WO2022264244A1 - Tobacco product - Google Patents
Tobacco product Download PDFInfo
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- WO2022264244A1 WO2022264244A1 PCT/JP2021/022621 JP2021022621W WO2022264244A1 WO 2022264244 A1 WO2022264244 A1 WO 2022264244A1 JP 2021022621 W JP2021022621 W JP 2021022621W WO 2022264244 A1 WO2022264244 A1 WO 2022264244A1
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- flow path
- raw material
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- tobacco product
- mesh member
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/40—Constructional details, e.g. connection of cartridges and battery parts
Definitions
- the present invention relates to tobacco products, more particularly, raw materials comprising pieces of Nicotiana plants (cut tobacco) or reconstituted products (reconstituted tobacco or reconstituted tobacco granules) consisting of fines of Nicotiana plants downstream of an aerosol-generating unit.
- tobacco products comprising an ingredient holding unit including a filling section.
- Non-combustible tobacco products are known in which vapors or aerosols are generated from an aerosol-generating substrate by electrical power supplied from a battery, passed through a tobacco-containing material, and the vapors or aerosols include tobacco components (e.g., Patent document 1).
- an object of the present invention is to provide a non-combustible tobacco product that supplies a predetermined amount of flavor components throughout smoking.
- a non-combustible tobacco product having a specific structure solves the above problems. That is, the above problems are solved by the present invention described below.
- a tobacco product comprising a raw material holding portion into which vapor or aerosol generated in the atomizing portion flows, In the raw material holding part, a region filled with a raw material containing pieces or dust of a Nicotiana plant, and a first net-like member arranged upstream of the region for sealing the raw material, Sa is the area of the image formed by vertically projecting the downstream end face of the flow channel in the atomizing section onto a plane perpendicular to the flow channel direction; When the area of the image formed by projection is S1, Sa ⁇ S1, A downstream end of the flow path in the atomizing section and the first mesh member are separated from each other, tobacco products.
- the tobacco product according to (1) further comprising a second mesh member downstream of the region where the raw material containing the Nicotiana plant pieces or dust is filled.
- the flow path direction length L of the spaced portion satisfies the following relationship: L ⁇ 0.05M (M is the maximum distance in the flow path direction between the downstream side surface of the first net member and the inner wall of the downstream end of the raw material holding portion when the second net member is not present, When the second net-like member exists, it is the maximum distance in the flow direction between the downstream side of the first net-like member and the upstream side of the second net-like member)
- M is the maximum distance in the flow path direction between the downstream side of the first net-like member and the upstream side of the second net-like member
- the flow path direction length L of the spaced portion satisfies the following relationship: L ⁇ 0.05M′ (M' is the maximum distance in the flow path direction between the downstream side of the flow path portion of the first mesh member and the inner wall of the downstream end of the raw material holding portion when the second mesh member does not exist, When the second mesh member exists, it is the maximum distance in the flow path direction between the downstream side of the flow path portion of the first mesh member and the upstream side of the flow path portion of the second mesh member)
- M' is the maximum distance in the flow path direction between the downstream side of the flow path portion of the first mesh member and the upstream side of the flow path portion of the second mesh member
- Diagram showing one aspect of an infused tobacco product Conceptual diagram for explaining the structure of the raw material holder Diagram explaining the structure of the cartridge Diagram explaining the structure of the cartridge A diagram for explaining an example of the power supply unit 10 Figure showing the results of Example A and Comparative Example A Figure showing the results of Example B Figure showing the results of Example C
- the tobacco product of the present invention comprises an atomizing part and a raw material holding part into which vapor or aerosol generated by the atomizing part flows.
- a raw material filling region including tobacco and a first net member are arranged upstream of the region for sealing the raw material.
- a widened portion is provided in the flow path of the vapor or aerosol. Specifically, the width of the flow path of the raw material holding portion is wider than that of the flow path at the end of the atomizing portion. Furthermore, the downstream end of the flow path in the atomizing section and the first mesh member are separated from each other.
- a tobacco-containing product comprising an ingredient holding unit containing is hereinafter also referred to as an "infused tobacco product".
- Infused tobacco products include a type that generates vapor or aerosol by heating an aerosol source such as glycerin, and a type that generates aerosol by applying vibration to the aerosol source.
- the infused tobacco product of the present invention may be of any type, but for the sake of brevity, the present invention will be described using the aforementioned types as examples.
- Fig. 1 shows one embodiment of the infused tobacco product of the present invention.
- 1 is an infused tobacco product
- 10 is a power supply unit
- 20 is a cartridge
- 30 is an atomizing section
- 40 is a raw material holding section. Vapor or aerosol generated in the atomizing section 30 is introduced into the raw material holding section 40 and flows to the mouthpiece end 3 .
- the non-mouthpiece end 2 side is called upstream, and the mouthpiece end 3 side is called downstream.
- the raw material holding part 40 also functions as a mouthpiece.
- FIG. 2 is a conceptual diagram illustrating the structure of the raw material holding unit 40.
- 40 is a raw material holding portion, and 41 is a spacing portion.
- 42 is a first net-like member
- 44 is a second net-like member
- 43 is an outer frame
- 46 is a raw material filling area
- 48 is an upstream end
- 49 is a downstream end.
- the first net-like member 42 and the second net-like member 44 seal the raw material and prevent the raw material filling area from moving.
- the second net-like member 44 is arranged in this aspect, the second net-like member 44 may be omitted.
- the atomizing section 30 is present upstream of the raw material holding section 40, and the downstream end of the flow path 38 in the atomizing section 30 and the outer frame 43 are joined or joined together.
- a method of joining the two members there is a method of utilizing the force of attraction between the permanent magnet embedded in the atomizing portion and the magnetic material embedded in the outer frame 43, and a method of fitting the two members together.
- the area S1 of the image formed by vertical projection onto the plane perpendicular to the direction satisfies the relationship Sa ⁇ S1.
- Sa is the area of the cross section perpendicular to the flow direction of the flow path 38 at the connecting portion between the atomizing portion 30 and the raw material holding portion 40 .
- S1 is the area of the cross section perpendicular to the flow direction of the portion of the first mesh member 42 that functions as the flow path.
- Sa and S1 are adjusted by the shape of the raw material holding portion 40, but S1 can also be adjusted by masking a part of the first mesh member 42 or the like.
- Said S1 is preferably 3 to 10 times greater than Sa.
- S1 is between 20 and 80 mm 2 in one aspect.
- the shape of the raw material holding part 40 is not limited, and can be a cylinder, a cube, or a rectangular parallelepiped. In this case, the diameter or width is appropriately adjusted so as to satisfy the relationship between S1 and Sa. In one aspect, the diameter or width is about 10 to 20 mm.
- the first mesh member 42 and the downstream end of the flow path 38 in the atomizing section are separated from each other. If the two are in contact with each other, the aerosol introduced from the atomizing part will condense in the first net-like member 42, causing clogging of the first net-like member 42. As a result, the supply amount of the flavor component will decrease during smoking. decreases or stops. However, in the present invention, since the first mesh member 42 and the downstream end of the flow path 38 in the atomizing section are spaced apart, the condensation can be avoided, and as a result, a sufficient amount of the flavor component can be produced throughout smoking. supplied.
- the length L of the spaced portion in the direction of the flow path (hereinafter also referred to as the “spacing distance L”) is preferably 0.5 mm or more, and more preferably 1.0 mm or more.
- the upper limit is preferably 7.5 mm or less.
- the separation distance L preferably satisfies the relationship of L ⁇ 0.05M, and more preferably satisfies the relationship of L ⁇ 0.08M.
