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WO2016082106A1 - Method for preparing soap using deteriorated edible oil - Google Patents

Method for preparing soap using deteriorated edible oil Download PDF

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Publication number
WO2016082106A1
WO2016082106A1 PCT/CN2014/092191 CN2014092191W WO2016082106A1 WO 2016082106 A1 WO2016082106 A1 WO 2016082106A1 CN 2014092191 W CN2014092191 W CN 2014092191W WO 2016082106 A1 WO2016082106 A1 WO 2016082106A1
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WIPO (PCT)
Prior art keywords
edible oil
soap
saponification
preparing
drying
Prior art date
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Ceased
Application number
PCT/CN2014/092191
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French (fr)
Chinese (zh)
Inventor
董盈泽
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Individual
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Individual
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Priority to PCT/CN2014/092191 priority Critical patent/WO2016082106A1/en
Publication of WO2016082106A1 publication Critical patent/WO2016082106A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined

Definitions

  • the present invention relates to a method for comprehensive utilization of waste, and in particular to a method for preparing soap using a deteriorated edible oil.
  • triglycerides in oil are decomposed into glycerol and fatty acids under the action of light, heat and bacteria, and the latter can be further oxidized into peroxides, ketones, aldehydes, etc.
  • a mixture of various substances has a "hala" taste.
  • the formation of toxic substances has a stimulating effect on the gastrointestinal tract, and can also cause damage to the nervous system and liver.
  • the preparation method of soap is generally after deodorization and deacidification treatment, adding sodium hydroxide solution, stirring constantly, after esterification, adding antioxidant, preservative and flavor, etc., stirring evenly, pouring into the mold After cooling, demould, shape, print the icon, put it in the dry room and dry it for a while.
  • the technical problem to be solved by the present invention is to provide a new method for preparing soap with metamorphic edible oil with reasonable design and reasonable operability for the deficiencies of the prior art.
  • the invention relates to a method for preparing soap by using metamorphic edible oil, which is characterized in that: all raw materials are edible oils having a shelf life, and are saponified, shaped and dried according to a certain formula; the formula is: to every 1000 ml In the shelf life edible oil, 450-550 ml of water, 450-550 g of sodium hydroxide, 15-25 g of salt, and 15-25 g of flavor are added; the saponification temperature is 80 ° C, and the saponification time is 35-45 minutes; The drying temperature is 55 65 ° C, and the drying time is 48 8 ⁇ .
  • the technical problem to be solved by the present invention can also be achieved by the following technical solutions.
  • the method for preparing soap by using the modified edible oil is characterized in that: the formula is to add 500 ml of water, 500 g of sodium hydroxide, 20 g of salt, and 20 g of flavor to each 1000 ml of shelf life edible oil.
  • the technical problem to be solved by the present invention can also be achieved by the following technical solutions.
  • the above method for preparing soap by using a deteriorated edible oil is characterized in that the saponification temperature is 80 ° C and the saponification time is 40 minutes.
  • the technical problem to be solved by the present invention can also be achieved by the following technical solutions.
  • the above method for preparing soap by using the deteriorated edible oil is characterized in that: the drying temperature is 60 ° C, and the drying time is 6 hours.
  • the soap prepared by the invention not only has strong decontamination ability, but also has a pleasant fragrance for washed articles.
  • Example 1 a method for preparing soap by using metamorphic edible oil: all raw materials are used in shelf life edible oil, saponified, shaped and dried according to a certain formula; the formula is: to every 1000 ml In the shelf life edible oil, 450-550 ml of water, 450-550 g of sodium hydroxide, 15-25 g of salt, and 15-25 g of flavor are added; the saponification temperature is 80 ° C, and the saponification time is 35-45 minutes; The drying temperature is 55 65 ° C, and the drying time is 48 8 ⁇ .
  • Embodiment 2 the method for preparing soap by using the modified edible oil in the embodiment 1: the formula is to add 500 ml of water, 500 g of sodium hydroxide, and salt 20 to each 1000 ml of shelf life edible oil. Grams, 20 grams of essence.
  • Embodiment 3 in the method for preparing soap by using the modified edible oil according to Embodiment 1, the saponification temperature is
  • the saponification time is 40 minutes.
  • Embodiment 4 in the method for preparing soap using the modified edible oil according to Embodiment 1, the drying temperature is At 60 ° C, the drying time is 6 hours.
  • Example 5 a method for preparing soap using metamorphic edible oil:
  • the mixed solution is poured into a stainless steel basin, while stirring, pour 1000 ml of edible oil, 20 grams of flavor;

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

A method for preparing a soap using a deteriorated edible oil, the method comprising using a shelf-life expired edible oil as all ingredients thereof; according to a certain formula, performing saponification, shaping, and drying, the formula being: adding 450-550 ml of water, 450-550 g of sodium hydroxide, 15-25 g of salt, and 15-25 g of fragrance to each 1000 ml of the shelf-life expired edible oil; the saponification temperature is 80°C, and the saponification time is 35-45 min; the drying temperature is 55-65°C and the drying time is 4-8 hrs. The prepared soap has a strong detergent effect, imparts a pleasant fragrance to a washed item, and re-utilizes waste oil.

