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WO2012003358A3 - Methods and systems for recovering liquified petroleum gas from natural gas - Google Patents

Methods and systems for recovering liquified petroleum gas from natural gas Download PDF

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Publication number
WO2012003358A3
WO2012003358A3 PCT/US2011/042654 US2011042654W WO2012003358A3 WO 2012003358 A3 WO2012003358 A3 WO 2012003358A3 US 2011042654 W US2011042654 W US 2011042654W WO 2012003358 A3 WO2012003358 A3 WO 2012003358A3
Authority
WO
WIPO (PCT)
Prior art keywords
stream
components
component
feed
feed stream
Prior art date
Application number
PCT/US2011/042654
Other languages
French (fr)
Other versions
WO2012003358A2 (en
Inventor
Kevin L. Currence
Robert A. Mortko
Original Assignee
Black & Veatch Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Black & Veatch Corporation filed Critical Black & Veatch Corporation
Priority to AU2011272754A priority Critical patent/AU2011272754B2/en
Priority to CA2805272A priority patent/CA2805272C/en
Publication of WO2012003358A2 publication Critical patent/WO2012003358A2/en
Publication of WO2012003358A3 publication Critical patent/WO2012003358A3/en

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0209—Natural gas or substitute natural gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0233—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of CnHm with 1 carbon atom or more
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0242—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of CnHm with 3 carbon atoms or more
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/04—Processes or apparatus using separation by rectification in a dual pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/74—Refluxing the column with at least a part of the partially condensed overhead gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/76—Refluxing the column with condensed overhead gas being cycled in a quasi-closed loop refrigeration cycle
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/78—Refluxing the column with a liquid stream originating from an upstream or downstream fractionator column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/02—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum
    • F25J2205/04—Processes or apparatus using other separation and/or other processing means using simple phase separation in a vessel or drum in the feed line, i.e. upstream of the fractionation step
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/60—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being (a mixture of) hydrocarbons
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2240/00—Processes or apparatus involving steps for expanding of process streams
    • F25J2240/02—Expansion of a process fluid in a work-extracting turbine (i.e. isentropic expansion), e.g. of the feed stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00—Processes or apparatus involving steps for recycling of process streams
    • F25J2245/02—Recycle of a stream in general, e.g. a by-pass stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/12—External refrigeration with liquid vaporising loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/60—Closed external refrigeration cycle with single component refrigerant [SCR], e.g. C1-, C2- or C3-hydrocarbons

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Separation By Low-Temperature Treatments (AREA)

Abstract

A process and system is provided for separating a feed gas stream containing methane, at least one C2 component, at least one C3 component, and optionally heavier components, into a volatile gas stream containing a major portion of the methane and at least one C2 component and a less volatile stream containing a major portion of the at least one C3 and heavier components. The feed stream is cooled, at least partially condensed, and fed to a fractionation column wherein the feed stream is separated into an overhead vapor stream comprising primarily the lighter components of the feed stream and a bottoms liquid stream comprising primarily the heavier components of the feed stream. The introduction of a reboiler onto the fractionation column assists in removing co-absorbed C2 and lighter components from the fractionation column bottoms thereby facilitating more efficient operation of a downstream deethanizer column. Addition of residue recycle can further supplement recovery of desired components.
PCT/US2011/042654 2010-07-01 2011-06-30 Methods and systems for recovering liquified petroleum gas from natural gas WO2012003358A2 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
AU2011272754A AU2011272754B2 (en) 2010-07-01 2011-06-30 Methods and systems for recovering liquified petroleum gas from natural gas
CA2805272A CA2805272C (en) 2010-07-01 2011-06-30 Methods and systems for recovering liquified petroleum gas from natural gas

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US36075310P 2010-07-01 2010-07-01
US61/360,753 2010-07-01

Publications (2)

Publication Number Publication Date
WO2012003358A2 WO2012003358A2 (en) 2012-01-05
WO2012003358A3 true WO2012003358A3 (en) 2012-04-12

Family

ID=45398673

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2011/042654 WO2012003358A2 (en) 2010-07-01 2011-06-30 Methods and systems for recovering liquified petroleum gas from natural gas

Country Status (5)

Country Link
US (1) US20120000245A1 (en)
AU (1) AU2011272754B2 (en)
CA (1) CA2805272C (en)
MY (1) MY172490A (en)
WO (1) WO2012003358A2 (en)