- M is the maximum distance (inner dimension distance) in the flow direction between the downstream side surface of the first net member 42 and the upstream side surface of the second net member 44 in the embodiment of FIG. 2(1) where the second net member is present. be. That is, M is the distance between the downstream major surface of the first mesh member 42 and the upstream major surface of the second mesh member 44 .
- M is the distance between the downstream major surface of the first mesh member 42 and the upstream major surface of the second mesh member 44 .
- M in a mode in which the first net-like member 42 is provided so as not to be perpendicular to the flow path direction, M is the downstream main surface of the first net-like member 42 and the is the maximum distance in the flow direction of the upstream main surface of the Further, in a mode in which the second net-like member 44 is not provided, M is the maximum distance (inner dimension distance) between the first net-like member 42 and the inner wall of the downstream end of the raw material holding portion 40 in the flow path direction. That is, in this case, M is the maximum distance in the flow path direction between the downstream main surface of the first mesh member 42 and the inner wall of the downstream end of the raw material holding portion.
- the value of M is appropriately adjusted in relation to the filling amount of the raw material, but in one aspect, it is about 8 to 15 mm.
- the upper limit value of L is appropriately adjusted within a relationship in which the total length of the raw material holding portion 40 in the flow path direction is optimally distributed by the separation distance L and the raw material filling portion length M, etc., and within a range in which the aerosol does not aggregate on the inner wall of the separation portion. is preferably L ⁇ 0.5M.
- the above L preferably satisfies the relationship of M′ and L ⁇ 0.05M′, and the relationship of L ⁇ 0.08M′ is satisfied. It is more preferable to satisfy M′ is the maximum distance (inner dimension distance) in the flow path direction between the downstream side surface of the flow path portion of the first mesh member 42 and the inner wall of the downstream end of the raw material holding portion 40 when the second mesh member 44 is not present. , and when the second mesh member 44 is present, it is the maximum distance in the flow direction between the downstream side of the flow path portion of the first mesh member 42 and the upstream side of the flow path portion of the second mesh member 44 . As shown in FIG.
- M and M' are the same in the aspect in which the first mesh member 42 is provided substantially perpendicular to the flow path direction.
- M and M' are different.
- M′ is specifically the maximum distance (inner dimension distance) in the flow direction between the portion of the first mesh member 42 functioning as the flow path and the portion of the second mesh member 44 functioning as the flow path. .
- Net-like member is a member having a net-like structure.
- the net-like member there are a non-woven fabric in which a plurality of fibers are randomly crossed to form a net-like structure, a mesh in which fibers are regularly crossed to form a net steel structure, and a plate-like member with openings. mentioned.
- Non-woven fabric is composed of fibers.
- the fibers are not limited, for example, polyolefin fibers such as polypropylene fibers and polyethylene fibers, polyester fibers such as polyethylene terephthalate fibers, and biodegradable materials such as natural fibers, cellulose fibers, wood pulp fibers, gramineous plant fibers, and agave. plant fiber, sisal fiber, mallow plant fiber, jute fiber, polylactic acid fiber, and the like.
- the nonwoven fabric may contain one kind of these fibers, or may contain two or more kinds. It is preferable that the nonwoven fabric and the outer frame body 43 are made of the same material because they can be welded together.
- the material of the outer frame 43 is preferably polyolefin, more preferably polypropylene. Therefore, the fibers are preferably polyolefin fibers, more preferably polypropylene fibers. Polypropylene sorbs a smaller amount of nicotine during storage, and can further suppress the decrease in the amount of nicotine before use.
- the material of the outer frame 43 is preferably polyester, more preferably PET. Therefore, the fibers are preferably polyester fibers, and more preferably PET fibers. PET fibers sorb less nicotine during storage, and can further suppress the decrease in the amount of nicotine before use.
- the density of the nonwoven fabric is preferably 0.04 g/cm 3 or more, more preferably 0.06 g/cm 3 or more, and still more preferably 0.08 g/cm 3 from the viewpoint of strength and raw material sealing properties. That's it.
- the upper limit is preferably 0.24 g/cm 3 or less, more preferably 0.20 g/cm 3 or less, still more preferably 0.15 g/cm 3 or less, from the viewpoint of ease of inhalation and nicotine filterability.
- the air permeability of the nonwoven fabric 42 is preferably 100 cc/cm 2 /sec or more, more preferably 150 cc/cm 2 /sec or more, from the viewpoint of aerosol breathability.
- the upper limit is preferably 1000 cc/cm 2 /sec or less, more preferably 500 cc/cm 2 /sec or less, from the viewpoint of the raw material sealing properties.
- the air permeability of a nonwoven fabric can be measured by a JIS air permeability test (L 1096).
- Nonwoven 44 may be of the same construction and structure as nonwoven 42 .
- Meshes include metal meshes or polymer meshes.
- the specification of the metal or polymer mesh may be a porosity ( ⁇ ) of 30% or more and 70% or less.
- the wire diameter (d) of the wire may be 0.1 mm or less in the case of metal mesh.
- the mesh size (A) of the wire may be 0.10 to 1.50 (mm).
- a metal plate (punching metal) in which holes are regularly drilled can be used as a plate-shaped member provided with openings.
- a hole opening method may be either a laser hole opening method or an etching method.
- the thickness of the mesh member 42 is preferably 5 mm or less, more preferably 3 mm or less, and even more preferably 2 mm or less. From the viewpoint of improving the strength, the lower limit is preferably 0.5 mm or more, more preferably 0.7 mm or more, and even more preferably 1.0 mm or more.
- the raw material filling region is filled with a raw material (hereinafter also referred to as "raw material piece") containing pieces or dust of Nicotiana plants.
- raw material pieces shredded tobacco, a molded product obtained by molding tobacco raw material into granules, and the like can be used.
- the raw material filling area may be filled with plants other than tobacco (for example, mints, herbs, etc.).
- a raw material containing tobacco may be added with a flavor such as menthol.
- the size of the raw material pieces is preferably 0.2-2.0 mm, more preferably 0.4-1.0 mm. The smaller the size of the raw material pieces, the greater the specific surface area, so that the flavor and taste components are more likely to be released.
- the raw material pieces are obtained by sieving according to JIS Z 8815 using a stainless steel sieve according to JIS Z 8801, for example.
- a stainless steel sieve with an opening of 0.71 mm the raw material pieces are sieved for 20 minutes by a dry and mechanical shaking method to pass through a stainless steel sieve with an opening of 0.71 mm.
- the filling amount of raw material pieces is preferably 300 mg or more, more preferably 350 mg or more.
- the cartridge 20 accommodates the atomization section 30 and the raw material holding section 40 .
- 3 and 4 are diagrams for explaining the structure of the cartridge.
- 30 is an atomizing section
- 40 is a raw material holding section.
- the cartridge 20 has a reservoir 21 , an atomizing device 22 , a channel forming body 23 and an outer frame body 24 .
- the cartridge 20 has a first channel 20X arranged downstream of the atomization device 22 as an aerosol channel.
- the reservoir 21 stores the aerosol source 21A.
- the reservoir 21 is positioned around the flow path forming body 23 in a cross section orthogonal to the flow direction of the aerosol.
- the reservoir 21 is positioned within the gap between the flow path forming body 23 and the outer frame body 24 .
- the reservoir 21 is made of, for example, a porous material such as a resin web or cotton.
- the reservoir 21 may be configured by a tank containing a liquid aerosol source 21A.
- the aerosol source 21A include glycerin and propylene glycol.
- the atomization device 22 atomizes the aerosol source 21A without combustion by the electric power supplied from the battery 11.
- the atomization device 22 is composed of a heating wire (coil) wound at a predetermined pitch.
