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WO2019019148A1 - Fibre de laine imperméable à l'eau contenant un parfum en microcapsules - Google Patents

Fibre de laine imperméable à l'eau contenant un parfum en microcapsules Download PDF

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Publication number
WO2019019148A1
WO2019019148A1 PCT/CN2017/094904 CN2017094904W WO2019019148A1 WO 2019019148 A1 WO2019019148 A1 WO 2019019148A1 CN 2017094904 W CN2017094904 W CN 2017094904W WO 2019019148 A1 WO2019019148 A1 WO 2019019148A1
Authority
WO
WIPO (PCT)
Prior art keywords
wool fiber
wool
fiber
microcapsule
chitosan
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/CN2017/094904
Other languages
English (en)
Chinese (zh)
Inventor
龚利峰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Jingcun Garment Co Ltd
Original Assignee
Suzhou Jingcun Garment Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Jingcun Garment Co Ltd filed Critical Suzhou Jingcun Garment Co Ltd
Priority to PCT/CN2017/094904 priority Critical patent/WO2019019148A1/fr
Publication of WO2019019148A1 publication Critical patent/WO2019019148A1/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
    • D02G3/04—Blended or other yarns or threads containing components made from different materials
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
    • D02G3/12—Threads containing metallic filaments or strips
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/12—Aldehydes; Ketones
    • D06M13/123—Polyaldehydes; Polyketones
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/12—Aldehydes; Ketones
    • D06M13/127—Mono-aldehydes, e.g. formaldehyde; Monoketones
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
    • D06M23/12—Processes in which the treating agent is incorporated in microcapsules

