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WO2011113676A2 - Méthode de traitement des cheveux - Google Patents

Méthode de traitement des cheveux Download PDF

Info

Publication number
WO2011113676A2
WO2011113676A2 PCT/EP2011/052735 EP2011052735W WO2011113676A2 WO 2011113676 A2 WO2011113676 A2 WO 2011113676A2 EP 2011052735 W EP2011052735 W EP 2011052735W WO 2011113676 A2 WO2011113676 A2 WO 2011113676A2
Authority
WO
WIPO (PCT)
Prior art keywords
dye
blue
acid
polymer
group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2011/052735
Other languages
English (en)
Other versions
WO2011113676A3 (fr
Inventor
Stephen Norman Batchelor
Jayne Michelle Bird
Sheng MENG
Qingsheng Tao
Jinfang Wang
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hindustan Unilever Ltd
Unilever NV
Original Assignee
Hindustan Unilever Ltd
Unilever NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hindustan Unilever Ltd, Unilever NV filed Critical Hindustan Unilever Ltd
Priority to JP2012557467A priority Critical patent/JP2013522256A/ja
Priority to BR112012023598A priority patent/BR112012023598A2/pt
Priority to EP11705872A priority patent/EP2547321A2/fr
Priority to PH1/2012/501848A priority patent/PH12012501848A1/en
Priority to AU2011229417A priority patent/AU2011229417A1/en
Priority to EA201290934A priority patent/EA201290934A1/ru
Priority to CN2011800148677A priority patent/CN102844020A/zh
Publication of WO2011113676A2 publication Critical patent/WO2011113676A2/fr
Publication of WO2011113676A3 publication Critical patent/WO2011113676A3/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
    • A61Q5/065—Preparations for temporary colouring the hair, e.g. direct dyes
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/57—Compounds covalently linked to a(n inert) carrier molecule, e.g. conjugates, pro-fragrances