- the atomization device 22 is preferably composed of a heating wire having a resistance value in the range of 1.0-3.0 ⁇ .
- the predetermined pitch is equal to or greater than the value at which the heating wire does not contact, and is preferably smaller.
- the predetermined pitch is preferably 0.40 mm or less, for example.
- the predetermined pitch is preferably constant in order to stabilize the atomization of the aerosol source 21A.
- the predetermined pitch is the interval between the centers of the heating wires adjacent to each other.
- the channel forming body 23 has a cylindrical shape that forms the first channel 20X extending along the flow direction of the aerosol.
- the outer frame body 24 has a cylindrical shape that accommodates the flow path forming body 23 .
- the outer frame body 24 accommodates a portion of the tobacco capsule 30 .
- the cartridge 20 is detachable from the power supply unit 10. Also, the raw material holding unit 40 is detachable from the cartridge 20 . That is, the cartridge 20 and the raw material holding portion 40 are each replaceable.
- the power supply unit 10 shown in FIG. 5 has a battery 11 .
- the battery 11 may be a disposable type battery or a rechargeable type battery.
- the initial value of the output voltage of the battery 11 is preferably in the range of 1.2V or more and 4.2V or less.
- the battery capacity of the battery 11 is preferably in the range of 100 mAh or more and 1000 mAh or less.
- Example A1 A rectangular parallelepiped raw material holding portion shown in FIG. 2(1) was prepared.
- the outer frame body of the raw material holding part was made of a transparent resin (VisiJet M3 crystal) and molded using a 3D printer (ProJet 3600). Its dimensions were as shown in Table 1.
- a 1-mm-thick non-woven fabric obtained by blending polyolefin fibers, polypropylene fibers, and polyethylene was used as the mesh member.
- the infused tobacco product shown in FIG. 1 having the raw material holding portion is prepared, the aerosol flow is substantially vertical, and the raw material filled in the raw material filling portion covers the upper surface of the net-like member on the atomizing portion side.
- an automatic smoking device Borgwaldt, LM4E
- one Cambridge filter was placed between the infused tobacco product and the automatic smoking device, and the aerosol generated by the infused tobacco product was filtered through the Cambridge filter. made it possible to collect
- a Cambridge filter is a flat circular glass fiber filter with a diameter of about 44 mm and a thickness of 1.5 mm, and is well known and widely used by those skilled in the art as a filter capable of capturing particulate matter.
- Cambridge filters are available from Cambridge Filter Japan Co., Ltd., Borgwald (catalog number 8020 285 2), and the like.
- the automatic smoking machine can be used up to 100 times under the conditions according to the smoking test conditions of “CORESTA RECOMMENDED METHOD No.81 “ROUTINE ANALYTICAL MACHINE FOR E-CIGARETTE AEROSOL GENERATION AND COLLECTION - DEFINITIONS AND STANDARD CONDITIONS (June 2015)””. A smoking motion was performed.
- the following 5 sections 1st section (equivalent to 5 smoking actions): ⁇ 10 times, 2nd section (equivalent to smoking motion 20 times): ⁇ 30 times, 3rd section (equivalent to smoking motion 40 times): ⁇ 50 times, 4th section (equivalent to smoking motion 60 times): ⁇ 70 times, 5th section (equivalent to smoking motion 80 times): ⁇ 90 times, 6th section (equivalent to smoking motion 95 times): ⁇ 100 times, was set for machine smoking.
- the Cambridge filter that had collected the aerosol was placed in a screw bottle, and 10 ml of ethanol containing 0.4 mg/mL of 1,3-butanediol was added as an internal standard. The sample was shaken at 280 times/minute for 1 hour to extract the collected aerosol. The extract was subjected to gas chromatography analysis to measure the amount of nicotine. As part of the component analysis of the collected aerosol, we examined the extent to which the amount of nicotine exhaled from the infused tobacco product increases or decreases with repeated smoking motions. Nicotine was quantified by a method commonly used by those skilled in the art.
- the ethanol solution containing the collected aerosol was analyzed by GC-MS (manufactured by Agilent Technology, model number 5977B GC/MSD, gas type He, gas flow rate 1.3 ml/min, column DB-WAX 30 mm ⁇ 0.25 mm ⁇ 0 .25 ⁇ m), the content components were comparatively quantitatively analyzed.
- GC-MS manufactured by Agilent Technology, model number 5977B GC/MSD, gas type He, gas flow rate 1.3 ml/min, column DB-WAX 30 mm ⁇ 0.25 mm ⁇ 0 .25 ⁇ m
- Section 1 The amount of nicotine discharged from 0 to 10 times was divided by 10 to obtain the amount of nicotine discharged ( ⁇ g/puff) per smoking action. Similarly, for the 2nd to 6th segments, the quantitative results were divided by the number of smoking motions corresponding to the segments. Then, the nicotine ejection amount ( ⁇ g/puff) in the first interval was set to 100, and the ratio of the nicotine ejection amount in each interval was shown (FIG. 6).
- Example A2 A smoking test was conducted and evaluated in the same manner as in Example 1, except that L was 2 mm.
- Comparative Example A A smoking test was conducted and evaluated in the same manner as in Example 1, except that L was set to 0 mm.
- Example B A smoking test was conducted and evaluated in the same manner as in Example 1, except that the shape was changed as shown in Table 2. These results are shown in FIG.
- Example C A smoking test was conducted and evaluated in the same manner as in Example 1, except that the shape was changed as shown in Table 3. These results are shown in FIG.
- non-combustion tobacco product of the present invention supplies a predetermined amount of flavor components throughout smoking.
- infused tobacco product 1 non-mouth end 3 mouth end 10 power supply unit 11 battery 20 cartridge 20X first channel 21 reservoir 21A aerosol source 22 atomizing device 23 channel forming body 24 outer frame 30 atomizing section 38 channel 40 Raw material holding part 41 Spacing part 42 First mesh member, nonwoven fabric 43 Outer frame body 44 Second mesh member, nonwoven fabric 48 Upstream end 49 Downstream end
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Abstract
Description
本発明は、たばこ製品に関し、より詳しくはエアロゾル発生ユニットの下流にタバコ属植物の細片(刻みたばこ)または同植物の細粉からなる再構成物(再構成たばこまたは再構成たばこ顆粒)を含む原料充填部を含む原料保持ユニットを備えるたばこ製品に関する。 TECHNICAL FIELD The present invention relates to tobacco products, more particularly, raw materials comprising pieces of Nicotiana plants (cut tobacco) or reconstituted products (reconstituted tobacco or reconstituted tobacco granules) consisting of fines of Nicotiana plants downstream of an aerosol-generating unit. Tobacco products comprising an ingredient holding unit including a filling section.
電池から供給される電力によってエアロゾル発生基材から蒸気またはエアロゾルを発生させ、たばこを含む原料に通過させて、蒸気またはエアロゾルにたばこ成分を含ませる非燃焼型たばこ製品が知られている(例えば、特許文献1)。 Non-combustible tobacco products are known in which vapors or aerosols are generated from an aerosol-generating substrate by electrical power supplied from a battery, passed through a tobacco-containing material, and the vapors or aerosols include tobacco components (e.g., Patent document 1).
