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WO2012154019A1 - Suspension de zéolite micronisée, procédé permettant de la préparer et de l'utiliser en tant qu'excipient dans des préparations agricoles - Google Patents

Suspension de zéolite micronisée, procédé permettant de la préparer et de l'utiliser en tant qu'excipient dans des préparations agricoles Download PDF

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Publication number
WO2012154019A1
WO2012154019A1 PCT/MX2012/000020 MX2012000020W WO2012154019A1 WO 2012154019 A1 WO2012154019 A1 WO 2012154019A1 MX 2012000020 W MX2012000020 W MX 2012000020W WO 2012154019 A1 WO2012154019 A1 WO 2012154019A1
Authority
WO
WIPO (PCT)
Prior art keywords
micronized
natural zeolite
suspension
zeolite
aqueous suspension
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/MX2012/000020
Other languages
English (en)
Spanish (es)
Inventor
Javier Isaías ALANIS ORTEGA
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to MX2013005263A priority Critical patent/MX364313B/es
Publication of WO2012154019A1 publication Critical patent/WO2012154019A1/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • A61K9/141—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers
    • A61K9/143—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers with inorganic compounds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/70—Fixation, conservation, or encapsulation of flavouring agents
    • A23L27/77—Use of inorganic solid carriers, e.g. silica
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/45—Ericaceae or Vacciniaceae (Heath or Blueberry family), e.g. blueberry, cranberry or bilberry

Definitions

  • the invention relates to an aqueous suspension of micronized natural zeolite and its use as a carrier of enzymatic microbial complexes, micronutrients, minerals, fertilizers, fungicidal solutions, bactericides and insecticides, citrus derivatives, etc. for foliar, root, spray, drip, etc. application.
  • the micronized natural zeolite suspension has a solids concentration of 50 to 55% and a particle size of 1 to 20 microns and a surface area of 20 to 30 m2 / g.
  • European Patent No. EP 0738 468 A2 describes the use of an aqueous suspension of chemically activated zeolite with silver (containing 5% silver) as a post-cut flower preservative comprising:
  • this patent exclusively describes the use of a Zeolite suspension chemically activated with silver, as a post-cut flower preserver.
  • the suspension of the natural micronized zeolite mentioned as a carrier of enzymatic microbial complexes, micronutrients, minerals, fertilizers, fungicidal solutions, bactericides and insecticides, citrus derivatives, etc. for foliar, root, spray, drip, etc. application.
  • a solids concentration of 50 to 55% mentioned nor is a particle size of 1 to 20 microns, nor a surface area of 20 to 30 m2 / g mentioned; nor is a milling process treated in a wet condition in a colloid mill mentioned.
  • this patent exclusively describes the use of a suspension of synthetic zeolite 4A, as a fortifying composition that regulates perspiration, protects leaves and fruits.
  • the suspension of the natural micronized zeolite mentioned as a carrier of enzymatic microbial complexes, micronutrients, minerals, fertilizers, fungicidal solutions, bactericides and insecticides, citrus derivatives, etc. for foliar, root, spray, drip, etc. application.
  • a solids concentration of 50 to 55% nor is a particle size of 1 to 20 microns mentioned, nor a surface area of 20 to 30 m2 / g; nor is a milling process treated in a wet condition in a colloid mill mentioned.
  • the granulated zeolite (2 to 4 mm) is subjected to an impregnation or enrichment process with a nutritive solution composed of major elements Nitrogen, Phosphorus and Potassium, humic acid and water.
  • this patent exclusively describes the use of granulated zeolite as an amending composition for agricultural soils, based on a granulated zeolite impregnated with a nutrient solution containing: Nitrogen, Phosphorus, Potassium, Dolomitic Lime, Agricultural Lime, Acid Humic and composted organic matter.
  • a nutrient solution containing: Nitrogen, Phosphorus, Potassium, Dolomitic Lime, Agricultural Lime, Acid Humic and composted organic matter.
  • the suspension of the natural micronized zeolite mentioned as a carrier of enzymatic microbial complexes, micronutrients, minerals, fertilizers, fungicidal solutions, bactericides and insecticides, citrus derivatives, etc. for foliar, root, spray, drip, etc. application.
  • the invention relates to an aqueous suspension of micronized natural zeolite and its use as a carrier of enzymatic microbial complexes, micronutrients, fertilizers, fungicidal solutions, bactericides and insecticides, citrus derivatives, etc. for foliar, root, spray, drip, etc. application. and its application in agricultural preparations comprising:
  • the invention relates to an aqueous suspension of micronized natural zeolite and its use as a carrier of enzymatic microbial complexes, micronutrients, minerals, fertilizers, fungicidal solutions, bactericides and insecticides, citrus derivatives, etc. for foliar, root, spray, drip, etc. application. and its application in agricultural preparations comprising:
  • the natural zeolite is micronized in a micronizer mill, whose rotors are propelled at high revolutions and countercurrent, conditions that are desirable for a fine grinding of the material. Subsequently, the micronized material is classified by means of a turbo classifier until obtaining a particle size of 1 to 20 microns and a surface area of 20 to 30 m2 / g.
  • a natural zeolite of the clinoptilolite / heulandite type was used with the following composition:
  • micronized zeolite is gradually added to the solution of water, dispersants, emulsifiers, humectants and defoamers and mixed at 350 rpm for 90 minutes at a temperature of 25 ° C to form the suspension.
  • micronized zeolite is gradually added to the solution of water, dispersants, emulsifiers, humectants and defoamers and mixed at 350 rpm for 90 minutes at a temperature of 25 ° C to form the suspension.
  • the suspension is formed, it is filtered through a system comprising a gear pump and a US 100 mesh screen to remove any impurity.
  • the final product obtained through this process shows a homogeneous and stable suspension of a micronized zeolite, ideal for use as a carrier of enzymatic microbial complexes, micronutrients, minerals, fertilizers, fungicidal solutions, bactericides and insecticides, citric derivatives, etc. for foliar, root, spray, drip, etc. application. and its application in agricultural preparations.
  • the main advantage of the process of the invention is that a micronized, homogeneous and stable suspension of micronized zeolite can be obtained quickly and effectively.
  • Dispersant 1 1 0.000 kg 2.025 kg
  • Emulsifier 3 0.000 kg 0.810 kg
  • the properties of the suspension were evaluated as follows: To check the suspensibility of the micronized zeolite, tests of Suspensibility, Water STD-D were performed.