Definitions

  • the invention belongs to the technical field of wool fibers, in particular to a waterproof wool fiber containing microcapsule fragrance.
  • Wool is an important raw material for the textile industry. It has the advantages of good elasticity, strong moisture absorption and good thermal insulation. It is not only comfortable to use in winter, but also suitable for use in spring and autumn. It is comfortable and dry. At the same time, wool has rich elasticity and direct contact with skin. The blood vessels help to improve the microcirculation of the human body. At the same time, the pores between the fibers under the rough surface form an air flow layer, which makes people feel more refreshed, comfortable and soft, and eliminates fatigue. However, the wool fiber has a large degree of curling, so the wool fiber fabric is easily contracted and deformed after being washed, and is easily damaged by insects and is not easy to store; the existing wool fiber is mostly poor in water resistance, and the wool has a unique odor.
  • the object of the present invention is to provide a waterproof wool fiber comprising a microcapsule fragrance, comprising a wool fiber body, wherein the wool fiber body is a bundle of heterogeneous wool fibers, ordinary wool fibers and stainless steel fibers, and is double a hollow structure, the hollow cavity is filled with bamboo fiber, and the bamboo fiber is wrapped with a cotton gauze, and the bamboo fiber contains a waterproof agent; the heterogeneous wool fiber and the ordinary wool fiber are loaded with microcapsule spice Wool fiber.
  • the cross-section of the heterogeneous wool fibers has a polygonal structure, preferably a regular hexagonal structure.
  • the cross-section of the heterogeneous wool fibers has a cross-shaped structure.
  • the cross-section of the heterogeneous wool fibers is in the shape of a trefoil or a four-leaf clover.
  • the stainless steel fibers have a diameter of 20-25 ⁇ m.
  • the waterproofing agent is ADM-666 water-based waterproofing agent (Dongmei Aimer Anti-Molding Technology Co., Ltd.).
  • the microcapsule fragrance is a microcapsule fragrance containing a chitosan as a shell, an oil-in-water mixture of a layered crystalline sodium disilicate and a ketone ketone fragrance as a capsule core.
  • the method for preparing wool fiber loaded with microcapsule fragrance comprises the following steps Step: thiophene ketone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)) is emulsified by alkyl glucoside emulsifier and added to layered crystal II
  • thiophene ketone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)
  • O/W oil-in-water
  • Aqueous solution reacting wool fiber with vanillin and triethanolamine fatty acid ester quaternary ammonium salt solution to obtain vanillin-wool fiber; immersing vanillin-wool fiber in chitosan microparticle coated with tamarind perfume
  • a reaction of adding a glutaraldehyde solution is obtained.
  • the aqueous chitosan solution has a concentration of from 10 to 15% by weight.
  • the fluorenone: layered crystalline sodium disilicate: chitosan mass ratio is 1:2:2.
  • the micro-capsule-containing waterproof wool fiber of the present invention is formed by juxtaposing bundled wool fibers, ordinary wool fibers and stainless steel fibers, and the stainless steel fibers have good resistance.
  • Static electricity, flame retardant, abrasion resistance, sound absorption, anti-electromagnetic wave effect increase the anti-wrinkle effect of wool fiber;
  • increase the waterproofing agent can effectively improve the waterproof performance of wool fiber;
  • wool fiber adopts chitosan and layered crystal silicon
  • the sodium salt is coated with the ketone ketone spice, and the chitosan amino group and the wool fiber amino group are cross-linked by glutaraldehyde to obtain a wool fiber having a fruity, floral, woody and the like flavor, and the flavor is sustained and sustained.
  • a waterproof wool fiber comprising a microcapsule spice, comprising a wool fiber body, wherein the wool fiber body is a bundle of a heterogeneous wool fiber, a common wool fiber and a stainless steel fiber, and has a double-sided hollow structure, and a hollow structure inner cavity
  • the bamboo fiber is filled, and the bamboo fiber is wrapped with a cotton gauze, and the bamboo fiber contains a waterproofing agent; the heterogeneous wool fiber and the ordinary wool fiber are wool fibers loaded with microcapsule fragrance.
  • the cross-section of the heterogeneous wool fibers has a polygonal structure, preferably a regular hexagon.
  • the stainless steel fiber has a diameter of 20 ⁇ m.
  • the waterproofing agent is ADM-666 water-repellent waterproofing agent (Dongmei Aimer Mildew Anti-bacteria Technology Co., Ltd.).
  • the microcapsule fragrance is a microcapsule fragrance containing a chitosan as a shell, a layered crystalline sodium disilicate and a sulphuric acid flavoring oil-in-water mixture as a capsule core.
  • the method for preparing wool fiber loaded with microcapsule fragrance comprises the following steps: thioxanthone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl) After being emulsified by an alkyl glycoside emulsifier, it is added to a layered crystalline sodium disilicate aqueous solution to obtain an oil-in-water (O/W) mixture of the scorpion ketone and the layered crystalline sodium disilicate, and then with the aqueous chitosan.
  • thioxanthone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)
  • O/W oil-in-water
  • Aqueous solution is reacted to obtain an aqueous solution of chitosan microcapsule coated with tamarind perfume; the wool fiber is impregnated and reacted with vanillin and triethanolamine fatty acid ester quaternary ammonium salt aqueous solution to obtain vanillin-wool fiber; vanillin - The wool fiber is immersed in an aqueous solution of chitosan microcapsules coated with tamarind perfume, and then reacted by adding a glutaraldehyde solution.
  • the aqueous chitosan solution concentration was 10% by weight.
  • Turbinone layered crystalline sodium disilicate: chitosan mass ratio is 1:2:2.
  • a waterproof wool fiber comprising a microcapsule spice, comprising a wool fiber body, wherein the wool fiber body is a bundle of a heterogeneous wool fiber, a common wool fiber and a stainless steel fiber, and has a double-sided hollow structure, and a hollow structure inner cavity
  • the bamboo fiber is filled, and the bamboo fiber is wrapped with a cotton gauze, and the bamboo fiber contains a waterproofing agent; the heterogeneous wool fiber and the ordinary wool fiber are wool fibers loaded with microcapsule fragrance.
  • the cross-section of the heterogeneous wool fiber has a cross-shaped structure.
  • the stainless steel fiber has a diameter of 25 ⁇ m.
  • the waterproofing agent is ADM-666 water-repellent waterproofing agent (Dongmei Aimer Mildew Anti-bacteria Technology Co., Ltd.).
  • the microcapsule fragrance is a microcapsule fragrance containing a chitosan as a shell, a layered crystalline sodium disilicate and a sulphuric acid flavoring oil-in-water mixture as a capsule core.
  • the method for preparing wool fiber loaded with microcapsule fragrance comprises the following steps: thioxanthone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl) After being emulsified by an alkyl glycoside emulsifier, it is added to a layered crystalline sodium disilicate aqueous solution to obtain an oil-in-water (O/W) mixture of the scorpion ketone and the layered crystalline sodium disilicate, and then with the aqueous chitosan.
  • thioxanthone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)
  • O/W oil-in-water
  • Aqueous solution is reacted to obtain an aqueous solution of chitosan microcapsule coated with tamarind perfume; the wool fiber is impregnated and reacted with vanillin and triethanolamine fatty acid ester quaternary ammonium salt aqueous solution to obtain vanillin-wool fiber; vanillin - The wool fiber is immersed in an aqueous solution of chitosan microcapsules coated with tamarind perfume, and then reacted by adding a glutaraldehyde solution.
  • the aqueous chitosan solution concentration was 15% by weight.
  • Turbinone layered crystalline sodium disilicate: chitosan mass ratio is 1:2:2.
  • a waterproof wool fiber comprising a microcapsule spice, comprising a wool fiber body, wherein the wool fiber body is a bundle of a heterogeneous wool fiber, a common wool fiber and a stainless steel fiber, and has a double-sided hollow structure, and a hollow structure inner cavity
  • the bamboo fiber is filled, and the bamboo fiber is wrapped with a cotton gauze, and the bamboo fiber contains a waterproofing agent; the heterogeneous wool fiber and the ordinary wool fiber are wool fibers loaded with microcapsule fragrance.
  • the cross-section of the heterogeneous wool fiber is trilobal or four-leaf clover.
  • the stainless steel fiber has a diameter of 22 ⁇ m.
  • the waterproofing agent is ADM-666 water-repellent waterproofing agent (Dongmei Aimer Mildew Anti-bacteria Technology Co., Ltd.).
  • the microcapsule fragrance is a microcapsule fragrance containing a chitosan as a shell, a layered crystalline sodium disilicate and a sulphuric acid flavoring oil-in-water mixture as a capsule core.
  • the method for preparing wool fiber loaded with microcapsule fragrance comprises the following steps: thioxanthone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl) After being emulsified by an alkyl glycoside emulsifier, it is added to a layered crystalline sodium disilicate aqueous solution to obtain an oil-in-water (O/W) mixture of the scorpion ketone and the layered crystalline sodium disilicate, and then with the aqueous chitosan.
  • thioxanthone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)
  • O/W oil-in-water
  • Aqueous solution is reacted to obtain an aqueous solution of chitosan microcapsule coated with tamarind perfume; the wool fiber is impregnated and reacted with vanillin and triethanolamine fatty acid ester quaternary ammonium salt aqueous solution to obtain vanillin-wool fiber; vanillin - The wool fiber is immersed in an aqueous solution of chitosan microcapsules coated with tamarind perfume, and then reacted by adding a glutaraldehyde solution.
  • the aqueous chitosan solution concentration was 12% by weight.
  • Turbinone layered crystalline sodium disilicate: chitosan mass ratio is 1:2:2.