Definitions

  • the present invention relates to a method for dying the hair.
  • Numerous cationic polymeric dyes have been disclosed for use as a colorant for human hair, for example in US 4,228,259; US 4,182,612 or FR 2 456 764, WO2008/009579 and WO2009/090121 to WO2009/090125.
  • the present invention relates to a method for colouring hair, comprising the step of applying to the hair a composition comprising a dye polymer in which the dye polymer is obtained more preferably obtained by the reaction of i)a NH 2 group directly and covalently bound to an aromatic ring of a dye with ii)a reactive group of a polymeric compound; in which the reactive group is selected from the group consisting of isocyanate; oxazolone; epoxide; ester, and anhydride.
  • the dye-polymer for use with the method of the invention is formed by the step of reaction a reactive polymer with the NH 2 group of a dye, the NH 2 group being directly covalently bound to an aromatic ring of the dye.
  • the reactive polymer has a group for reacting with the NH 2 , the group selected from: isocyanate; oxazolone; epoxide; ester, and anhydride, preferably epoxide or anhydride, most preferably anhydride.
  • ester classes activated esters are preferred.
  • Suitable post-polymerization modifications of reactive polymers for use with the invention are described in detail in Gauthier, M.A., Gibson, M.I., and Klok H-A., Angew. Chem. Int. Ed 2009 48, 48058.
  • the reactions are selected from:
  • R is H, alkyl, aryl or selected so that the COOR group forms an anhydride.
  • R groups examples include .
  • Z is a polymer.
  • reaction is of the form
  • Non-limiting examples of polymers formed by such reactions are:
  • Catalysts may be used to accelerate the reactions.
  • the dye must contain an NH 2 group covalently bound to an aromatic ring of the dye.
  • the NH 2 is covalently bound to an aromatic ring of the dye, wherein the aromatic ring is in conjugation with the chromophore of the dye.
  • the dye preferably contains the moiety within the aromatic ring structure of the dye.
  • Preferred dyes include:
  • the dye does not contain reactive groups or polymerisable double bonds.
  • a dye containing a reactive groups is made up of a chromophore which is linked to a reactive group that undergoes addition or substitution reactions with - OH, -SH and -NH 2 groups to form covalent bonds.
  • Reactive dyes are described in Industrial Dyes (K.Hunger ed, Wiley VCH 2003). Many Reactive dyes are listed in the colour index (Society of Dyers and Colourists and American Association of Textile Chemists and Colorists). Reactive groups are, for example,
  • dichlorotriazinyl difluorochloropyrimidine, monofluorotrazinyl, dichloroquinoxaline, vinylsulfone, difluorotriazine, monochlorotriazinyl, bromoacrlyamide and
  • Dyes are organic molecules that have an absorption coefficient of greater than 4000, preferably greater than 10 000 mol "1 L cm “1 at any wavelength in the range 400-700nm. Molar absorption coefficients are preferably measured in an organic solvent, preferably propan-2-ol, using a 1 , 5 or 10 cm cell.
  • the dye is preferably selected from organic dyes selected from the following chromophore classes: Aminoketone, anthraquinone, azo, oxazine, azine, triphenodioxazine, triphenyl methane, naphthalimide, xanthene and
  • phthalocyanin more preferably azo, anthraquinone, naphthalimide and azine chromophore classes, most preferably azo and anthraquinone.
  • the dye of preference is an anthraquinone.
  • the dye may be cationic, anionically, or uncharged. Examples of uncharged dyes are found in the disperse dye category. Examples of anionic charged dyes are found in the acid and direct dye category. Examples of cationic charged dyes are found in the basic dye category.
  • the dye is preferably uncharged or has an anionic charge. Most preferably the dye is an anionic charged dye.
  • Preferred dyes containing -NH 2 groups covalently bound to an aromatic ring of the dye are: acid violet 1 ; acid violet 3; acid violet 6; acid violet 1 1 ; acid violet 13; acid violet 14; acid violet 19; acid violet 20; acid violet 36; acid violet 36:1 ; acid violet 41 ; acid violet 42; acid violet 43; acid violet 50; acid violet 51 ; acid violet 63; acid violet 48; acid blue 25; acid blue 40; acid blue 40:1 ; acid blue 41 ; acid blue 45; acid blue 47; acid blue 49; acid blue 51 ; acid blue 53; acid blue 56; acid blue 61 ; acid blue 61 :1 ; acid blue 62; acid blue 69; acid blue 78; acid blue 81 :1 ; acid blue 92; acid blue 96; acid blue 108; acid blue 1 1 1 ; acid blue 215; acid blue 230; acid blue 277; acid blue 344; acid blue 1 17; acid blue 124; acid blue 129; acid blue 129:1 ; acid blue
  • disperse blue 81 disperse blue 83; disperse blue 87; disperse blue 104; disperse blue 1 18; disperse violet 1 ; disperse violet 4, disperse violet 8, disperse violet 17, disperse violet 26; disperse violet 28; solvent violet 26; solvent blue 12; solvent blue 13; solvent blue 18; solvent blue 68; solvent blue 76; disperse red 4; disperse red 1 1 ; disperse red 15; disperse red 31 ; disperse red 53; disperse red 55;
  • Further preferred dyes are selected from mono-azo dyes which contain a phenyl group directly attached to the azo group, wherein the phenyl group has an NH 2 groups covalent bound to it.
  • the reactive polymer may be synthesised by polymerisation of the monomers, preferably the monomers are alkenes.
  • the monomers are alkenes.
  • 2-80 mol%, more preferably 5- 55 mol%. of the monomer are selected from monomers which contain or form isocyanate; oxazolone; epoxide; ester, or anhydride groups on polymerisation.
  • Preferred Suitable monomers include maleic anhydride, glycidyl acrylate, 2- glycidyl methacrylate, 2-vinyl-4,4-dimethyl-5-oxazolone, vinyl isocyanate, 2- Isocyanatoethyl methacrylate, N-methacryloxysuccinimide,.
  • the reactive polymer may comprise a co-monomer.
  • Preferred co-monomers may be selected from alkenes, acrylates and styrenes. Suitable co-monomers include diethylaminoethylmethacrylate, dimethylaminopropyl metacryamide, methyl vinylether, methacrylic acid, 2-acrylamido-2-methyl-1 -propanesulfonic acid, 2- hydroxyethyl acrylate; 2-hydroxyethyl methacrylate dimethylaminoethyl methacrylate, methyl methacrylate, methyl acrylate, hydroxyethyl methacrylate, ethyl methacrylate, ethyl acrylate, hydroxyethyl acrylate, butyl methacrylate, butyl acrylate, acrylamide, t-butyl methacrylate, t-butyl acrylate, sodium 4- vinylbenzenesulphonate, styrene
  • the monomers within the polymer may be arranged in any suitable manner. For example as alternating copolymers possess regularly alternating monomer residues; Periodic copolymers have monomer residue types arranged in a repeating sequence; Random copolymers have a random sequence of monomer residue types; Statistical copolymers have monomer residues arranged according to a known statistical rule; Block copolymers have two or more homopolymer subunits linked by covalent bonds. Most preferably the polymer is a random copolymer.
  • the polymer preferably has a molecular weight of 2000 and greater. Preferred ranges are from 2000 to 1 000 000, more preferred ranges are from 5000 to 100 000. In this context the molecular weight is the number average molecular weight.
  • the polymeric compound can comprise a siloxane polymers with pendant isocyanate; oxazolone; epoxide; ester, or anhydride groups.
  • the polymeric compound within the dye polymer is covalently bound to 1 to 100 dye molecules. More preferably 1 to 40 dye molecules. Most preferably 1 to 10 dye molecules.
  • the polymer may contain cationic and anionic charged groups.
  • the dye is preferably uncharged or anionic charged.
  • the polymer does not contain a primary amine.
  • the dye is preferably uncharged or has an anionic charge. Most preferably the dye is anionic charged.
  • Anionic dyes are particularly preferred when the polymer carries anionic groups on the co-monomers. Particularly preferred is a dye polymer having a poly (methyl vinyl ether-alt-maleic anhydride) polymer reacted with an anionic dye.
  • Combination of polymeric dyes may be used to achieve a wide colour palette
  • a palette of three or more polymeric dyes is preferable, particularly preferred is a palette of three polymeric dyes. It is most effective to use dye-polymer mixtures containing a red dye-polymer, a yellow dye-polymer and a blue dye polymer. Variation of the fractions of blue, yellow, and red in the mixture enables many colours to be reached, for example black, and brown.
  • Poly (methyl vinyl ether-alt-maleic anhydride) polymers reacted with an anionic dye are most preferred.
  • the anionic dye contains 1 or 2 sulphonate groups, most preferably 1 .
  • the level of polymeric dye within the composition is preferably from 0.001 to 5wt% of the total composition, more preferably from 0.01 to 1wt% most preferably from 0.04 to 0.4wt%.
  • the method of the invention comprises a rinse-off step.
  • the method of the invention comprises applying the dye compositions directly to dry or wet hair.
  • the application temperature is from 18 to 38 °C.
  • the composition is a shampoo, conditioner or hair dye composition.
  • the composition is a shampoo it preferably comprises from 5 to 50wt% of the total composition of a cleansing surfactant.
  • the cleansing surfactant comprises anionic and amphoteric surfactant.
  • the composition is a conditioning composition it preferably comprises a conditioning active such as fatty alcohols, fatty acids, fatty amides and fatty esters, silicones, cationic surfactants etc.
  • the composition contains a perfume.
  • the perfume is present at 0.001 to 5wt% of the total composition.
  • the composition of the invention has a pH of from 3 to 9, preferably from 4 to 8.
  • the composition contains greater than 40wt% of the total composition of water.
  • the composition is a liquid and the viscosity of the liquid is greater than 4 centipoise at 293K. Viscosity was measured using a falling ball