Landscapes

  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Inorganic Chemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Microbiology (AREA)
  • Nutrition Science (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Medical Informatics (AREA)
  • Food Science & Technology (AREA)
  • Mycology (AREA)
  • Medicinal Preparation (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fertilizers (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

L'invention concerne une suspension aqueuse de zéolite naturelle micronisée ainsi que son utilisation en tant qu'excipient de complexes microbiens enzymatiques, de micronutriments, de minéraux, d'engrais, de solutions fongicides, bactéricides et insecticides, de dérivés citriques, etc. pour une application foliaire, radiculaire, par aspersion, par goutte-à-goutte, etc. En particulier, la suspension de zéolite naturelle micronisée présente une concentration de solides comprise entre 50 et 55% et une taille particulaire de 1 à 20 microns ainsi qu'une surface utile de 20 à 30m2/g. Le principal avantage du procédé décrit dans l'invention réside dans la possibilité d'obtenir d'une manière rapide et efficace une suspension de zéolite micronisée homogène et stable. L'excipient selon l'invention peut être utilisé pour l'élaboration de préparations agricoles sous forme de suspensions.
PCT/MX2012/000020 2011-05-11 2012-02-23 Suspension de zéolite micronisée, procédé permettant de la préparer et de l'utiliser en tant qu'excipient dans des préparations agricoles Ceased WO2012154019A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
MX2013005263A MX364313B (es) 2011-05-11 2012-02-23 Suspensión de zeolita micronizada, proceso para su preparación y su utilización como acarreador en preparaciones agrícolas.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
MXPCT/MX2011/000053 2011-05-11
PCT/MX2011/000053 WO2012154018A1 (fr) 2011-05-11 2011-05-11 Zéolite activé et micronisée, procédé permettant son activation et sa micronisation et utilisation de celle-ci en tant qu'exicipient dans des préparations pharmaceutiques et des compléments alimentaires

Publications (1)

Publication Number Publication Date
WO2012154019A1 true WO2012154019A1 (fr) 2012-11-15

Family

ID=47139373

Family Applications (2)

