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WO2013147548A2 - Gynura procumbens enrichi en vanadium et procédé de culture de celui-ci - Google Patents

Gynura procumbens enrichi en vanadium et procédé de culture de celui-ci Download PDF

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Publication number
WO2013147548A2
WO2013147548A2 PCT/KR2013/002635 KR2013002635W WO2013147548A2 WO 2013147548 A2 WO2013147548 A2 WO 2013147548A2 KR 2013002635 W KR2013002635 W KR 2013002635W WO 2013147548 A2 WO2013147548 A2 WO 2013147548A2
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Prior art keywords
vanadium
water
cultivation
myeongwolcho
cluster
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Korean (ko)
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WO2013147548A3 (fr
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김해용
장재형
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G7/00—Botany in general
    • A01G7/06—Treatment of growing trees or plants, e.g. for preventing decay of wood, for tingeing flowers or wood, for prolonging the life of plants
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G22/00—Cultivation of specific crops or plants not otherwise provided for
    • A01G22/15—Leaf crops, e.g. lettuce or spinach 
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof

Definitions

  • the present invention relates to vanadium-enhanced Myeongwolcho and its cultivation method, and more particularly, by using vanadium-enhanced tillage during the cultivation of Myeongwolcho, the content of vanadium is significantly enhanced compared to that of cultivated Moonwolcho. It relates to a vanadium-enhanced Myeongwolcho and its cultivation method suitable for application to cosmetics, pharmaceuticals and the like.
  • Myeongwolcho is a perennial plant belonging to the Gukje (Guksamchil) family with a plant classification. It has one stem and grows in the form of a leaf spread based on the stem, and the leaf is green in color and has an egg shape. The leaf upper part is pointed and the lower part is elliptical. Leaf edges are flat or wavy. Both surface of the leaves are smooth and the lines are clear.
  • Myeongwolcho can be grown by cutting, and it is reproduced by picking leaves, eating leaves with food, or drying leaves and making tea.
  • Myeongwolcho is called Myeongwolcho in China, and life preserve in Japan, and also called diabetic or tribombanyawa in Korea. It clears blood and is effective in preventing aging, thrombolysis, blood sugar, blood pressure, cholesterol, and improving gastrointestinal disorders. It is known to be helpful, and in particular, it can be used as a material for the treatment effect of diabetes and hypertension.
  • vanadium is an essential mineral component in the human body that affects glucose metabolism by altering the activity of insulin, acting like insulin, or altering the activity of glucose-6-phosphatase. It has the effect of treating and preventing diabetes, and also has the effect of preventing Atherosclerosis by interfering with the biosynthetic process of cholesterol, and is involved in the formation of bone, cartilage and teeth, especially cardiovascular and heart in the case of vanadium deficiency It is known to cause disease and a decrease in fertility.
  • Vanadium is contained in fish, carrots, unrefined grains, etc., and is consumed through them. It also produces and sells vanadium-containing bottled water.
  • An object of the present invention is to provide an enhanced moonshine vinegar and a method of cultivating the vanadium component, which is transferred to the early moon moonshine to facilitate absorption of vanadium, which is an essential mineral component, by using cultivated water containing vanadium.
  • an object of the present invention is to provide a food, cosmetics, and medicines using Myeongwolcho, the vanadium component is enhanced.
  • the present invention to achieve the above object
  • the content of the vanadium component of Myeongwolcho is at least 9 ppb, preferably 20-5000 ppb, more preferably 30-1000 ppb.
  • the cultivated water provides a cultivation method of Myeongwolcho, which has been enhanced with vanadium components, comprising a vanadium component.
  • the content of the vanadium component of the tilled water is 0.5-100 ppb.
  • the present invention provides a food, cosmetics, or medicines using Myeongwolcho reinforced with the vanadium component.
  • the vanadium component-enhanced Myeongwolcho and its cultivation method according to the present invention is a nutritional and pharmacologically excellent food using vanadium-enhanced Myeongwolcho by transferring vanadium, which is an essential mineral component, to the human body for easy absorption by the human body.