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)
  • Coloring (AREA)

Abstract

La présente invention concerne une méthode de coloration des cheveux qui comprend l'étape d'application sur les cheveux d'une composition comprenant un polymère de coloration. Dans cette étape d'application, le polymère de coloration est obtenu par la réaction d'un groupe NH2 lié directement et par covalence à un anneau aromatique d'un colorant i) avec un groupe réactif d'un composé polymère ii) ledit groupe réactif étant sélectionné dans le groupe formé par isocyanate; oxazolone; époxyde; ester et anhydride.
PCT/EP2011/052735 2010-03-19 2011-02-24 Méthode de traitement des cheveux Ceased WO2011113676A2 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
JP2012557467A JP2013522256A (ja) 2010-03-19 2011-02-24 毛髪を処理する方法
BR112012023598A BR112012023598A2 (pt) 2010-03-19 2011-02-24 método para coloração dos cabelos
EP11705872A EP2547321A2 (fr) 2010-03-19 2011-02-24 Méthode de traitement des cheveux
PH1/2012/501848A PH12012501848A1 (en) 2010-03-19 2011-02-24 Method of treating hair
AU2011229417A AU2011229417A1 (en) 2010-03-19 2011-02-24 Method of treating hair
EA201290934A EA201290934A1 (ru) 2010-03-19 2011-02-24 Способ обработки волос
CN2011800148677A CN102844020A (zh) 2010-03-19 2011-02-24 处理毛发的方法

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
CN2010071157 2010-03-19
CNPCT/CN2010/071157 2010-03-19
CNPCT/CN2010/075833 2010-08-10
PCT/CN2010/075833 WO2011113249A1 (fr) 2010-03-19 2010-08-10 Procédé de traitement capillaire