非燃焼型たばこ製品にも、燃焼型たばこ製品と同様に、吸引時に香味成分が所定の量で供給されることが望まれている。しかし、従来の非燃焼型たばこ製品においては、特に喫煙の後期において十分な香味成分の供給が達成されない傾向があり、改善が望まれていた。かかる事情に鑑み、本発明は喫煙の終始にわたって香味成分が所定の量で供給される非燃焼型たばこ製品を提供することを課題とする。 As with combustible tobacco products, it is desired that a predetermined amount of flavor components be supplied to non-combustible tobacco products at the time of inhalation. However, conventional non-combustion tobacco products tend not to supply sufficient flavoring components, especially in the later stages of smoking, and improvements have been desired. In view of such circumstances, an object of the present invention is to provide a non-combustible tobacco product that supplies a predetermined amount of flavor components throughout smoking.
発明者らは、特定の構造を有する非燃焼型たばこ製品が前記課題を解決することを見出した。すなわち、前記課題は以下の本発明によって解決される。
(1)霧化部と、
霧化部で発生された蒸気またはエアロゾルが流入される原料保持部と、を備えるたばこ製品であって、
前記原料保持部内に、タバコ属植物の細片または細粉を含む原料が充填される領域と、当該原料を封止するために当該領域の上流側に配置された第1網状部材とを備え、
前記霧化部における流路の下流端面を流路方向に垂直な面に垂直投影して形成された像の面積をSa、前記第1網状部材における流路面を流路方向に垂直な面に垂直投影して形成された像の面積をS1とするとき、Sa<S1であり、
前記霧化部における流路の下流端と前記第1網状部材が離間されている、
たばこ製品。
(2)前記タバコ属植物の細片または細粉を含む原料が充填される領域の下流に第2網状部材をさらに備える、(1)に記載のたばこ製品。
(3)前記離間部の流路方向長さLが、以下の関係を満たす、
L≧0.05M
(Mは、第2網状部材が存在しない場合は、第1網状部材の下流側面と原料保持部の下流端内壁との流路方向における最大距離、
第2網状部材が存在する場合は、第1網状部材の下流側面と第2網状部材の上流側面との流路方向における最大距離である)
(1)または(2)に記載のたばこ製品。
(4)前記離間部の流路方向長さLが、以下の関係を満たす、
L≧0.05M’
(M’は、第2網状部材が存在しない場合は、第1網状部材の流路部分の下流側面と原料保持部の下流端内壁との流路方向における最大距離、
第2網状部材が存在する場合は、第1網状部材の流路部分の下流側面と第2網状部材の流路部分の上流側面との流路方向における最大距離である)
(1)~(3)のいずれかに記載のたばこ製品。
(5)前記Lが、1mm以上である、(1)~(4)のいずれかに記載のたばこ製品。
(6)S1とSaが以下の関係を満たす、
3Sa≦S1≦10Sa
(1)~(5)のいずれかに記載のたばこ製品。
(7)前記S1が20~80mm2である、(1)~(6)のいずれかに記載のたばこ製品。
(8)前記第2網状部材における流路面を流路方向に垂直な面に垂直投影して形成された像の面積をS2とするとき、S1>S2である、(2)~(7)のいずれかに記載のたばこ製品。
The inventors have found that a non-combustible tobacco product having a specific structure solves the above problems. That is, the above problems are solved by the present invention described below.
(1) an atomizing section;
A tobacco product comprising a raw material holding portion into which vapor or aerosol generated in the atomizing portion flows,
In the raw material holding part, a region filled with a raw material containing pieces or dust of a Nicotiana plant, and a first net-like member arranged upstream of the region for sealing the raw material,
Sa is the area of the image formed by vertically projecting the downstream end face of the flow channel in the atomizing section onto a plane perpendicular to the flow channel direction; When the area of the image formed by projection is S1, Sa<S1,
A downstream end of the flow path in the atomizing section and the first mesh member are separated from each other,
tobacco products.
(2) The tobacco product according to (1), further comprising a second mesh member downstream of the region where the raw material containing the Nicotiana plant pieces or dust is filled.
(3) the flow path direction length L of the spaced portion satisfies the following relationship:
L≧0.05M
(M is the maximum distance in the flow path direction between the downstream side surface of the first net member and the inner wall of the downstream end of the raw material holding portion when the second net member is not present,
When the second net-like member exists, it is the maximum distance in the flow direction between the downstream side of the first net-like member and the upstream side of the second net-like member)
The tobacco product according to (1) or (2).
(4) the flow path direction length L of the spaced portion satisfies the following relationship:
L≧0.05M′
(M' is the maximum distance in the flow path direction between the downstream side of the flow path portion of the first mesh member and the inner wall of the downstream end of the raw material holding portion when the second mesh member does not exist,
When the second mesh member exists, it is the maximum distance in the flow path direction between the downstream side of the flow path portion of the first mesh member and the upstream side of the flow path portion of the second mesh member)
A tobacco product according to any one of (1) to (3).
(5) The tobacco product according to any one of (1) to (4), wherein L is 1 mm or more.
(6) S1 and Sa satisfy the following relationship,
3 Sa ≤ S1 ≤ 10 Sa
A tobacco product according to any one of (1) to (5).
(7) The tobacco product according to any one of (1) to (6), wherein S1 is 20-80 mm 2 .
(8) of (2) to (7), wherein S1>S2, where S2 is the area of an image formed by vertically projecting the flow path surface of the second mesh member onto a plane perpendicular to the flow path direction; A tobacco product according to any one of the preceding claims.
本発明によって、喫煙の終始にわたって香味成分が所定の量で供給される非燃焼型たばこ製品を提供できる。 According to the present invention, it is possible to provide a non-combustible tobacco product in which flavor components are supplied in a predetermined amount throughout smoking.
本発明のたばこ製品は、霧化部と、霧化部で発生された蒸気またはエアロゾルが流入される原料保持部とを備える。当該原料保持部内には、たばこを含む原料充填領域と、当該原料を封止するために当該領域の上流側に第1網状部材が配置されている。蒸気またはエアロゾルの流路には拡幅部が設けられており、具体的には霧化部の末端の流路に比べて、原料保持部の流路は拡幅されている。さらに霧化部における流路の下流端と前記第1網状部材は離間されている。 The tobacco product of the present invention comprises an atomizing part and a raw material holding part into which vapor or aerosol generated by the atomizing part flows. In the raw material holding portion, a raw material filling region including tobacco and a first net member are arranged upstream of the region for sealing the raw material. A widened portion is provided in the flow path of the vapor or aerosol. Specifically, the width of the flow path of the raw material holding portion is wider than that of the flow path at the end of the atomizing portion. Furthermore, the downstream end of the flow path in the atomizing section and the first mesh member are separated from each other.
本発明のたばこ製品のように、エアロゾル発生ユニットの下流にタバコ属植物の細片(刻みたばこ)または同植物の細粉からなる再構成物(再構成たばこまたは再構成たばこ顆粒)を含む原料充填部を含む原料保持ユニットを備えるたばこを含む製品を、以下「インフューズドたばこ製品」ともいう。インフューズドたばこ製品は、グリセリン等のエアロゾル源を加熱することによって蒸気やエアロゾルを発生するタイプと、エアロゾル源に振動を印加してエアロゾルを発生させるタイプが存在する。本発明のインフューズドたばこ製品はいずれのタイプでもよいが、説明を簡潔にするため、以下前記のタイプを例にして本発明を説明する。 Like the tobacco product of the present invention, a raw material filling section containing tobacco pieces (cut tobacco) or a reconstituted product (reconstituted tobacco or reconstituted tobacco granules) consisting of tobacco shavings downstream of the aerosol-generating unit. A tobacco-containing product comprising an ingredient holding unit containing is hereinafter also referred to as an "infused tobacco product". Infused tobacco products include a type that generates vapor or aerosol by heating an aerosol source such as glycerin, and a type that generates aerosol by applying vibration to the aerosol source. The infused tobacco product of the present invention may be of any type, but for the sake of brevity, the present invention will be described using the aforementioned types as examples.