  • vanadium which is an essential mineral component
  • FIG. 1 is a view showing the configuration of a vanadium extraction system for selectively extracting vanadium using the cluster of the present invention.
  • FIG. 2 is a view showing the configuration of the first vanadium elution tank in the vanadium extraction system of the present invention.
  • FIG 3 is a view showing the configuration of a second vanadium elution tank in the vanadium extraction system of the present invention.
  • the inventors of the present invention are plants that can enhance the vanadium by selectively absorbing the mineral vanadium in the cultivated water, which has not been reported at all until now, and the vanadium-enriched Myeongwolcho is more nutritious than the conventional moonshine.
  • the present invention has been shown to show very good efficacy both pharmacologically and pharmacologically.
  • the present invention provides moonshine reinforced with vanadium component which is an essential mineral.
  • vanadium component which is an essential mineral.
  • Myeongwolcho does not contain any vanadium components or contains only a very small amount, and even in the case of Myeongwolcho grown in a volcanic region, the amount is less than 5 ppb.
  • the vanadium component is at least 9 ppb, preferably 20-5000 ppb, more preferably 30-1000 ppb.
  • Myeongwolcho in the present invention includes all roots, stems, leaves and flowers.
  • Myeongwolcho enhanced with vanadium component is enhanced by vanadium, which is an essential mineral for human body, in various pharmacological effects that Myungwolcho has, and directly consumes vanadium-enhanced Myeongwolcho, or consumes foods and medicines using the same. If you do, diabetes, hypertension, arteriosclerosis, etc. can bring more pronounced treatment and prevention effects.
  • functional cosmetics which are functional cosmetics manufactured with Myeongwolcho, have excellent efficacy in preventing skin aging, antioxidant, whitening, and skin soothing by UV rays. can do.
  • vanadium-enriched moonshine vine is cut into a suitable size and included in the food, or vanadium-enriched moonshine vinegar is dried and powdered into food, or vanadium-enriched moonshine vinegar water.
  • the alcohol extract may be added to the food.
  • vanadium-enhanced moonshine vinegar when used in medicine, vanadium-enhanced moonshine vinegar may be dried and powdered or vanadium-enhanced moonshine vinegar water or alcohol extract may be included in the medicine.
  • vanadium-enhanced moonshine vinegar when used in cosmetics, vanadium-enhanced moonshine vinegar may be dried and powdered, or vanadium-enhanced moonshine vinegar water or alcohol extracts may be included in the medicine.
  • vanadium-enhanced moonshine vinegar in foods, medicines and cosmetics, except for using vanadium-enhanced moonshine vinegar
  • methods related to the manufacture of known food, medicine, or cosmetics may be used, and vanadium
  • the content of this enhanced moonshinechoe can be arbitrarily adjusted, for example, vanadium-enhanced moonshineweed in cosmetics is suitably 0.01 to 20% by weight based on water or alcohol extract.
  • the vanadium-enhanced Myeongwolcho is a nutritional and pharmacological formula of vanadium and Myeongwolcho without fear of mineral toxicity by using the first absorbed vanadium, which is a mineral component, in a form that is easily absorbed by the human body. It is useful because it can have synergy effect.
  • the present invention provides a cultivation method of Myongwolcho, which is reinforced with vanadium components, characterized in that the cultivation method comprises vanadium components.
  • cultivation water may be applied to the general cultivation method of Myeongwolcho, as well as giving cultivation water containing vanadium components to Myongwolcho planted in soil or hydroponic cultivation.
  • cultivation water containing vanadium components the use of cultivated water containing vanadium as a liquid fertilizer, or the cultivation soil containing vanadium in advance by giving cultivation to the culture soil to be cultivated in early spring.
  • the vanadium component may be eluted from the mineral containing the vanadium component and included in the tilled water.
  • a mineral containing vanadium is scoria.
  • the cultivated water of the present invention includes an electrolytic cell that generates ionized water separated by acidic water and hydrogen water by electrolyzing water heated to a predetermined temperature;
  • a first tank containing the clusters in a partitioned space and connected to an electrolytic cell and heating the electrolyzed ionized water to a temperature and time to promote reaction of the clusters with acidic or hydrogen ions to extract the cluster concentrate from the clusters;
  • the clusters and magnesium are contained in a compartment, connected to the first tank and reacting with the concentrated concentrate and magnesium from the first tank to release acidic or hydrogen ions.