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US9243842B2 (en) 2008-02-15 2016-01-26 Black & Veatch Corporation Combined synthesis gas separation and LNG production method and system
US10113127B2 (en) 2010-04-16 2018-10-30 Black & Veatch Holding Company Process for separating nitrogen from a natural gas stream with nitrogen stripping in the production of liquefied natural gas
US9777960B2 (en) 2010-12-01 2017-10-03 Black & Veatch Holding Company NGL recovery from natural gas using a mixed refrigerant
US10451344B2 (en) 2010-12-23 2019-10-22 Fluor Technologies Corporation Ethane recovery and ethane rejection methods and configurations
FR2970258B1 (en) * 2011-01-06 2014-02-07 Technip France PROCESS FOR PRODUCING C3 + HYDROCARBON RICH CUT AND METHANE ETHANE RICH CURRENT FROM HYDROCARBON RICH POWER CURRENT AND ASSOCIATED PLANT.
US10852060B2 (en) 2011-04-08 2020-12-01 Pilot Energy Solutions, Llc Single-unit gas separation process having expanded, post-separation vent stream
US10139157B2 (en) 2012-02-22 2018-11-27 Black & Veatch Holding Company NGL recovery from natural gas using a mixed refrigerant
WO2014047464A1 (en) 2012-09-20 2014-03-27 Fluor Technologies Corporation Configurations and methods for ngl recovery for high nitrogen content feed gases
US10563913B2 (en) 2013-11-15 2020-02-18 Black & Veatch Holding Company Systems and methods for hydrocarbon refrigeration with a mixed refrigerant cycle
GB201403560D0 (en) * 2014-02-28 2014-04-16 Eltek As Inverter system
US9574822B2 (en) 2014-03-17 2017-02-21 Black & Veatch Corporation Liquefied natural gas facility employing an optimized mixed refrigerant system
KR101550046B1 (en) * 2014-04-09 2015-09-04 동아대학교 산학협력단 Floating Liquefied Natural Gas Fractional Distillation Process Using Diabatic Divided Wall Column
WO2017075310A1 (en) * 2015-10-29 2017-05-04 Black & Veatch Holding Company Enhanced low temperature separation process
US10006701B2 (en) 2016-01-05 2018-06-26 Fluor Technologies Corporation Ethane recovery or ethane rejection operation
US10330382B2 (en) 2016-05-18 2019-06-25 Fluor Technologies Corporation Systems and methods for LNG production with propane and ethane recovery
US10533794B2 (en) * 2016-08-26 2020-01-14 Ortloff Engineers, Ltd. Hydrocarbon gas processing
US10551118B2 (en) 2016-08-26 2020-02-04 Ortloff Engineers, Ltd. Hydrocarbon gas processing
US10551119B2 (en) * 2016-08-26 2020-02-04 Ortloff Engineers, Ltd. Hydrocarbon gas processing
CA3033088A1 (en) 2016-09-09 2018-03-15 Fluor Technologies Corporation Methods and configuration for retrofitting ngl plant for high ethane recovery
CA3077409A1 (en) 2017-10-20 2019-04-25 Fluor Technologies Corporation Phase implementation of natural gas liquid recovery plants
JP7051372B2 (en) * 2017-11-01 2022-04-11 東洋エンジニアリング株式会社 Hydrocarbon separation method and equipment
JP7043126B6 (en) * 2017-11-06 2022-04-18 東洋エンジニアリング株式会社 A device for separating and recovering multiple types of hydrocarbons from LNG
US12098882B2 (en) 2018-12-13 2024-09-24 Fluor Technologies Corporation Heavy hydrocarbon and BTEX removal from pipeline gas to LNG liquefaction
US12215922B2 (en) 2019-05-23 2025-02-04 Fluor Technologies Corporation Integrated heavy hydrocarbon and BTEX removal in LNG liquefaction for lean gases
US20240417639A1 (en) * 2023-06-19 2024-12-19 Air Products And Chemicals, Inc. Apparatus and Process for Removal of Heavy Hydrocarbons from a Feed Gas

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KR20000052749A (en) * 1996-10-25 2000-08-25 엘코 코포레이션 Hydrocarbon gas processing
US6405561B1 (en) * 2001-05-15 2002-06-18 Black & Veatch Pritchard, Inc. Gas separation process
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Also Published As

Publication number Publication date
MY172490A (en) 2019-11-27
CA2805272C (en) 2015-08-11
AU2011272754B2 (en) 2016-02-11
US20120000245A1 (en) 2012-01-05
WO2012003358A2 (en) 2012-01-05
CA2805272A1 (en) 2012-01-05
AU2011272754A1 (en) 2013-01-17

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