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

Une fibre de laine imperméable à l'eau contenant un parfum en microcapsules, formée en groupant une fibre de laine de forme spéciale, une fibre de laine ordinaire et une fibre d'acier inoxydable en parallèle. La fibre d'acier inoxydable présente de bonnes performances antistatiques, d'ininflammabilité, de résistance à l'usure, d'absorption acoustique et d'isolation, et d'effets de prévention d'ondes électromagnétiques, et améliore l'effet antirides de la fibre de laine; les performances d'étanchéité à l'eau de la fibre de laine peut être efficacement améliorée par l'ajout d'un agent imperméable à l'eau; de fibres de laine avec un parfum de fruit, un parfum floral, un parfum boisés, etc. sont préparés en utilisant du chitosane et du disilicate de sodium cristallin en couches pour encapsuler un parfum de damascone et réticuler des groupes amino chitosane et des groupes amino de fibres de laine au moyen de glutaraldéhyde, de telle sorte que le parfum soit lentement libéré et durable.
PCT/CN2017/094904 2017-07-28 2017-07-28 Fibre de laine imperméable à l'eau contenant un parfum en microcapsules Ceased WO2019019148A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PCT/CN2017/094904 WO2019019148A1 (fr) 2017-07-28 2017-07-28 Fibre de laine imperméable à l'eau contenant un parfum en microcapsules

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2017/094904 WO2019019148A1 (fr) 2017-07-28 2017-07-28 Fibre de laine imperméable à l'eau contenant un parfum en microcapsules

Publications (1)

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WO2019019148A1 true WO2019019148A1 (fr) 2019-01-31

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112680845A (zh) * 2020-12-05 2021-04-20 安徽颍上县富颍纺织有限公司 一种防水抗菌的混纺再生棉纱

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080193761A1 (en) * 2005-04-22 2008-08-14 Universidade Do Minho Microcapsules With Functional Reactive Groups For Binding To Fibres and Process Of Application and Fixation
CN103103708A (zh) * 2012-11-09 2013-05-15 无锡成龙制衣有限公司 印花、色织防静电防辐射面料的生产工艺
CN103876299A (zh) * 2012-12-22 2014-06-25 青岛同冠王实业有限公司 防辐射内衣的制作工艺
CN104562351A (zh) * 2015-02-09 2015-04-29 苏州陈恒织造有限公司 一种含不锈钢纤维的羊毛生产工艺
CN106592253A (zh) * 2016-12-30 2017-04-26 珠海威丝曼股份有限公司 一种含香羊毛纤维及其制备方法
CN107217356A (zh) * 2017-07-26 2017-09-29 苏州井村服饰有限公司 一种含微胶囊香料的防水羊毛纤维

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080193761A1 (en) * 2005-04-22 2008-08-14 Universidade Do Minho Microcapsules With Functional Reactive Groups For Binding To Fibres and Process Of Application and Fixation
CN103103708A (zh) * 2012-11-09 2013-05-15 无锡成龙制衣有限公司 印花、色织防静电防辐射面料的生产工艺
CN103876299A (zh) * 2012-12-22 2014-06-25 青岛同冠王实业有限公司 防辐射内衣的制作工艺
CN104562351A (zh) * 2015-02-09 2015-04-29 苏州陈恒织造有限公司 一种含不锈钢纤维的羊毛生产工艺
CN106592253A (zh) * 2016-12-30 2017-04-26 珠海威丝曼股份有限公司 一种含香羊毛纤维及其制备方法
CN107217356A (zh) * 2017-07-26 2017-09-29 苏州井村服饰有限公司 一种含微胶囊香料的防水羊毛纤维

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112680845A (zh) * 2020-12-05 2021-04-20 安徽颍上县富颍纺织有限公司 一种防水抗菌的混纺再生棉纱

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