本発明のインフューズドたばこ製品の一態様を図1に示す。図中、1はインフューズドたばこ製品、10は電源ユニット、20はカートリッジ、30は霧化部、40は原料保持部である。霧化部30で発生された蒸気またはエアロゾルは、原料保持部40に導入され、吸口端3へと流れる。非吸口端2側を上流、吸口端3側を下流という。原料保持部40はマウスピースの機能も兼ねる。
Fig. 1 shows one embodiment of the infused tobacco product of the present invention. In the figure, 1 is an infused tobacco product, 10 is a power supply unit, 20 is a cartridge, 30 is an atomizing section, and 40 is a raw material holding section. Vapor or aerosol generated in the atomizing
[原料保持部]
1)構造
図2は原料保持部40の構造を説明する概念図である。図中、40は原料保持部、41は離間部である。42は第1網状部材、44は第2網状部材、43は外枠体、46は原料充填領域、48は上流端、49は下流端である。第1網状部材42、第2網状部材44は原料を封止し、原料充填領域が移動することを防止する。本態様では第2網状部材44が配置されているが、第2網状部材44は省略することもできる。原料保持部40の上流には霧化部30が存在し、霧化部30における流路38の下流端と、外枠体43は、互いに接合されるか継ぎ合わされている。両部材を接合する方式としては、霧化部に埋め込まれた永久磁石と外枠体43に埋め込まれた磁性体が引きあう力を利用する方式や、両部材を嵌合する方式が挙げられる。流路38の下流端面(下流端の内周で形成される面)を流路方向に垂直な面に垂直投影して形成された像の面積Sa、前記第1網状部材における流路面を流路方向に垂直な面に垂直投影して形成された像の面積S1は、Sa<S1の関係を満たす。Saは、霧化部30と原料保持部40結合部における流路38の流れ方向に垂直な断面の面積である。同様にS1は第1網状部材42の流路として機能する部分の流れ方向に垂直な断面の面積である。SaおよびS1は原料保持部40の形状によって調整されるが、S1は第1網状部材42の一部をマスキングする等によっても調整できる。前記S1は、好ましくはSaの3~10倍である。またS1は、一態様において20~80mm2である。原料保持部40の形状は限定されず、円筒体、立方体、または直方体とすることができる。この場合、直径または幅は前記S1とSaの関係を満たすように適宜調整されるが、一態様において直径または幅は10~20mm程度である。
[Raw material holding part]
1) Structure FIG. 2 is a conceptual diagram illustrating the structure of the raw
第1網状部材42と霧化部における流路38の下流端は離間している。両者が接触していると、霧化部から導入されたエアロゾルが第1網状部材42中で結露し、第1網状部材42が目詰まりを起こし、この結果、喫煙の途中で香味成分の供給量が低下または停止してしまう。しかし、本発明においては、第1網状部材42と霧化部における流路38の下流端は離間しているので、前記結露を回避でき、その結果、喫煙の終始にわたり十分な量の香味成分が供給される。離間部の流路方向長さL(以下「離間距離L」ともいう)は具体的に、好ましくは0.5mm以上であり、より好ましくは1.0mm以上である。その上限は好ましくは7.5mm以下である。
The
離間距離Lは好ましくはL≧0.05Mの関係を満たし、より好ましくはL≧0.08Mの関係を満たす。Mは第2網状部材が存在する図2(1)の態様においては、第1網状部材42の下流側面と第2網状部材44の上流側面との流路方向における最大距離(内寸距離)である。すなわちMは、第1網状部材42の下流主面と第2網状部材44の上流主面の距離である。また、図2(2)に示すように第1網状部材42が流路方向に垂直とならないように設けられた態様においては、Mは第1網状部材42の下流主面と第2網状部材44の上流主面の流路方向の最大距離である。また第2網状部材44を設けない態様においては、Mは第1網状部材42と原料保持部40の下流端内壁との流路方向における最大距離(内寸距離)である。すなわちこの場合Mは、第1網状部材42の下流主面と原料保持部下流端内壁との流路方向における最大距離である。Mの値は、原料の充填量との関係で適宜調整されるが、一態様において8~15mm程度である。Lの上限値は、原料保持部40の流路方向における全長を、離間距離Lと原料充填部長さM等で最適配分する関係や、エアロゾルが離間部の内壁に凝集しない範囲で適宜調整されるが、好ましくはL≦0.5Mである。
The separation distance L preferably satisfies the relationship of L≧0.05M, and more preferably satisfies the relationship of L≧0.08M. M is the maximum distance (inner dimension distance) in the flow direction between the downstream side surface of the first
また、第1網状部材42の一部が流路を形成している場合、前記Lは、M’とL≧0.05M’の関係を満たすことが好ましく、L≧0.08M’の関係を満たすことがより好ましい。M’は、第2網状部材44が存在しない場合は、第1網状部材42の流路部分の下流側面と原料保持部40の下流端内壁との流路方向における最大距離(内寸距離)であり、第2網状部材44が存在する場合は、第1網状部材42の流路部分の下流側面と第2網状部材44の流路部分の上流側面との流路方向における最大距離である。図2(1)に示すように、第1網状部材42が流路方向に対し略垂直に設けられている態様においては、MとM’は同一である。一方、図2(2)に示すように第1網状部材42が流路方向に対し非垂直に設けられていて、かつ一部がマスキングされている態様においては、MとM’は異なる。この態様において、M’は具体的に第1網状部材42の流路として機能する部分と第2網状部材44の流路として機能する部分間の流路方向における最大距離(内寸距離)である。
Further, when a part of the
第2網状部材44における流路面を流路方向に垂直な面に垂直投影して形成された像の面積をS2とするとき、S1>S2であることが好ましい。
When the area of the image formed by vertically projecting the flow path surface of the
2)網状部材
網状部材とは、網状の構造を有する部材である。網状部材としては複数の繊維がランダムに交差して網状構造を形成している不織布や、繊維を規則的に交差させて網鋼構造を形成しているメッシュ、開口部を設けた板状部材が挙げられる。
2) Net-like member A net-like member is a member having a net-like structure. As the net-like member, there are a non-woven fabric in which a plurality of fibers are randomly crossed to form a net-like structure, a mesh in which fibers are regularly crossed to form a net steel structure, and a plate-like member with openings. mentioned.
