ Os microcarreadores da presente invenção permitem a expansão celular em bioprocessos; ✓ Os microcarreadores da presente invenção são comestíveis; ✓ Os microcarreadores da presente invenção têm custo de fabricação que não onera o preço do produto final; ✓ Os microcarreadores da presente invenção não afetam o sabor e qualidade do produto final; ✓ Os microcarreadores da presente invenção são indicados para produção de gordura animal cultivada; ✓ Os microcarreadores da presente invenção podem contribuir nas propriedades nutricionais do produto final; ✓ Os microcarreadores da presente invenção promovem a aderência de células de origem animal para entrarem rapidamente em um estágio de diferenciação; ✓ Os microcarreadores da presente invenção possuem boa biocompatibilidade e permitem adesão e proliferação celular; ✓ Os microcarreadores da presente invenção são aplicáveis a produção de carne e gordura em substituição ao abate animal; ✓ Os microcarreadores da presente invenção permitem a diferenciação celular, como em músculo e gordura. [0059]. Tendo sido descrito um exemplo de uma concretização preferida da presente invenção, deve ser entendido que o escopo da presente invenção abrange outras variações possíveis do conceito inventivo descrito, sendo limitadas tão somente pelo teor das reivindicações apensas, aí incluídos os possíveis equivalentes. Invention Patent Descriptive Report for “PROCESS FOR PREPARING MICROCARRIERS, SAID MICROCARRIERS AND USE OF SAID MICROCARRIERS” FIELD OF THE INVENTION [001]. The present invention refers to the Biotechnology technological sector and concerns the production process of microcarriers particularly suitable for alternative production of cultured meat and fat. The objective of the present invention is to provide technology to enable the production of meat and fat equivalent to animal products. This reduces animal slaughter, which is currently a critical factor in our society. [002]. Furthermore, the present invention relates to microcarriers and their application in the production of cultured meat and fat. BASICS OF THE INVENTION [003]. The production of meat and fat by culturing mammalian cells (e.g.: fat culture) is one of the ways that the new food industry has to meet the latest consumer demands, especially for the replacement of protein and fat from of animal slaughter. It is based on the ability of cells and tissues, in this specific case mainly mammalian cells (e.g.: bovine, porcine) to multiply (e.g.: proliferate) and mature in a highly controlled extracorporeal system that provides the cells with all the ingredients necessary for this. [004]. At the end of the production process, it is expected to obtain a large quantity of cells of interest, in this case adipose (or fatty) cells, which biologically have the capacity to store excess energy, when properly stimulated, in large fat vesicles within its cytoplasm. All this starting from a small initial cultivation. [005]. In this way, the final product is very similar to fatty tissue originating from animal slaughter, as this tissue is mainly composed of the same cells that were now produced in an industrial setup, and can therefore meet the organoleptic characteristics necessary to replace the use of fat originating from animal slaughter. [006]. Depending on what is expected from the final product, for organoleptic reasons, the three-dimensional (3D) organization of cells produced in culture may be highly relevant. To achieve this, existing technologies (microcarriers, microencapsulation, etc.) can be employed or developed using tissue engineering techniques with the raw material cultivated (e.g.: 3D bioprinting, seeding in edible scaffolds, etc.). [007]. We highlight below some teachings from the state of the art that refer to this matter: [008]. Document US2015079238 describes edible microcarriers, including microcarrier beads, microspheres and microsponges, suitable for use in a bioreactor for culturing cells that can be used to form an edible meat product. This document describes edible microcarriers formed from cross-linked pectin, such as pectin-thiopropionylamide (PTP) and RGD-containing polypeptide, such as thiolated cardosin A. [009]. Document CN113684177A describes a composite microcarrier for the manufacture of cell cultured meat. This composite microcarrier comprises microcarrier beads with a network-like structure of polysaccharide, aldehyde acid and protein. [0010]. Document CN114317394A discloses an edible and dissolvable microcarrier for three-dimensional cell culture. The polysaccharide microcarrier is edible, soluble, with good biocompatibility and cell adhesion, capable of supporting cell adhesion, growth and proliferation, and can be used for rapid large-scale cell production and reducing the cost of cell culture meat products, especially used in the field of cell culture meat, and wide in