Application Number Title Priority Date Filing Date
PCT/MX2011/000053 Ceased WO2012154018A1 (fr) 2011-05-11 2011-05-11 Zéolite activé et micronisée, procédé permettant son activation et sa micronisation et utilisation de celle-ci en tant qu'exicipient dans des préparations pharmaceutiques et des compléments alimentaires
PCT/MX2012/000020 Ceased WO2012154019A1 (fr) 2011-05-11 2012-02-23 Suspension de zéolite micronisée, procédé permettant de la préparer et de l'utiliser en tant qu'excipient dans des préparations agricoles

Family Applications Before (1)

Application Number Title Priority Date Filing Date
PCT/MX2011/000053 Ceased WO2012154018A1 (fr) 2011-05-11 2011-05-11 Zéolite activé et micronisée, procédé permettant son activation et sa micronisation et utilisation de celle-ci en tant qu'exicipient dans des préparations pharmaceutiques et des compléments alimentaires

Country Status (2)

Country Link
MX (2) MX351668B (fr)
WO (2) WO2012154018A1 (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102976867A (zh) * 2012-12-17 2013-03-20 本溪清迈尾矿综合利用有限公司 磁化高硅铁尾矿复合土壤修复肥的生产方法及产品
CN107793196A (zh) * 2016-08-30 2018-03-13 苏州丰倍生物科技有限公司 一种高浓度悬浮水溶肥的制备方法

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MX387430B (es) * 2013-11-21 2025-03-11 Javier Isaias Alanis Ortega Zeolita activada y micronizada, proceso para su preparacion y su utilizacion como modulador del estrés oxidativo y detoxificante.
CN112638490B (zh) 2018-06-15 2023-01-03 格雷斯公司 消泡剂活性物质、其制造方法和消泡制剂
US20210252428A1 (en) * 2018-06-15 2021-08-19 W.R. Grace & Co.-Conn. Defoamer Active, Manufacturing Method Thereof, and Defoaming Formulation

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1488697A1 (fr) * 2002-03-27 2004-12-22 Kumiai Chemical Industry Co., Ltd. Poudre mouillable granulee
WO2005075602A1 (fr) * 2004-02-09 2005-08-18 Ballance Agri-Nutrients Limited Compositions d'engrais
WO2010148158A1 (fr) * 2009-06-17 2010-12-23 Isp Investments Inc. Procédé de préparation de substances actives biocides stables, microencapsulées et à libération lente et composition apparentée

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050031708A1 (en) * 2003-08-06 2005-02-10 Portney Micah S. Composition comprising a zeolite compound for treatment of diseases
WO2010018418A1 (fr) * 2008-08-12 2010-02-18 Novatech D.O.O. Formulation à base de clinoptilolite micronisée utilisée en tant qu’agent thérapeutique produisant un silicium extrêmement biodisponible

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1488697A1 (fr) * 2002-03-27 2004-12-22 Kumiai Chemical Industry Co., Ltd. Poudre mouillable granulee
WO2005075602A1 (fr) * 2004-02-09 2005-08-18 Ballance Agri-Nutrients Limited Compositions d'engrais
WO2010148158A1 (fr) * 2009-06-17 2010-12-23 Isp Investments Inc. Procédé de préparation de substances actives biocides stables, microencapsulées et à libération lente et composition apparentée

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
REHAKOVA.M ET AL.: "Agricultural and agrochemical uses of natural zeolite of the clinoptilolite type", CURRENT OPINION IN SOLID STATE AND MATERIALS SCIENCE, vol. 8, 2008, pages 397 - 404 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102976867A (zh) * 2012-12-17 2013-03-20 本溪清迈尾矿综合利用有限公司 磁化高硅铁尾矿复合土壤修复肥的生产方法及产品
CN102976867B (zh) * 2012-12-17 2016-01-20 北京清迈华清控股(集团)有限公司 磁化高硅铁尾矿复合土壤修复肥的生产方法及产品
CN107793196A (zh) * 2016-08-30 2018-03-13 苏州丰倍生物科技有限公司 一种高浓度悬浮水溶肥的制备方法

Also Published As

Publication number Publication date
MX2012005979A (es) 2012-10-29
WO2012154018A1 (fr) 2012-11-15
MX351668B (es) 2017-10-24
MX364313B (es) 2019-04-17
MX2013005263A (es) 2013-06-28

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