不織布は繊維で構成される。当該繊維は限定されないが、例えばポリプロピレン繊維、ポリエチレン繊維等のポリオレフィン繊維、ポリエチレンテレフタラート繊維等のポリエステル繊維等、生分解性の素材として天然繊維、セルロース繊維、木材パルプ繊維、イネ科植物繊維、リュウゼツラン科植物繊維、サイザル麻繊維、アオイ科ソナツ属植物繊維、ジュート繊維、ポリ乳酸繊維等が挙げられる。不織布はこれらの繊維を一種含んでもよく、二種以上含んでもよい。不織布と外枠体43が同じ材料であると、両者を溶着させることができるので好ましい。一態様において外枠体43の材質は、ポリオレフィンが好ましく、ポリプロピレンがさらに好ましい。よって前記繊維としてはポリオレフィン繊維が好ましく、ポリプロピレン繊維がさらに好ましい。ポリプロピレンは、蔵置によるニコチンの収着量がより少なく、使用前におけるニコチン量の低減をより抑制できる。別態様において、外枠体43の材質は、ポリエステルが好ましく、PETがさらに好ましい。よって前記繊維としては、ポリエステル繊維が好ましく、PET繊維がより好ましい。PET繊維は、蔵置によるニコチンの収着量がより少なく、使用前におけるニコチン量の低減をより抑制できる。
Non-woven fabric is composed of fibers. Although the fibers are not limited, for example, polyolefin fibers such as polypropylene fibers and polyethylene fibers, polyester fibers such as polyethylene terephthalate fibers, and biodegradable materials such as natural fibers, cellulose fibers, wood pulp fibers, gramineous plant fibers, and agave. plant fiber, sisal fiber, mallow plant fiber, jute fiber, polylactic acid fiber, and the like. The nonwoven fabric may contain one kind of these fibers, or may contain two or more kinds. It is preferable that the nonwoven fabric and the
不織布の密度は、強度と原料の封止性の観点から、好ましくは0.04g/cm3以上であり、より好ましくは0.06g/cm3以上であり、さらに好ましくは0.08g/cm3以上である。その上限は、吸いやすさやニコチンの濾過性の観点から、好ましくは0.24g/cm3以下、より好ましくは0.20g/cm3以下、さらに好ましくは0.15g/cm3以下である。 The density of the nonwoven fabric is preferably 0.04 g/cm 3 or more, more preferably 0.06 g/cm 3 or more, and still more preferably 0.08 g/cm 3 from the viewpoint of strength and raw material sealing properties. That's it. The upper limit is preferably 0.24 g/cm 3 or less, more preferably 0.20 g/cm 3 or less, still more preferably 0.15 g/cm 3 or less, from the viewpoint of ease of inhalation and nicotine filterability.
不織布42の通気度は、エアロゾルの通気性等の観点から、100cc/cm2/sec以上であることが好ましく、150cc/cm2/sec以上であることがより好ましい。また、その上限は、原料の封止性の観点から、1000cc/cm2/sec以下であることが好ましく、500cc/cm2/sec以下であることがより好ましい。不織布の通気度は、JIS通気性試験(L 1096)により測定することができる。不織布44は不織布42と同じ構成および構造とすることができる。
The air permeability of the
メッシュとしては、金属メッシュまたはポリマーメッシュが挙げられる。金属またはポリマーメッシュの規格は、開孔率(ε)が30%以上、70%以下であってよい。開孔率(ε)は、メッシュを構成する各要素を用いて以下のように定義される。
開孔率(ε)=(A/(A+d))2×100
A:線材の目開き(単位mm)
d:線材の線径(単位mm)
線材の線径(d)としては金属メッシュの場合0.1mm以下であってよい。線材の目開き(A)は0.10~1.50(mm)であってよい。
Meshes include metal meshes or polymer meshes. The specification of the metal or polymer mesh may be a porosity (ε) of 30% or more and 70% or less. The porosity (ε) is defined as follows using each element that constitutes the mesh.
Porosity (ε) = (A/(A+d)) 2 × 100
A: Wire mesh opening (unit: mm)
d: Wire diameter of wire (unit: mm)
The wire diameter (d) of the wire may be 0.1 mm or less in the case of metal mesh. The mesh size (A) of the wire may be 0.10 to 1.50 (mm).
また開口部が設けられた板状部材としては、規則的に孔が穿たれた金属板(パンチングメタル)等が挙げられる。開孔方法はレーザー開孔法またはエッチング法のいずれでもよい。 A metal plate (punching metal) in which holes are regularly drilled can be used as a plate-shaped member provided with openings. A hole opening method may be either a laser hole opening method or an etching method.
網状部材42の厚みは、5mm以下であることが好ましく、3mm以下であることがより好ましく、2mm以下であることがさらに好ましい。また、その下限は、強度向上の観点から、0.5mm以上であることが好ましく、0.7mm以上であることがより好ましく、1.0mm以上であることがさらに好ましい。
The thickness of the
3)原料充填領域
原料充填領域には、タバコ属植物の細片または細粉を含む原料(以下「原料片」ともいう)が充填される。原料片としては、刻みたばこ、たばこ原料を粒状に成形した成形体等を用いることができる。原料充填領域には、たばこ以外の植物(例えば、ミント、ハーブ等)が充填されてもよい。また、たばこを含む原料には、メントールなどの香料が付与されていてもよい。原料片のサイズは、好ましくは0.2~2.0mm、より好ましくは0.4~1.0mmである。原料片のサイズが小さいほど、比表面積が増大するため、香喫味成分が放出されやすい。
3) Raw Material Filling Region The raw material filling region is filled with a raw material (hereinafter also referred to as "raw material piece") containing pieces or dust of Nicotiana plants. As raw material pieces, shredded tobacco, a molded product obtained by molding tobacco raw material into granules, and the like can be used. The raw material filling area may be filled with plants other than tobacco (for example, mints, herbs, etc.). In addition, a raw material containing tobacco may be added with a flavor such as menthol. The size of the raw material pieces is preferably 0.2-2.0 mm, more preferably 0.4-1.0 mm. The smaller the size of the raw material pieces, the greater the specific surface area, so that the flavor and taste components are more likely to be released.
ここで、前記原料片は、例えば、JIS Z 8801に準拠したステンレス篩を用いて、JIS Z 8815に準拠する篩分けによって得られる。例えば、0.71mmの目開きを有するステンレス篩を用いて、乾燥式かつ機械式振とう法によって20分間に亘って原料片を篩分けによって、0.71mmの目開きを有するステンレス篩を通過する原料片を得る。続いて、0.212mmの目開きを有するステンレス篩を用いて、乾燥式かつ機械式振とう法によって20分間に亘って原料片を篩分けによって、0.212mmの目開きを有するステンレス篩を通過する原料片を取り除く。すなわち、前記原料片は、上限を規定するステンレス篩(目開き=0.71mm)を通過し、下限を規定するステンレス篩(目開き=0.212mm)を通過しない原料片である。 Here, the raw material pieces are obtained by sieving according to JIS Z 8815 using a stainless steel sieve according to JIS Z 8801, for example. For example, using a stainless steel sieve with an opening of 0.71 mm, the raw material pieces are sieved for 20 minutes by a dry and mechanical shaking method to pass through a stainless steel sieve with an opening of 0.71 mm. Obtain raw material pieces. Subsequently, using a stainless sieve with an opening of 0.212 mm, the raw material pieces are sieved for 20 minutes by a dry and mechanical shaking method to pass through a stainless sieve with an opening of 0.212 mm. remove the raw material pieces. That is, the raw material piece is a raw material piece that passes through a stainless sieve (opening=0.71 mm) that defines the upper limit and does not pass through a stainless sieve (opening=0.212 mm) that defines the lower limit.
原料片の充填量は、喫煙時のニコチンの揮散量を増加させる観点から、300mg以上であることが好ましく、350mg以上であることがより好ましい。 From the viewpoint of increasing the volatilization amount of nicotine during smoking, the filling amount of raw material pieces is preferably 300 mg or more, more preferably 350 mg or more.