application prospect. [0011]. Document WO2020149791 discloses methods for forming and producing renewable primary cell lines of muscle and/or fat, immortalized cell lines and stem cell lines from shrimp, prawn, crab, crayfish and/or lobster species and the cell lines as well as human and animal meat products produced from them. [0012]. Therefore, there is no equivalent solution in the state of the art to the one presented here in the present invention that combines technical differences, economic advantages, safety and reliability. OBJECTIVES OF THE INVENTION [0013]. Thus, it is an objective of the present invention to provide microcarriers that allow cell expansion in bioprocesses. [0014]. It is another objective of the present invention to provide microcarriers that are edible. [0015]. It is another objective of the present invention to provide microcarriers with a manufacturing cost that does not increase the price of the final product. [0016]. It is yet another objective of the present invention to provide microcarriers that do not affect the taste and quality of the final product. [0017]. It is yet another objective of the present invention to provide microcarriers suitable for the production of cultured animal fat. [0018]. It is also another objective of the present invention to provide microcarriers that can contribute to the nutritional properties of the final product. [0019]. It is also another objective of the present invention to provide microcarriers that promote the adherence of cells of animal origin to quickly enter a differentiation stage. [0020]. It is yet another objective of the present invention to provide microcarriers, with good biocompatibility, adhesion and cell proliferation. [0021]. It is also another objective of the present invention to provide technologies applicable to the production of meat and fat to replace animal slaughter. [0022]. It is yet another objective of the present invention to provide microcarriers that allow cell differentiation, such as muscle and fat. SUMMARY OF THE INVENTION [0023]. The present invention achieves these and other objectives through a microcarrier production process that comprises: - selection of appropriate vegetable regions; - decellularization of said vegetables and production of microcarriers; - chemical and thermal processing of microcarriers; - arrangement of microcarriers for adhesion of cells capable of adhesion. [0024]. The present invention achieves these and other objectives through microcarriers obtained from the above process. [0025]. Furthermore, the present invention achieves these and other objectives through the use of said microcarriers to produce material similar to meat and fat of animal origin. DETAILED DESCRIPTION OF THE DRAWINGS [0026]. The present invention is better detailed through the attached figures: [0027]. Figure 1 is an image of the final result of the microcarrier object of the present invention; [0028]. Figure 2 is a first preferred embodiment of use/application of the object of the present invention; [0029]. Figure 3 is a second preferred embodiment of use/application of the object of the present invention; [0030]. Figure 4 is a graph that illustrates the results of DNA quantification after a certain period in cultivation. DETAILED DESCRIPTION OF THE INVENTION [0031]. The present invention relates to a microcarrier production process comprising: - selection of appropriate vegetable regions; - decellularization of said vegetables and production of microcarriers; - chemical and thermal processing of microcarriers; - arrangement of microcarriers for adhesion of cells capable of adhesion. [0032]. In a preferred embodiment of the present invention, the microcarrier production process comprises: - selection of appropriate vegetable regions; - decellularization of said vegetables and preparation of microcarriers; - chemical and thermal processing of microcarriers; - arrangement of microcarriers for adhesion of cells capable of adhesion. [0033]. The microcarriers prepared through the above process are indicated for production in bioreactors of meat or fat similar to products of animal origin. [0034]. A microcarrier or microtransporter is a support matrix that allows the growth of adherent cells in bioreactors. Instead of on a flat surface, cells are grown on the surface of microcarriers so that each particle carries several hundred cells, and therefore the expansion capacity can be multiplied several times. It provides a simple way to scale up cultural systems for industrial production of cell- or protein-based therapies, or for research purposes. [0035]. The advantages of applying microcarrier technology in the biotechnology industry include (a) ease of scaling, (b) ability to precisely control cell growth conditions in bioreactors even with remote control, (c) significant reduction in space required for