Description

利用变质食用油制备肥皂的方法  Method for preparing soap by using metamorphic edible oil

技术领域  Technical field

[0001] 本发明涉及一种废弃物综合利用方法, 具体涉及一种利用变质食用油制备肥皂 的方法。  [0001] The present invention relates to a method for comprehensive utilization of waste, and in particular to a method for preparing soap using a deteriorated edible oil.

背景技术  Background technique

[0002] 食用油贮存过程中, 在光、 热及细菌作用下, 油中的甘油三酯分解为甘油和脂 肪酸, 后者可进一步氧化成为过氧化物、 酮类、 醛类等, 所产生的多种物质混 合出现 "哈喇 "味。 形成的有毒物质对胃肠道有刺激作用, 也可引起神经系统及肝 脏损害。  [0002] During the storage of edible oil, triglycerides in oil are decomposed into glycerol and fatty acids under the action of light, heat and bacteria, and the latter can be further oxidized into peroxides, ketones, aldehydes, etc. A mixture of various substances has a "hala" taste. The formation of toxic substances has a stimulating effect on the gastrointestinal tract, and can also cause damage to the nervous system and liver.

[0003] 肥皂的制备方法一般是将油脂经脱臭、 脱酸处理后, 加入氢氧化钠溶液, 不停 搅拌, 酯化好后, 加入抗氧化剂、 防腐剂和香精等, 搅拌均匀, 倒入模具, 冷 却后脱模、 整形、 打印图标, 放到干燥室内干燥一定吋间即可。  [0003] The preparation method of soap is generally after deodorization and deacidification treatment, adding sodium hydroxide solution, stirring constantly, after esterification, adding antioxidant, preservative and flavor, etc., stirring evenly, pouring into the mold After cooling, demould, shape, print the icon, put it in the dry room and dry it for a while.

技术问题  technical problem

[0004] 本发明所要解决的技术问题是针对现有技术的不足, 提供一种新的、 方法设计 合理、 可操作性强的用变质食用油制备肥皂的方法。  [0004] The technical problem to be solved by the present invention is to provide a new method for preparing soap with metamorphic edible oil with reasonable design and reasonable operability for the deficiencies of the prior art.

问题的解决方案  Problem solution

技术解决方案  Technical solution

[0005] [0004]本发明所要解决的技术问题是通过以下的技术方案来实现的。 本发明是 一种利用变质食用油制备肥皂的方法, 其特点是: 所有原料为过保质期食用油 , 按照一定配方, 经皂化、 造型、 烘干而成; 所述配方为: 向每 1000毫升过保 质期食用油中加入水 450— 550毫升、 氢氧化钠 450— 550克、 食盐 15— 25克、 香 精 15— 25克; 所述皂化温度为 80°C, 皂化吋间为 35— 45分钟; 所述烘干温度为 55 65°C, 烘干吋间为 4 8小吋。  [0004] The technical problem to be solved by the present invention is achieved by the following technical solutions. The invention relates to a method for preparing soap by using metamorphic edible oil, which is characterized in that: all raw materials are edible oils having a shelf life, and are saponified, shaped and dried according to a certain formula; the formula is: to every 1000 ml In the shelf life edible oil, 450-550 ml of water, 450-550 g of sodium hydroxide, 15-25 g of salt, and 15-25 g of flavor are added; the saponification temperature is 80 ° C, and the saponification time is 35-45 minutes; The drying temperature is 55 65 ° C, and the drying time is 48 8 吋.

[0006] 本发明所要解决的技术问题还可以通过以下的技术方案来实现的。 以上所述的 利用变质食用油制备肥皂的方法, 其特点是: 所述配方为向每 1000毫升过保质 期食用油中加入水水 500毫升、 氢氧化钠 500克、 食盐 20克、 香精 20克。 [0007] 本发明所要解决的技术问题还可以通过以下的技术方案来实现的。 以上所述的 利用变质食用油制备肥皂的方法, 其特点是: 所述皂化温度为 80°C, 皂化吋间为 40分钟。 The technical problem to be solved by the present invention can also be achieved by the following technical solutions. The method for preparing soap by using the modified edible oil is characterized in that: the formula is to add 500 ml of water, 500 g of sodium hydroxide, 20 g of salt, and 20 g of flavor to each 1000 ml of shelf life edible oil. [0007] The technical problem to be solved by the present invention can also be achieved by the following technical solutions. The above method for preparing soap by using a deteriorated edible oil is characterized in that the saponification temperature is 80 ° C and the saponification time is 40 minutes.