[カートリッジ]
図1に示すインフューズドたばこ製品1においては、カートリッジ20内に霧化部30と原料保持部40が収容される。図3および図4は当該カートリッジの構造を説明する図である。図中、30は霧化部、40は原料保持部である。カートリッジ20は、リザーバ21と、霧化装置22と、流路形成体23と、外枠体24とを有する。カートリッジ20は、エアロゾル流路として、霧化装置22よりも下流側に配置された第1流路20Xを有する。
[cartridge]
In the infused
リザーバ21は、エアロゾル源21Aを貯留する。リザーバ21は、エアロゾルの流れ方向に直交する断面において流路形成体23の周囲に位置する。リザーバ21は、流路形成体23と外枠体24との間の空隙内に位置する。リザーバ21は、例えば、樹脂ウェブや綿等の多孔体によって構成される。また、リザーバ21は、液体のエアロゾル源21Aを収容するタンクによって構成されていてもよい。エアロゾル源21Aとしては、例えばグリセリン、プロピレングリコール等が挙げられる。
The
霧化装置22は、電池11から供給される電力によって燃焼を伴わずにエアロゾル源21Aを霧化する。霧化装置22は、所定ピッチで巻き回された電熱線(コイル)によって構成されている。霧化装置22は、1.0~3.0Ωの範囲の抵抗値を有する電熱線によって構成されていることが好ましい。所定ピッチは、電熱線が接触しない値以上であり、またより小さい値であることが好ましい。所定ピッチは、例えば、0.40mm以下であることが好ましい。所定ピッチは、エアロゾル源21Aの霧化を安定させるために一定であることが好ましい。所定ピッチとは、互いに隣接する電熱線の中心の間隔である。
The
流路形成体23は、エアロゾルの流れ方向に沿って延びる第1流路20Xを形成する筒状形状を有する。外枠体24は、流路形成体23を収容する筒状形状を有する。外枠体24はたばこカプセル30の一部を収容する。
The
カートリッジ20は、電源ユニット10に対して着脱可能である。また、原料保持部40は、カートリッジ20に対して着脱可能である。すなわち、カートリッジ20および原料保持部40は、それぞれ交換可能である。
The
[電源ユニット]
電源ユニット10の一例を図5に示す。図5に示される電源ユニット10は、電池11を有する。電池11は、使い捨てタイプの電池であってもよく、充電タイプの電池であってもよい。電池11の出力電圧の初期値は、1.2V以上4.2V以下の範囲であることが好ましい。また、電池11の電池容量は、100mAh以上1000mAh以下の範囲であることが好ましい。
[Power supply unit]
An example of the
[実施例A1]
図2(1)に示す直方体の原料保持部を準備した。当該原料保持部の外枠体は透明な樹脂(VisiJet M3 crystal)からなり、3Dプリンタ(ProJet 3600)を用いて成形された。その寸法は表1のとおりであった。網状部材として、ポリオレフィン繊維、ポリプロピレン繊維とポリエチレンを混紡した厚み1mmの不織布を用いた。
[Example A1]
A rectangular parallelepiped raw material holding portion shown in FIG. 2(1) was prepared. The outer frame body of the raw material holding part was made of a transparent resin (VisiJet M3 crystal) and molded using a 3D printer (ProJet 3600). Its dimensions were as shown in Table 1. A 1-mm-thick non-woven fabric obtained by blending polyolefin fibers, polypropylene fibers, and polyethylene was used as the mesh member.
前記原料保持部を備える図1に示すインフューズドたばこ製品を準備し、これをエアロゾルの流れが略鉛直方向となり、原料充填部に充填された原料が霧化部側の網状部材の上面を覆うように自動喫煙装置(Borgwaldt社製、LM4E)に接続し、インフューズドたばこ製品と自動喫煙装置の間にケンブリッジフィルタを1枚配し、インフューズドたばこ製品が発生させたエアロゾルをケンブリッジフィルタで捕集できるようにした。 The infused tobacco product shown in FIG. 1 having the raw material holding portion is prepared, the aerosol flow is substantially vertical, and the raw material filled in the raw material filling portion covers the upper surface of the net-like member on the atomizing portion side. Connected to an automatic smoking device (Borgwaldt, LM4E) as in the above, one Cambridge filter was placed between the infused tobacco product and the automatic smoking device, and the aerosol generated by the infused tobacco product was filtered through the Cambridge filter. made it possible to collect
ケンブリッジフィルタは、直径約44mm、厚さ1.5mmの平たい円形のガラス繊維のフィルタで、粒子状物質を捕捉可能なフィルタとして、当業者に周知であり汎用されている。ケンブリッジフィルタは、日本ケンブリッジフィルタ株式会社、Borgwaldt社(カタログ番号8020 285 2)等より入手可能である。
自動喫煙機は、“CORESTA RECOMMENDED METHOD No.81 “ROUTINE ANALYTICAL MACHINE FOR E-CIGARETTE AEROSOL GENERATION AND COLLECTION - DEFINITIONS AND STANDARD CONDITIONS (June 2015)””の喫煙試験条件に準じた条件で、最大で100回まで喫煙動作を行わせた。喫煙動作の回数に応じ、次の5区間
第1区間(5回喫煙動作相当):~10回、
第2区間(20回喫煙動作相当):~30回、
第3区間(40回喫煙動作相当):~50回、
第4区間(60回喫煙動作相当):~70回、
第5区間(80回喫煙動作相当):~90回、
第6区間(95回喫煙動作相当):~100回、
を設定して機械喫煙を行った。
A Cambridge filter is a flat circular glass fiber filter with a diameter of about 44 mm and a thickness of 1.5 mm, and is well known and widely used by those skilled in the art as a filter capable of capturing particulate matter. Cambridge filters are available from Cambridge Filter Japan Co., Ltd., Borgwald (catalog number 8020 285 2), and the like.
The automatic smoking machine can be used up to 100 times under the conditions according to the smoking test conditions of “CORESTA RECOMMENDED METHOD No.81 “ROUTINE ANALYTICAL MACHINE FOR E-CIGARETTE AEROSOL GENERATION AND COLLECTION - DEFINITIONS AND STANDARD CONDITIONS (June 2015)””. A smoking motion was performed. Depending on the number of smoking actions, the following 5 sections 1st section (equivalent to 5 smoking actions): ~ 10 times,
2nd section (equivalent to
3rd section (equivalent to
4th section (equivalent to
5th section (equivalent to
6th section (equivalent to smoking motion 95 times): ~ 100 times,
was set for machine smoking.
各区間で設定した回数の機械喫煙が終了した後、直ちにエアロゾルを捕集したケンブリッジフィルタをスクリュー瓶に収容し、内部標準物質として1,3-ブタンジオールを0.4mg/mL含むエタノール10mlを加えて、280回/分の条件で1時間振盪して、捕集されたエアロゾルを抽出した。抽出液をガスクロマトグラフィー分析に供し、ニコチン量を測定した。捕集されたエアロゾルの内容成分分析として、インフューズドたばこ製品から吐出されるニコチン量が、喫煙動作を重ねるごとに増減する程度を検討した。ニコチンの定量は当業者慣用の方法で行った。すなわち捕集されたエアロゾルを含むエタノール溶液を、GC-MS(Agilent Technology社製、型番5977B GC/MSD、ガス種He、ガス流速1.3ml/min、カラム DB-WAX 30mm×0.25mm×0.25μm)にて、内容成分を比較定量分析した。
Immediately after mechanical smoking was completed for the set number of times in each section, the Cambridge filter that had collected the aerosol was placed in a screw bottle, and 10 ml of ethanol containing 0.4 mg/mL of 1,3-butanediol was added as an internal standard. The sample was shaken at 280 times/minute for 1 hour to extract the collected aerosol. The extract was subjected to gas chromatography analysis to measure the amount of nicotine. As part of the component analysis of the collected aerosol, we examined the extent to which the amount of nicotine exhaled from the infused tobacco product increases or decreases with repeated smoking motions. Nicotine was quantified by a method commonly used by those skilled in the art. That is, the ethanol solution containing the collected aerosol was analyzed by GC-MS (manufactured by Agilent Technology, model number 5977B GC/MSD, gas type He, gas flow rate 1.3 ml/min, column DB-
第1区間:0~10回におけるニコチン量を、10で除して1回喫煙動作によるニコチン吐出量(μg/puff)を求めた。同様に、第2~6区間について、当該区間が相当する喫煙動作回数で定量結果を除した。そのうえで、第1区間のニコチン吐出量 (μg/puff)を100とした各区間のニコチン吐出量の割合で示した(図6)。 Section 1: The amount of nicotine discharged from 0 to 10 times was divided by 10 to obtain the amount of nicotine discharged (μg/puff) per smoking action. Similarly, for the 2nd to 6th segments, the quantitative results were divided by the number of smoking motions corresponding to the segments. Then, the nicotine ejection amount (μg/puff) in the first interval was set to 100, and the ratio of the nicotine ejection amount in each interval was shown (FIG. 6).