  • a second tank in which a selective reaction is induced to elute a large amount of mineral concentrate; And it may be prepared using a mineral extraction system including a reservoir for introducing the mineral concentrate eluted from the second tank to store by concentration and supply to the outside.
  • FIG. 1 to 3 is one of the mineral extraction system
  • Figure 1 is a view showing the configuration of the vanadium extraction system for selectively extracting vanadium using a cluster
  • Figure 2 is a configuration of the first vanadium elution tank in the vanadium extraction system
  • 3 is a view showing the configuration of a second vanadium elution tank in the vanadium extraction system.
  • the vanadium extraction system includes a first heating tank 100 having a first instantaneous heating module 102, an electrolytic cell 200, a hydrogen water heating tank 220, a first vanadium elution tank 300, and a second vanadium elution.
  • Tank 400 low concentration tank 500, medium concentration tank 600, high concentration tank 700, a second instantaneous heating module 710 and a control unit (not shown).
  • the control unit controls the plurality of solenoid valves connected to the tank or the reservoir to move the concentrated liquid or ionized water generated in each device, the instantaneous heating module installed in the tank to control the instantaneous heating of the concentrated liquid or ionized water stored in the tank do.
  • the first heating tank 100 heats the filtered raw water to the range of 40-60 ° C. using the first instantaneous heating module 102 to supply the electrolyzer 200.
  • it is 40 degrees C or less or 60 degrees C or more, it is the temperature condition which is not electrolyzed for making acidic water and hydrogen water.
  • the first instantaneous heating module 102 includes a heating body including a heating plate which is electrically connected to a heating wire for applying electric power to one end thereof, and a heating module controller electrically connected to the heating body.
  • the electrolyzer 200 is divided into an anode chamber electrode and a cathode chamber electrode by a diaphragm that can pass only ions having electrical properties, and when a voltage is applied, filtered raw water is electrolyzed and acidic water and strong alkali water (hydrogen water). Produce ionized water, including
  • the hydrogen water ranges from pH 7.1-14, and means hydrogen water within about 3 ppm containing a large amount of dissolved hydrogen.
  • the electrolyzer 200 supplies the generated acidic water to the acidic water storage tank 210 and supplies hydrogen water to the hydrogen water heating tank 220.
  • the hydrogen water heating tank 220 is provided with a heating module and connected to the first vanadium elution tank 300 to heat hydrogen water to a range of 50-90 ° C. to supply the first vanadium elution tank 300.
  • the first vanadium elution tank 300 is provided with a first heater rod 340 and connected to the second vanadium elution tank 400 and connected to the low concentration storage tank 500, the medium concentration storage tank 600 and the high concentration storage tank 700. It is.
  • the second vanadium elution tank 400 is provided with a second heater rod 440 and is connected to the low concentration storage tank 500, the medium concentration storage tank 600, and the high concentration storage tank 700.
  • the first vanadium elution tank 300 is a reaction of the clusters and hydrogen by stirring in the lower space of the cylindrical first meshed basket 310 and the first meshed basket 310 to form a predetermined space for containing the clusters In order to promote the first stirring screw 330 and the first heater rods 340 for heating the electrolyzed hydrogen water is positioned.
  • the first meshed basket 310 includes a first meshed separator 320 having a flat plate shape to divide and separate the space to form a plurality of storage spaces in the internal space.
  • the first meshed basket 310 and the first meshed separator 320 are made of porous to facilitate the movement of ions and solutions.
  • the second vanadium elution tank 400 is a cluster and hydrogen by stirring in the lower space of the cylindrical second mesh basket 410 and the second mesh basket 410 forming a predetermined space for containing the cluster and magnesium
  • the second stirring screw 430 for promoting the reaction of the second heater rod 440 for heating the electrolyzed hydrogen water is positioned.
  • the second meshed basket 410 includes a second meshed separator plate 420 in the form of a plate that divides the space to form a plurality of storage spaces in the internal space.