Publications (2)

Publication Number Publication Date
WO2011113676A2 true WO2011113676A2 (fr) 2011-09-22
WO2011113676A3 WO2011113676A3 (fr) 2012-05-31

Family

ID=44625256

Family Applications (4)

Application Number Title Priority Date Filing Date
PCT/CN2010/075834 Ceased WO2011113250A1 (fr) 2010-03-19 2010-08-10 Procédé de traitement capillaire
PCT/CN2010/075833 Ceased WO2011113249A1 (fr) 2010-03-19 2010-08-10 Procédé de traitement capillaire
PCT/EP2011/052735 Ceased WO2011113676A2 (fr) 2010-03-19 2011-02-24 Méthode de traitement des cheveux
PCT/EP2011/052733 Ceased WO2011113675A2 (fr) 2010-03-19 2011-02-24 Méthode de traitement des cheveux

Family Applications Before (2)

Application Number Title Priority Date Filing Date
PCT/CN2010/075834 Ceased WO2011113250A1 (fr) 2010-03-19 2010-08-10 Procédé de traitement capillaire
PCT/CN2010/075833 Ceased WO2011113249A1 (fr) 2010-03-19 2010-08-10 Procédé de traitement capillaire

Family Applications After (1)

Application Number Title Priority Date Filing Date
PCT/EP2011/052733 Ceased WO2011113675A2 (fr) 2010-03-19 2011-02-24 Méthode de traitement des cheveux

Country Status (10)

Country Link
EP (2) EP2547321A2 (fr)
JP (2) JP2013522255A (fr)
CN (2) CN102844019A (fr)
AR (2) AR080761A1 (fr)
AU (2) AU2011229416A1 (fr)
BR (2) BR112012023498A2 (fr)
EA (2) EA201290925A1 (fr)
PH (2) PH12012501847A1 (fr)
TW (2) TW201138892A (fr)
WO (4) WO2011113250A1 (fr)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2015086676A1 (fr) 2013-12-13 2015-06-18 L'oreal Procédé pour colorer des substances kératiniques à partir d'oligomères et/ou de polymères colorés provenant de méta-phénylènediamines, composition et agent de coloration
WO2015086675A1 (fr) 2013-12-13 2015-06-18 L'oreal Procédé de coloration de fibres de kératine au moyen d'oligomères et/ou de polymères colorés dérivés de composés auto-oxydants, composition et agent colorant pour celui-ci
US9949543B2 (en) 2014-10-29 2018-04-24 Noxell Corporation Hair colouration, method and kit thereof
US9949542B2 (en) 2014-10-29 2018-04-24 Noxell Corporation Hair colouration, method and kit thereof

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101531904B1 (ko) * 2010-10-13 2015-06-29 롬엔드하스전자재료코리아유한회사 신규한 유기 전자재료용 화합물 및 이를 포함하는 유기 전계 발광 소자
DE102011119729A1 (de) * 2011-11-30 2013-06-06 S & V Technologies Ag Polymerisierbare Farbstoffe und deren Zusammensetzungen für opthalmologische Anwendungen
JP5919021B2 (ja) * 2012-02-15 2016-05-18 花王株式会社 インクジェット記録用顔料水分散液
EP3145997B1 (fr) * 2014-05-21 2023-07-12 ROLIC Technologies AG Colorants dichroïques polymérisables
US20200048468A1 (en) * 2018-08-07 2020-02-13 Michael Milbocker Polymeric hair color composition

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4182612A (en) 1977-01-31 1980-01-08 The Gillette Company Method for dyeing human hair with cationic polymeric dyes
US4228259A (en) 1976-08-12 1980-10-14 L'oreal Water-soluble cationic polymer dye compounds and process for producing the same
FR2456764A2 (fr) 1979-05-18 1980-12-12 Oreal Nouveaux polymeres colorants, leur preparation et leur utilisation
WO2008009579A1 (fr) 2006-07-18 2008-01-24 Ciba Holding Inc. Colorants polymères pour cheveux
WO2009090121A1 (fr) 2008-01-17 2009-07-23 Basf Se Colorants capillaires polymères
WO2009090125A1 (fr) 2008-01-17 2009-07-23 Basf Se Colorants capillaires polymères