manufacturing operation , (d) relevant reduction in technical work and (e) a more natural environment for cell culture that promotes differentiation. [0036]. In order to develop microcarriers that allow cell expansion in bioprocesses and that are edible, it was decided to use vegetables. In a preferred embodiment, it was decided to use broccoli florets due to their appearance similar to a microcarrier, which simplifies the process and is a relevant technical advantage. [0037]. In alternative embodiments of the present invention, other Vegetables can be used to prepare microcarriers such as spinach, lettuce, cauliflower, peas, kale and other vegetables with similar characteristics. [0038]. For the present invention, appropriate vegetable regions are used. In preferred embodiments, the selection of vegetables is carried out according to size (less than 500um) and rounded shape. [0039]. Next, the vegetables undergo a decellularization technique and are then decellularized. Decellularization consists of a technique that involves removing cells from a tissue or organ, leaving only the structure that surrounds them, this being the extracellular matrix. [0040]. This process involves exposing living tissues to a sequence of detergents to remove intracellular components, leaving behind the extracellular matrix intact. Furthermore, plant cell walls, after undergoing plant decellularization, are mainly composed of cellulose, pectin and hemicellulose. Therefore, they are nutritionally beneficial in most diets. [0041]. The detergent will be selected from combinations of ionic detergents and non-ionic detergents, whether or not including disinfectants. Examples of detergents that can be used in this process, but not limited to these, are: combined use of ionic (cetyltrimethylammonium bromide) and non-ionic detergents such as octyl phenol ethoxylate (Triton®-x-100) and digitonin. Detergents can be combined with the use of disinfectants. Preferably, detergents between 2% and 16% are used, preferably in the following concentration ranges: between 2 and 4%; between 4.1 and 6%; between 6.1% and 8%; between 8.1 and 10%; between 10.1 and 12%, between 12.1% and 14%, between 14.1 and 16%. [0042]. This step takes place at a temperature that varies between 2°C and 34°C, preferably being one of the following temperature ranges: between 2°C and 6°C; between 6.1°C and 10°C; between 10.1°C and 14°C; between 14°C and 18°C; between 18°C and 22°C; between 22°C and 26°C; between 26°C and 30°C; between 30°C and 34°C. Preferably, in this case, a refrigerator and oven are used to reach said temperatures. [0043]. At this stage, exchanges also occur, preferably between 5 and 8 exchanges; between 9 and 12 exchanges; between 13 and 16 exchanges; between 17 and 20 exchanges; under agitation of the mixture reached 0 rpm to 200 rpm; 200rpm to 400rpm; 400rpm to 600rpm; 600rpm to 800rpm preferably using a magnetic stirrer. [0044]. Following the preparation of the microcarriers, a thermal and chemical procedure is carried out. This procedure allows the improvement of cell adhesion. [0045]. Chemical processing involves the use of different concentrations of inorganic salt solution that contains cation and anion. Together, temperature cycles are carried out with the microcarriers soaked in solution for a determined period of time. [0046]. In preferred embodiments, inorganic salt such as potassium periodate is used in concentrations ranging from 0.004 mg/ml to 14 mg/ml, preferably between 0.004 mg/ml to 0.04 mg/ml; from 0.04 mg/ml to 0.4 mg/ml; from 0.4 mg/ml to 4 mg/ml; from 4 mg/ml to 14 mg/ml of salt in H20 solution at a temperature ranging between 35°C and 65°C, preferably 35°C to 45°C, 46°C to 55°C and 56°C at 65°C temperatures are reached using an oven in a period of time that varies between 20 and 40 minutes per cycle; between 40 and 80 minutes per cycle; between 80 and 120 minutes per cycle; between 120 and 160 minutes per cycle. Preferably, the number of cycles varies between 2 to 4 cycles of salt exposure; 3 to 5 cycles of salt exposure; 4 to 6 cycles of salt exposure. [0047]. Next, cells of animal origin are added to assess cell viability for at least 7 days, preferably for a period that varies between 7 and 35 days. At the end of this period, DNA extraction is performed to evaluate the quality of the decellularization step as well as maintaining the viability of the cells during this period when in contact with the microcarriers of the present invention. [0048]. In order for the present invention to be tested in order to prove its effectiveness, the following test protocol was developed: [0049]. (A) DNA extraction protocol: a. Macerate a sample of the selected vegetable with a buffer solution; B. Vortex; w. Add Proteinase K (20mg/mL) and 15 µl of 10% SDS; d. Incubate at a temperature of 37°C until the sample breaks down and completes