  • the second meshed basket 410 and the second meshed separator 420 are made of porous to facilitate the movement of ions and solutions.
  • magnesium forms a chip or porous sponge having a size of 0.01-20 mm to promote the dissociation rate of hydrogen ions in order to maximize the contact area with the electrolyzed hydrogen water and to secure a large amount of hydrogen ions. Include the form of the material. Magnesium has a purity of 99.0-99.99%.
  • the first and second mesh modules are formed in a porous structure along a circular edge including upper and lower sides, left and right sides, and easy to move hydrogen water into the space inside the module.
  • the shape of the cluster is in the form of powder granules and particles of 5 ⁇ m-20mm in order to maximize the contact area with the electrolyzed hydrogen water and to actively perform the substitution reaction of vanadium and hydrogen ions.
  • the first vanadium elution tank 300 heats the electrolyzed hydrogen water in the pH 7.1-14 range through the hydrogen water heating tank 220 to a certain temperature and time to promote the reaction between the cluster and the hydrogen ions. Vanadium is selectively extracted from.
  • the second vanadium elution tank 400 reacts the cluster concentrate reacted with hydrogen introduced from the primary vanadium elution tank with magnesium, the second vanadium elution tank induces a selective reaction between the released hydrogen ions and the vanadium contained in the cluster to elute a large amount of vanadium. Let's do it.
  • the controller selectively extracts low concentration vanadium, medium concentration vanadium and high concentration vanadium from the cluster using electrolyzed hydrogen water in the range of pH 7.1-14.
  • the method of extracting low concentration vanadium from clusters is as follows.
  • the first vanadium elution tank 300 heats the electrolyzed hydrogen water in the range of pH 7.1-14 introduced from the hydrogen water heating tank 220 at a temperature of 60 ° C. or lower for at least 1 hour.
  • the pH range of 7.1-14 of the hydrogen water is a value optimized for extracting vanadium contained in the cluster.
  • the control unit closes the solenoid valves 900, 920, 930, and 940 of a, c, d and e, opens the solenoid valves 910 and 950 of b and f and extracts the vanadium concentrate from the first vanadium elution tank 300. Move to the low concentration storage tank (500).
  • the reason for heating the first heater rod 340 at a temperature of 60 ° C. or lower for at least 1 hour is to suppress the volatilization of hydrogen ions while increasing the reaction temperature of hydrogen ions and vanadium contained in the cluster.
  • the method for extracting the concentrated vanadium from the clusters is as follows.
  • the first vanadium elution tank 300 receives the electrolyzed hydrogen water in the pH 7.1-14 range from the hydrogen water heating tank 220, preheated to a predetermined temperature, and then moved to the second vanadium elution tank 400. .
  • the second vanadium elution tank 400 operates the second heater rod 440 to heat the cluster concentrate flowing from the first vanadium elution tank 300 at a temperature of 60-80 ° C. for at least 1 hour.
  • the second vanadium elution tank 400 reacts the vanadium contained in the cluster with the hydrogen ions released by reacting the cluster concentrate (basic solution) (or vanadium concentrate) introduced from the first vanadium elution tank 300 with magnesium. Selective reactions are induced to elute medium concentrations of vanadium.
  • the control unit closes the solenoid valves 910, 930 and 950 of b, d and f, opens the solenoid valves 900, 920 and 940 of a, c and e and extracts the vanadium concentrate from the second vanadium elution tank 400. This moves to the medium concentration tank (600).
  • the method of extracting the concentrated vanadium from the clusters is as follows.
  • the first vanadium elution tank 300 is introduced into the electrolyzed hydrogen water in the pH 7.1-14 range from the hydrogen water heating tank 220 to preheat to a predetermined temperature and then moved to the second vanadium elution tank 400. .
  • the second vanadium elution tank 400 operates the second heater rod 440 to heat the cluster concentrate flowing from the first vanadium elution tank 300 at a temperature of 70-100 ° C. for about 6 hours or more.