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LU51345A1 (fr) * 1966-06-16 1967-12-18
DE1794352C3 (de) * 1961-10-05 1979-09-27 L'oreal, Paris Verwendung von gefärbten Polymerisaten als färbender Bestandteil in Haarfärbemitteln
FR1498464A (fr) * 1965-09-06 1967-10-20 Oreal Nouvelles résines colorées, laques et lotions de mise en plis colorées pour cheveux, à base de ces résines
US6306182B1 (en) * 1999-12-29 2001-10-23 Revlon Consumer Products Corporation Polymeric dye compounds and compositions and methods for coloring hair
EP1256602A1 (fr) * 2001-05-08 2002-11-13 Rolic AG Mélange dichroique
DE10309523A1 (de) * 2003-03-05 2004-09-16 Wella Ag Mittel und Verfahren zum Färben von Keratinfasern
EP1454614B1 (fr) * 2003-03-06 2007-08-29 KPSS-Kao Professional Salon Services GmbH Composition pour la coloration des cheveux humains
US20050268405A1 (en) * 2004-05-28 2005-12-08 Gaelle Brun Composition for dyeing keratin fibers, comprising at least one pigment and polymers capable of reacting with each other to form covalent bonds
US7799092B2 (en) * 2005-06-29 2010-09-21 L'oreal S.A. Composition for simultaneously bleaching and dyeing keratin fibers, comprising at least one anionic or nonionic direct dye and at least one associative polymer

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4228259A (en) 1976-08-12 1980-10-14 L'oreal Water-soluble cationic polymer dye compounds and process for producing the same
US4182612A (en) 1977-01-31 1980-01-08 The Gillette Company Method for dyeing human hair with cationic polymeric dyes
FR2456764A2 (fr) 1979-05-18 1980-12-12 Oreal Nouveaux polymeres colorants, leur preparation et leur utilisation
WO2008009579A1 (fr) 2006-07-18 2008-01-24 Ciba Holding Inc. Colorants polymères pour cheveux
WO2009090121A1 (fr) 2008-01-17 2009-07-23 Basf Se Colorants capillaires polymères
WO2009090125A1 (fr) 2008-01-17 2009-07-23 Basf Se Colorants capillaires polymères

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Title
"Industrial Dyes", 2003, WILEY VCH
GAUTHIER, M.A., GIBSON, M.I., KLOK H-A., ANGEW. CHEM. INT. ED, vol. 48, 2009, pages 48058
MACROMOLECULES, vol. 27, 1994, pages 7121 - 7126
ZOLLINGER: "Color Chemistry", 2003, WILEY-VCH

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2015086676A1 (fr) 2013-12-13 2015-06-18 L'oreal Procédé pour colorer des substances kératiniques à partir d'oligomères et/ou de polymères colorés provenant de méta-phénylènediamines, composition et agent de coloration
WO2015086675A1 (fr) 2013-12-13 2015-06-18 L'oreal Procédé de coloration de fibres de kératine au moyen d'oligomères et/ou de polymères colorés dérivés de composés auto-oxydants, composition et agent colorant pour celui-ci
US9949543B2 (en) 2014-10-29 2018-04-24 Noxell Corporation Hair colouration, method and kit thereof
US9949542B2 (en) 2014-10-29 2018-04-24 Noxell Corporation Hair colouration, method and kit thereof
US10681971B2 (en) 2014-10-29 2020-06-16 Noxell Corporation Hair colouration, method and kit thereof
US10687594B2 (en) 2014-10-29 2020-06-23 Noxell Corporation Hair colouration, method and kit thereof

Also Published As

Publication number Publication date
EA201290925A1 (ru) 2013-03-29
PH12012501848A1 (en) 2013-01-07
WO2011113250A1 (fr) 2011-09-22
EP2547321A2 (fr) 2013-01-23
AU2011229416A1 (en) 2012-10-11
JP2013522256A (ja) 2013-06-13
AU2011229417A1 (en) 2012-10-11
WO2011113675A3 (fr) 2012-05-31
TW201138853A (en) 2011-11-16
WO2011113249A1 (fr) 2011-09-22
EP2547319A2 (fr) 2013-01-23
TW201138892A (en) 2011-11-16
CN102844020A (zh) 2012-12-26
WO2011113676A3 (fr) 2012-05-31
BR112012023598A2 (pt) 2016-08-02
JP2013522255A (ja) 2013-06-13
EA201290934A1 (ru) 2013-04-30
PH12012501847A1 (en) 2013-02-04
AR080760A1 (es) 2012-05-09
AR080761A1 (es) 2012-05-09
CN102844019A (zh) 2012-12-26
BR112012023498A2 (pt) 2016-05-31
WO2011113675A2 (fr) 2011-09-22

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