本明細書で使用する「喫煙動作」との文言について説明する。インフューズドたばこ製品は、紙巻たばこ製品と異なり、たばこ原料を燃焼しないことから、一般的に燃焼や熱分解によって生じたガスまたは微粒子が浮遊する気体である「煙」は生じない。従って、人がそれからエアロゾルを吐出させる動作は厳密には「喫煙動作」ではなく、「吸引動作」とも言える。また、人がエアロゾルを吐出させる動作に相当する自動喫煙機による動作も同様である。しかしながら、たばこ製造業および関連する国際規格において、当該動作の慣用表現としては未だ「喫煙動作」が一般的である。本明細書では、慣用表現を尊重して「喫煙動作」との文言をそのまま利用する。 The term "smoking motion" used in this specification will be explained. Unlike cigarette products, infused tobacco products do not burn tobacco raw materials, and therefore do not generate "smoke", which is generally gas generated by combustion or thermal decomposition or gas with fine particles suspended therein. Therefore, the action from which a person discharges an aerosol is not strictly a "smoking action", but can also be called a "sucking action". The same applies to the action of an automatic smoking machine, which corresponds to the action of a person discharging an aerosol. However, in the tobacco industry and related international standards, the idiomatic expression for the action is still "smoking action". In this specification, the phrase "smoking action" is used as it is, respecting the common expression.
[実施例A2]
Lを2mmにした以外は、実施例1と同じ方法で喫煙試験を行い、評価した。
[比較例A]
Lを0mmにした以外は、実施例1と同じ方法で喫煙試験を行い、評価した。これらの結果を図6に示す。
[Example A2]
A smoking test was conducted and evaluated in the same manner as in Example 1, except that L was 2 mm.
[Comparative Example A]
A smoking test was conducted and evaluated in the same manner as in Example 1, except that L was set to 0 mm. These results are shown in FIG.
[実施例B]
形状を表2に示すとおりに変更した以外は、実施例1と同じ方法で喫煙試験を行い、評価した。これらの結果を図7に示す。
[Example B]
A smoking test was conducted and evaluated in the same manner as in Example 1, except that the shape was changed as shown in Table 2. These results are shown in FIG.
[実施例C]
形状を表3に示すとおりに変更した以外は、実施例1と同じ方法で喫煙試験を行い、評価した。これらの結果を図8に示す。
[Example C]
A smoking test was conducted and evaluated in the same manner as in Example 1, except that the shape was changed as shown in Table 3. These results are shown in FIG.
本発明の非燃焼型たばこ製品は、喫煙の終始にわたって香味成分が所定の量で供給されることが明らかである。 It is clear that the non-combustion tobacco product of the present invention supplies a predetermined amount of flavor components throughout smoking.
1 インフューズドたばこ製品
2 非吸口端
3 吸口端
10 電源ユニット
11 電池
20 カートリッジ
20X 第1流路
21 リザーバ
21A エアロゾル源
22 霧化装置
23 流路形成体
24 外枠体
30 霧化部
38 流路
40 原料保持部
41 離間部
42 第1網状部材、不織布
43 外枠体
44 第2網状部材、不織布
48 上流端
49 下流端
1 infused
Claims (8)
霧化部で発生された蒸気またはエアロゾルが流入される原料保持部と、を備えるたばこ製品であって、
前記原料保持部内に、タバコ属植物の細片または細粉を含む原料が充填される領域と、当該原料を封止するために当該領域の上流側に配置された第1網状部材とを備え、
前記霧化部における流路の下流端面を流路方向に垂直な面に垂直投影して形成された像の面積をSa、前記第1網状部材における流路面を流路方向に垂直な面に垂直投影して形成された像の面積をS1とするとき、Sa<S1であり、
前記霧化部における流路の下流端と前記第1網状部材が離間されている、
たばこ製品。 an atomizing section;
A tobacco product comprising a raw material holding portion into which vapor or aerosol generated in the atomizing portion flows,
In the raw material holding part, a region filled with a raw material containing pieces or dust of a Nicotiana plant, and a first net-like member arranged upstream of the region for sealing the raw material,
Sa is the area of the image formed by vertically projecting the downstream end face of the flow channel in the atomizing section onto a plane perpendicular to the flow channel direction; When the area of the image formed by projection is S1, Sa<S1,
A downstream end of the flow path in the atomizing section and the first mesh member are separated from each other,
tobacco products.
L≧0.05M
(Mは、第2網状部材が存在しない場合は、第1網状部材の下流側面と原料保持部の下流端内壁との流路方向における最大距離、
第2網状部材が存在する場合は、第1網状部材の下流側面と第2網状部材の上流側面との流路方向における最大距離である)
請求項1または2に記載のたばこ製品。 The flow path direction length L of the spaced portion satisfies the following relationship:
L≧0.05M
(M is the maximum distance in the flow path direction between the downstream side surface of the first net member and the inner wall of the downstream end of the raw material holding portion when the second net member is not present,
When the second net-like member exists, it is the maximum distance in the flow direction between the downstream side of the first net-like member and the upstream side of the second net-like member)
3. A tobacco product according to claim 1 or 2.
L≧0.05M’
(M’は、第2網状部材が存在しない場合は、第1網状部材の流路部分の下流側面と原料保持部の下流端内壁との流路方向における最大距離、
第2網状部材が存在する場合は、第1網状部材の流路部分の下流側面と第2網状部材の流路部分の上流側面との流路方向における最大距離である)
請求項1~3のいずれかに記載のたばこ製品。 The flow path direction length L of the spaced portion satisfies the following relationship:
L≧0.05M′
(M' is the maximum distance in the flow path direction between the downstream side of the flow path portion of the first mesh member and the inner wall of the downstream end of the raw material holding portion when the second mesh member does not exist,
When the second mesh member exists, it is the maximum distance in the flow path direction between the downstream side of the flow path portion of the first mesh member and the upstream side of the flow path portion of the second mesh member)
A tobacco product according to any one of claims 1-3.
3Sa≦S1≦10Sa
請求項1~5のいずれかに記載のたばこ製品。 S1 and Sa satisfy the following relationship,
3 Sa ≤ S1 ≤ 10 Sa
A tobacco product according to any one of claims 1-5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/JP2021/022621 WO2022264244A1 (en) | 2021-06-15 | 2021-06-15 | Tobacco product |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/JP2021/022621 WO2022264244A1 (en) | 2021-06-15 | 2021-06-15 | Tobacco product |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016075748A1 (en) * | 2014-11-10 | 2016-05-19 | 日本たばこ産業株式会社 | Non-combusting flavor inhaler |
| WO2016208757A1 (en) * | 2015-06-26 | 2016-12-29 | 日本たばこ産業株式会社 | Atomization unit |
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2021
- 2021-06-15 WO PCT/JP2021/022621 patent/WO2022264244A1/en not_active Ceased
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016075748A1 (en) * | 2014-11-10 | 2016-05-19 | 日本たばこ産業株式会社 | Non-combusting flavor inhaler |
| WO2016208757A1 (en) * | 2015-06-26 | 2016-12-29 | 日本たばこ産業株式会社 | Atomization unit |
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