  • the second vanadium elution tank 400 reacts the vanadium contained in the cluster with the hydrogen ions released by reacting the cluster concentrate (basic solution) (or vanadium concentrate) introduced from the first vanadium elution tank 300 with magnesium. Selective reactions are induced to elute high concentrations of vanadium.
  • the control unit closes the solenoid valves 910, 940 and 950 of b, e, and f, opens the solenoid valves 900, 920 and 930 of a, c and d and extracts the vanadium concentrate from the second vanadium elution tank 400. This moves to the medium concentration tank (600).
  • the control unit passes the vanadium concentrate stored in the low concentration storage tank 500, the medium concentration storage tank 600, the high concentration storage tank 700 to the instantaneous temperature module (cooling or heating), and supplies the crops to the final storage tank at an appropriate supply temperature.
  • the method for extracting the vanadium concentrate from the clusters described above extracts vanadium concentrates of low concentration, medium concentration, and high concentration through components such as temperature, time, and magnesium.
  • the concentration of the vanadium concentrate may be adjusted according to the mixing ratio of the cluster and the magnesium in the second vanadium elution tank 400.
  • the high concentration vanadium concentrate is extracted in a short time and supplied to the high concentration storage tank 700, and in the case of 60: 30 (or 70: 30), the medium concentration vanadium concentrate is extracted In the case of 80: 20 (or 90: 10), the medium vanadium concentrate is extracted and supplied to the medium storage tank 600.
  • the control unit moves the electrolyzed hydrogen water to the tank (the first vanadium elution tank 300 and the second vanadium elution tank 400) in which the cluster for each purpose is stored to adjust the concentration by contact time, and the concentration of the vanadium concentrate
  • the electrolyzed acidic water is supplied diluted in an appropriate mixing ratio.
  • Vanadium-containing cultivated water stored in the storage tanks 500, 600, and 700 of the system may be directly used as cultivated water for cultivation of Myeongwolcho of the present invention, or diluted and used as cultivated water, in the cultivation method of the present invention.
  • the content of the vanadium component of the cultivated water is 0.5-100 ppb, and the content of the vanadium may be arbitrarily adjusted.
  • the arable water containing the vanadium may be fertilized in foliar fertilization or soil by mixing with known liquid fertilizer or nutrients.
  • it may be used in combination with foliar fertilization or fertilized with known natural bactericidal extract or natural insecticidal extract.
  • natural bactericidal extract wood vinegar, eoseongcho extract, green tea extract, polyphenols, ginseng extract, rhubarb extract, cinnamon extract, or yeonkyo extract may be used.
  • the mixing ratio may be arbitrarily adjusted and diluted.
  • the content of vanadium in the fertilized mixture is 5 to 200 ppb.
  • Cultivated water with a vanadium content of 1-5 ppb was prepared from the clusters using a mineral extraction system.
  • Myeongwolcho was cultivated using the tilling water.
  • Table 1 Cultivation period Vanadium content in ppb Immediately after cutting Less than 1 Myeongwolcho root after 2 months of cultivation 25.76 Myeongwolcho stem after 2 months of cultivation 11.32 Myeongwolcho leaves after 2 months of cultivation 9.63 Myeongwolcho root after 3 months cultivation 612.08 Myeongwolcho stem after 3 months of cultivation 108.75 Myeongwolcho leaves after 3 months of cultivation 141.39
  • Cultivated water with a vanadium content of 1-5 ppb was prepared from the clusters using a mineral extraction system.
  • Myeongwolcho was hydroponically grown using the above tillage.
  • Skin external preparation was prepared with vanadium-enhanced Myeongwolcho extract extracted from Myeongwolcho leaves grown for 30 days with vanadium-containing cultivated water in Example 2 with water at 90 to 100 ° C.
  • the skin external preparations are 5.0 parts by weight of vanadium-enhanced moonshine extract, 0.2 parts by weight of triethanolamine, 0.3 parts by weight of carbomer, 8.0 parts by weight of cetearyl alcohol, 1.0 parts by weight of sorbitan stearate, 5.0 parts by weight of polysorbate, hydro It was prepared by mixing 30.0 parts by weight of generated polyisobutene, 1.0 part by weight of disodium ethane, 15 parts by weight of glycerin and 34.5 parts by weight of purified water.