digestion; It is. Centrifuge for 2 min at a speed of 12,000 rpm; f. Transfer the collected supernatant to another reaction tube; g. Add phenol (buffered pH 8) in proportion to the volume of the supernatant collected; H. Homogenize for a period of 10 min, turning the tubes gently; i. Centrifuge for a period of 5 min at 12,000 rpm, at a temperature of 10°C; j. Transfer the supernatant (aqueous phase) to a new tube reaction; k. Add chloroform/isoamyl alcohol in proportion to the volume of supernatant collected; l. Shake for a period of 5 minutes with your hands; m. Centrifuge for a period of 5 min at 12,000 rpm; n. Transfer the supernatant to a new reaction tube; O. Optionally, add NaCl until a final concentration of 0.3M is reached; P. Add ice-cold absolute ethanol (at a temperature of - 20°C) in a proportion of 2x the volume collected in step n; q. Shake the system by inverting the tube a few times; r. Incubate the system at -20°C for a period of 30 min; s. Centrifuge for a period of 30 min at a speed of 14,000 rpm at a temperature of 10°C; t. Discard the ethanol and add 1 mL of 70% alcohol; u. Centrifuge for a period of 5 min at a speed of 14,000 rpm at a temperature of 10°C; v. Discard the supernatant, dry the pellet on paper towel; w. Resuspend the pellet in a solution of 50 µl of TE (Tris-Edta) + 0.5 µl of RNAse A; x. Incubate at a temperature of 37°C for a period of 20 min; y. Quantification is carried out in absorbance for a specific range of DNA (result in ng/ l); [0050]. Figure 1 illustrates the final result of the microcarrier object of the present invention, which clearly illustrates the application of the decellularization technique to an appropriate region of the selected vegetable. [0051]. Figure 2 illustrates the result of applying the present invention to a caramel food mixture. [0052]. Figure 3 illustrates the result of applying the present invention to a meat product (sausage). [0053]. Figure 4 illustrates the result of DNA quantification. [0054]. Analyzing figure 4, it can be seen that there was a satisfactory result after the decellularization of the vegetable. In the groups containing the cells, it was observed that the cells maintained their viability with and without the presence of the microcarrier for 7 days. [0055]. Figure 4 presents DNA quantification data from the groups described above. Below is the caption to figure 4: - MCdp = decellularized microcarrier with thermal and chemical processing (present invention); - MCd = decellularized microcarrier (result of the first two steps of the process of the present invention); - CA + MCdp = animal cells adhered to the microcarrier of the present invention; - CA + MCd = animal cells adhered to the decellularized microcarrier (result of the first two steps of the process of the present invention); - CA = animal cells. [0056]. This graph (figure 4) illustrates that the process of the present invention offers significant results in terms of the number of cells adhered to the microcarrier, proving what is proposed. It was observed that the quantification of DNA, which is related to the number of cells, was higher in the CA + MCdp group compared to the CA + MCd group. [0057]. Considering the results achieved, it can be understood that there is potential for cell proliferation in the microcarriers of present invention for a longer period of time. [0058]. The present invention presents numerous technical and economic advantages when compared to the state of the art, some of which are listed below: ✓ The microcarriers of the present invention allow cell expansion in bioprocesses; ✓ The microcarriers of the present invention are edible; ✓ The microcarriers of the present invention have a manufacturing cost that does not increase the price of the final product; ✓ The microcarriers of the present invention do not affect the flavor and quality of the final product; ✓ The microcarriers of the present invention are indicated for the production of cultured animal fat; ✓ The microcarriers of the present invention can contribute to the nutritional properties of the final product; ✓ The microcarriers of the present invention promote the adherence of cells of animal origin to quickly enter a differentiation stage; ✓ The microcarriers of the present invention have good biocompatibility and allow cell adhesion and proliferation; ✓ The microcarriers of the present invention are applicable to the production of meat and fat to replace animal slaughter; ✓ The microcarriers of the present invention allow cell differentiation, such as in muscle and fat. [0059]. Having described an example of a preferred embodiment of the present invention, it must be understood that the scope of the present invention covers other possible variations of the described inventive concept, being limited only by the content of the appended claims, including possible equivalents.