[0008] 本发明所要解决的技术问题还可以通过以下的技术方案来实现的。 以上所述的 利用变质食用油制备肥皂的方法, 其特点是: 所述烘干温度为 60°C, 烘干吋间为 6小吋。  [0008] The technical problem to be solved by the present invention can also be achieved by the following technical solutions. The above method for preparing soap by using the deteriorated edible oil is characterized in that: the drying temperature is 60 ° C, and the drying time is 6 hours.

发明的有益效果  Advantageous effects of the invention

有益效果  Beneficial effect

[0009] 与现有技术相比, 本发明制备的肥皂不仅去污能力强, 洗涤过的物品清香宜人 Compared with the prior art, the soap prepared by the invention not only has strong decontamination ability, but also has a pleasant fragrance for washed articles.

, 而且还实现了废弃油品的再利用。 , but also the reuse of waste oil.

实施该发明的最佳实施例  BEST MODE FOR CARRYING OUT THE INVENTION

本发明的最佳实施方式  BEST MODE FOR CARRYING OUT THE INVENTION

[0010] 以下进一步描述本发明的具体技术方案, 以便于本领域的技术人员进一步地理 解本发明, 而不构成对其权利的限制。 [0010] The specific technical solutions of the present invention are further described below, so that those skilled in the art can further understand the present invention without limiting the rights thereof.

本发明的实施方式 Embodiments of the invention

[0011] 实施例 1, 一种利用变质食用油制备肥皂的方法: 所有原料为过保质期食用油 , 按照一定配方, 经皂化、 造型、 烘干而成; 所述配方为: 向每 1000毫升过保 质期食用油中加入水 450— 550毫升、 氢氧化钠 450— 550克、 食盐 15— 25克、 香 精 15— 25克; 所述皂化温度为 80°C, 皂化吋间为 35— 45分钟; 所述烘干温度为 55 65°C, 烘干吋间为 4 8小吋。  [0011] Example 1, a method for preparing soap by using metamorphic edible oil: all raw materials are used in shelf life edible oil, saponified, shaped and dried according to a certain formula; the formula is: to every 1000 ml In the shelf life edible oil, 450-550 ml of water, 450-550 g of sodium hydroxide, 15-25 g of salt, and 15-25 g of flavor are added; the saponification temperature is 80 ° C, and the saponification time is 35-45 minutes; The drying temperature is 55 65 ° C, and the drying time is 48 8 吋.

[0012] 实施例 2, 实施例 1所述的利用变质食用油制备肥皂的方法中: 所述配方为向每 1000毫升过保质期食用油中加入水水 500毫升、 氢氧化钠 500克、 食盐 20克、 香 精 20克。  [0012] Embodiment 2, the method for preparing soap by using the modified edible oil in the embodiment 1: the formula is to add 500 ml of water, 500 g of sodium hydroxide, and salt 20 to each 1000 ml of shelf life edible oil. Grams, 20 grams of essence.

[0013] 实施例 3, 实施例 1所述的利用变质食用油制备肥皂的方法中: 所述皂化温度为 [0013] Embodiment 3, in the method for preparing soap by using the modified edible oil according to Embodiment 1, the saponification temperature is

80°C, 皂化吋间为 40分钟。 At 80 ° C, the saponification time is 40 minutes.

[0014] 实施例 4, 实施例 1所述的利用变质食用油制备肥皂的方法中: 所述烘干温度为 60°C, 烘干吋间为 6小吋。 [0014] Embodiment 4, in the method for preparing soap using the modified edible oil according to Embodiment 1, the drying temperature is At 60 ° C, the drying time is 6 hours.