  • the skin external preparation was prepared by the same method as the above with the general Myeongwolcho extract (vanadium content 0 ppb), which was extracted with water of 90 to 100 ° C. before cultivation with vanadium-containing cultivated water.
  • a skin primary stimulation test of the skin external preparations prepared above was carried out.
  • the skin stimulation test was a human patch test. Twenty healthy men and women were tested for human skin irritation according to CTFA guidelines (The Cosmetic, Toiletry and Fragrance Association. Inc. Washington, D.C., 20036, 1991). A certain amount of the skin external preparations were applied to the subject's back and fixed with a Finn chamber and a micropore tape. After 24 hours the pin chamber and micropore tape were removed, the applied material was gently wiped off and the skin changes were read visually. As a result, it was confirmed that the external skin preparations containing the vanadium-enhanced Myeongwolcho extract and the general Myeongwolcho extract of the present invention are non-irritating to the human body.
  • the skin external preparations containing the vanadium-enhanced moonshine vinegar extract of the present invention showed a 41% erythema reduction rate, but the skin external preparations containing the general moon-weed extract showed a erythema reduction rate of 16%. It was confirmed that the skin external preparation containing the erythema suppression effect by ultraviolet rays is remarkably excellent.
  • Radical scavenging ability was measured by lyophilizing Myeongwolcho leaves grown for 30 days with vanadium-containing cultivated water in Example 2.
  • the experimental method used the DPPH method. Specifically, 1 ml of ethanol was added to 1 ml of 0.2 mM DPPH solution dissolved in methanol, 1 ml of the extract described in Table 3 was added thereto, mixed, and then allowed to stand at room temperature for 10 min, and then absorbance was measured at 517 nm with a spectrometer. The magnitude of the activity was the control (control) when no sample was added and the experimental group (experimental) with the sample was expressed as the inhibition rate of DPPH by the following equation. Scavenging activity was expressed as the concentration of sample (Free radical scavenging activity. FSC50, ug / mL) required to reduce the concentration of DPPH by 50%.
  • FSC50 Free radical scavenging activity
  • the vanadium-enhanced Myeongwolcho extract of the present invention was confirmed that the SC 50 (ug / ml) has an excellent radical scavenging ability of 373.6.
  • the vanadium component-enhanced Myeongwolcho and its cultivation method according to the present invention is a nutritional and pharmacologically excellent food using vanadium-enhanced Myeongwolcho by transferring vanadium, which is an essential mineral component, to the human body for easy absorption by the human body.
  • vanadium which is an essential mineral component

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  • Life Sciences & Earth Sciences (AREA)
  • Biodiversity & Conservation Biology (AREA)
  • Ecology (AREA)
  • Forests & Forestry (AREA)
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  • Polymers & Plastics (AREA)
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  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
PCT/KR2013/002635 2012-03-30 2013-03-29 Gynura procumbens enrichi en vanadium et procédé de culture de celui-ci Ceased WO2013147548A2 (fr)

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KR10-2012-0033430 2012-03-30
KR20120033430 2012-03-30

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JP2003158920A (ja) * 2001-11-28 2003-06-03 Marine Bio Kk バナジウム含有キノコ類およびそれを利用した機能性食品ならびにそれらの製造方法
JP2006166833A (ja) * 2004-12-17 2006-06-29 Taiyo Koko Co Ltd バナジウム含有カイワレ大根及びその栽培方法
JP2006180716A (ja) * 2004-12-24 2006-07-13 Taiyo Koko Co Ltd バナジウム含有アガリクス菌糸体の生産方法及びアガリクス機能性食品。
KR100973069B1 (ko) * 2007-05-08 2010-07-29 (주)석경에이.티 자외선 차단 조성물
KR101610300B1 (ko) * 2009-04-17 2016-04-08 (주)아모레퍼시픽 화장료 조성물
KR20120016995A (ko) * 2010-08-17 2012-02-27 (주)복슨로하스 천연미네랄 용출 방법 및 천연미네랄제제, 그리고 이를 이용한 가공품

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