Claims

REIVINDICAÇÕES 1. Processo de produção de microcarreadores caracterizado por compreender as seguintes etapas: a. seleção de regiões apropriadas de hortaliças; b. descelularização das ditas hortaliças e confecção dos microcarreadores; c. processamento químico e térmico dos microcarreadores; d. disposição dos microcarreadores para aderência de células aptas para adesão. 2. Processo de acordo com a reivindicação 1 caracterizado por a etapa a. considerar o tamanho das regiões da hortaliça sendo menor que 500µm e formato arredondado. 3. Processo de acordo com a reivindicação 1 ou 2 caracterizado por a etapa b. exposição de tecidos vivos a uma sequência de detergentes para remover componentes intracelulares. 4. Processo de acordo com a reivindicação 3 caracterizado por o detergente ser selecionado dentre combinações entre detergentes iônicos e detergentes não-iônicos compreendendo ou não desinfetantes. 5. Processo de acordo com a reivindicação 4 caracterizado por o detergente iônico ser brometo de cetriltrimetilamônio e o detergente não-iônico ser selecionado entre octil fenol etoxilato, digitonina e mistura destes. 6. Processo de acordo com qualquer uma das reivindicações 1 a 5 caracterizado por a etapa c. adicionar os microcarreadores da etapa b. em uma solução de sal inorgânico compreendendo cátion e ânion sendo submetida a ciclos de temperaturas em período de tempo determinado. 2/2 7. Processo de acordo com a reivindicação 6 caracterizado por o sal inorgânico é periodato de potássio em uma concentração que varia entre 0,004 mg/ml a 14 mg/ml. 8. Microcarreadores caracterizados por serem obteníveis por meio do processo conforme definido em qualquer uma das reivindicações 1 a 7. 9. Uso de microcarreadores conforme definidos na reivindicação 8 caracterizado por ser para aplicação em processo de produção de material similar a carne e gordura de origem animal. 10. Uso de microcarreadores, de acordo com a reivindicação 9, caracterizado por os ditos microcarreadores aderirem a células selecionadas aptas a proliferação e diferenciação. CLAIMS 1. Microcarrier production process characterized by comprising the following steps: a. selection of appropriate vegetable regions; B. decellularization of said vegetables and production of microcarriers; w. chemical and thermal processing of microcarriers; d. arrangement of microcarriers for adhesion of cells capable of adhesion. 2. Process according to claim 1 characterized by step a. consider the size of the vegetable regions to be less than 500µm and round in shape. 3. Process according to claim 1 or 2 characterized by step b. exposure of living tissues to a sequence of detergents to remove intracellular components. 4. Process according to claim 3, characterized in that the detergent is selected from combinations of ionic detergents and non-ionic detergents comprising or not disinfectants. 5. Process according to claim 4, characterized in that the ionic detergent is cetyltrimethylammonium bromide and the non-ionic detergent is selected from octyl phenol ethoxylate, digitonin and a mixture thereof. 6. Process according to any one of claims 1 to 5 characterized in that step c. add the microcarriers from step b. in an inorganic salt solution comprising cation and anion being subjected to temperature cycles over a determined period of time. 2/2 7. Process according to claim 6 characterized in that the inorganic salt is potassium periodate in a concentration ranging between 0.004 mg/ml to 14 mg/ml. 8. Microcarriers characterized by being obtainable through the process as defined in any one of claims 1 to 7. 9. Use of microcarriers as defined in claim 8 characterized by being for application in a process of producing material similar to meat and fat of origin animal. 10. Use of microcarriers, according to claim 9, characterized in that said microcarriers adhere to selected cells capable of proliferation and differentiation.
PCT/BR2023/050382 2022-11-09 2023-11-09 Method for producing microcarriers, said microcarriers and use of said microcarriers Ceased WO2024098130A1 (en)

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