[0015] 实施例 5, 一种利用变质食用油制备肥皂的方法实验: [0015] Example 5, a method for preparing soap using metamorphic edible oil:

[0016] 1、 预备 1000毫升过期食用油; [0016] 1. Prepare 1000 ml of expired edible oil;

[0017] 2、 将 500毫升冷水倒入烧杯中, 加入食盐 20克, 搅拌至完全溶化;  [0017] 2, 500 ml of cold water is poured into the beaker, adding 20 grams of salt, stirred until completely dissolved;

[0018] 3、 称取 500克烧碱倒入水中, 使其完全溶化; [0018] 3, weighed 500 grams of caustic soda into the water, so that it is completely dissolved;

[0019] 4、 将混合溶液倒入不锈钢盆内, 一边搅拌一边倒入 1000毫升质食用油、 20克 香精;  [0019] 4, the mixed solution is poured into a stainless steel basin, while stirring, pour 1000 ml of edible oil, 20 grams of flavor;

[0020] 5、 继续搅拌混合溶液, 并加热至 80°C, 保温 40分钟, 并不断搅拌;  [0020] 5, continue to stir the mixed solution, and heated to 80 ° C, held for 40 minutes, and constantly stirring;

[0021] 6、 将稠液倒入模具盒中, 用烘干机烘干, 烘干温度为 60°C, 烘干吋间为 6小吋 [0021] 6. Pour the thick liquid into the mold box, and dry it with a dryer. The drying temperature is 60 ° C, and the drying time is 6 hours.

, 取出晾至室温, 稠液渐渐凝固, 将成型肥皂脱模即可。 , take it out to room temperature, the thick liquid gradually solidifies, and the molded soap can be released.

Claims

权利要求书 Claim 一种利用变质食用油制备肥皂的方法, 其特征在于所有原料为过 保质期食用油, 按照一定配方, 经皂化、 造型、 烘干而成; 所述 配方为: 向每 1000毫升过保质期食用油中加入水 450 - 550毫升、 氢氧化钠 450— 550克、 食盐 15— 25克、 香精 15— 25克; 所述皂化 温度为 80°C, 皂化吋间为 35— 45分钟; 所述烘干温度为 55— 65°C , 烘干吋间为 4 8小吋。 The invention relates to a method for preparing soap by using metamorphic edible oil, characterized in that all the raw materials are edible oil having a shelf life, and are saponified, shaped and dried according to a certain formula; the formula is: to per 1000 ml of shelf life edible oil Adding 450-550 ml of water, 450-550 g of sodium hydroxide, 15-25 g of salt, and 15-25 g of flavor; the saponification temperature is 80 ° C, and the saponification time is 35-45 minutes; the drying temperature It is 55-65 ° C, and the drying time is 48 8 inches. 根据权利要求 1所述的利用变质食用油制备肥皂的方法, 其特征在 于: 所述配方为向每 1000毫升过保质期食用油中加入水水 500毫升 、 氢氧化钠 500克、 食盐 20克、 香精 20克。 The method for preparing soap by using a modified edible oil according to claim 1, wherein: the formula is to add 500 ml of water, 500 g of sodium hydroxide, 20 g of salt, and flavor to each 1000 ml of shelf life edible oil. 20 grams. 根据权利要求 1所述的利用变质食用油制备肥皂的方法, 其特征在 于: 所述皂化温度为 80°C, 皂化吋间为 40分钟。 The method for preparing a soap using a deteriorated edible oil according to claim 1, wherein the saponification temperature is 80 ° C and the saponification time is 40 minutes. 根据权利要求 1所述的利用变质食用油制备肥皂的方法, 其特征在 于: 所述烘干温度为 60°C, 烘干吋间为 6小吋。 A method of preparing a soap using a deteriorated edible oil according to claim 1, wherein the drying temperature is 60 ° C and the drying time is 6 hours.
PCT/CN2014/092191 2014-11-25 2014-11-25 Method for preparing soap using deteriorated edible oil Ceased WO2016082106A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PCT/CN2014/092191 WO2016082106A1 (en) 2014-11-25 2014-11-25 Method for preparing soap using deteriorated edible oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2014/092191 WO2016082106A1 (en) 2014-11-25 2014-11-25 Method for preparing soap using deteriorated edible oil

Publications (1)

Publication Number Publication Date
WO2016082106A1 true WO2016082106A1 (en) 2016-06-02

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102057048A (en) * 2008-04-09 2011-05-11 索拉兹米公司 Direct chemical modification of microbial biomass and microbial oils
CN102911816A (en) * 2012-11-14 2013-02-06 沈阳信达信息科技有限公司 Super fatted soap and production method thereof
CN103509666A (en) * 2012-06-18 2014-01-15 林昆仪 porous instant soap

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102057048A (en) * 2008-04-09 2011-05-11 索拉兹米公司 Direct chemical modification of microbial biomass and microbial oils
CN103509666A (en) * 2012-06-18 2014-01-15 林昆仪 porous instant soap
CN102911816A (en) * 2012-11-14 2013-02-06 沈阳信达信息科技有限公司 Super fatted soap and production method thereof

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