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WO2011008009A3 - 유기 클로로하이드로실란과 이의 제조방법 - Google Patents

유기 클로로하이드로실란과 이의 제조방법 Download PDF

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Publication number
WO2011008009A3
WO2011008009A3 PCT/KR2010/004548 KR2010004548W WO2011008009A3 WO 2011008009 A3 WO2011008009 A3 WO 2011008009A3 KR 2010004548 W KR2010004548 W KR 2010004548W WO 2011008009 A3 WO2011008009 A3 WO 2011008009A3
Authority
WO
WIPO (PCT)
Prior art keywords
chlorosilane
organic
present
preparing same
bond
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/KR2010/004548
Other languages
English (en)
French (fr)
Other versions
WO2011008009A9 (ko
WO2011008009A2 (ko
Inventor
정일남
홍순현
김은성
현상일
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lotte Fine Chemical Co Ltd
Original Assignee
Samsung Fine Chemicals Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Samsung Fine Chemicals Co Ltd filed Critical Samsung Fine Chemicals Co Ltd
Priority to CN201080040874XA priority Critical patent/CN102498117A/zh
Priority to US13/383,697 priority patent/US20120114544A1/en
Priority to JP2012520540A priority patent/JP2012532927A/ja
Publication of WO2011008009A2 publication Critical patent/WO2011008009A2/ko
Publication of WO2011008009A3 publication Critical patent/WO2011008009A3/ko
Publication of WO2011008009A9 publication Critical patent/WO2011008009A9/ko
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/123—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-halogen linkages
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0255—Phosphorus containing compounds
    • B01J31/0267—Phosphines or phosphonium compounds, i.e. phosphorus bonded to at least one carbon atom, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, the other atoms bonded to phosphorus being either carbon or hydrogen
    • B01J31/0268—Phosphonium compounds, i.e. phosphine with an additional hydrogen or carbon atom bonded to phosphorous so as to result in a formal positive charge on phosphorous

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

본 발명은 실리콘 고분자를 제조하는데 유용한 출발물질인 유기 클로로하이드로실란과 이의 제조방법에 관한 것으로서, 더욱 상세하게는 4차 유기 포스포니움염 화합물을 촉매로 사용하여 값싸고 쉽게 얻을 수 있는 클로로실란의 Si-H 결합과 다른 유기클로로실란의 Si-Cl 결합을 교환시켜 여러 가지 새로운 유기 클로로하이드로실란을 고 수율로 합성하고, 또한 촉매를 사용한 후 회수하여 재사용이 가능하기 때문에 매우 경제적이므로 실리콘 원료물질을 대량생산하는데 효과적이다.
PCT/KR2010/004548 2009-07-13 2010-07-13 유기 클로로하이드로실란과 이의 제조방법 Ceased WO2011008009A2 (ko)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN201080040874XA CN102498117A (zh) 2009-07-13 2010-07-13 有机氢氯硅烷及其制备方法
US13/383,697 US20120114544A1 (en) 2009-07-13 2010-07-13 Organic chlorohydrosilane and method for preparing them
JP2012520540A JP2012532927A (ja) 2009-07-13 2010-07-13 有機クロロヒドロシラン及びその製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020090063616A KR101263789B1 (ko) 2009-07-13 2009-07-13 유기 클로로하이드로실란과 이의 제조방법
KR10-2009-0063616 2009-07-13

Publications (3)

Publication Number Publication Date
WO2011008009A2 WO2011008009A2 (ko) 2011-01-20
WO2011008009A3 true WO2011008009A3 (ko) 2011-06-23
WO2011008009A9 WO2011008009A9 (ko) 2011-08-04

Family

ID=43449959

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2010/004548 Ceased WO2011008009A2 (ko) 2009-07-13 2010-07-13 유기 클로로하이드로실란과 이의 제조방법

Country Status (5)

Country Link
US (1) US20120114544A1 (ko)
JP (1) JP2012532927A (ko)
KR (1) KR101263789B1 (ko)
CN (1) CN102498117A (ko)
WO (1) WO2011008009A2 (ko)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102762763B (zh) 2010-02-17 2014-12-31 乔治洛德方法研究和开发液化空气有限公司 SiCOH低K膜的气相沉积法
US8637695B2 (en) 2011-12-30 2014-01-28 Momentive Performance Materials Inc. Synthesis of organohalosilane monomers from conventionally uncleavable Direct Process Residue
US8697901B2 (en) * 2011-12-30 2014-04-15 Momentive Performance Materials Inc. Synthesis of organohalosilane monomers via enhanced cleavage of direct process residue
CN102850387A (zh) * 2012-09-18 2013-01-02 太仓市运通化工厂 一种二环戊基二氯硅烷的合成方法
JP6044361B2 (ja) * 2013-01-21 2016-12-14 信越化学工業株式会社 ジクロロモノヒドロシラン化合物の製造方法
JP6775418B2 (ja) * 2013-03-14 2020-10-28 モーメンティブ・パフォーマンス・マテリアルズ・インク 高屈折率シロキサン
KR101728308B1 (ko) * 2015-09-14 2017-04-19 기초과학연구원 비전이금속 촉매법 수소규소화 반응을 이용한 규소 고분자 제조방법
WO2018186882A1 (en) * 2017-04-07 2018-10-11 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Catalytic reduction of halogenated carbosilanes and halogenated carbodisilanes
US11008349B2 (en) * 2017-09-20 2021-05-18 Momentive Performance Materials Inc. Process for the production of organohydridochlorosilanes
WO2019060486A1 (en) 2017-09-20 2019-03-28 Momentive Performance Materials Inc. PROCESS FOR PRODUCING ORGANOHYDRIDOCHLOROSILANES FROM HYDRUROSILANES
WO2020048597A1 (de) 2018-09-06 2020-03-12 Wacker Chemie Ag Verfahren zur dehydrierung von dichlorsilan
KR102654573B1 (ko) * 2018-12-10 2024-04-05 엔테그리스, 아이엔씨. 트리아이오도실란의 제조
KR102231991B1 (ko) * 2019-10-30 2021-03-25 주식회사 서연이화 테일게이트 인너 판넬용 폴리프로필렌 수지 조성물 및 이의 성형품

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JPH08337588A (ja) * 1995-06-07 1996-12-24 Huels Ag アルキルヒドロゲンクロルシランの製造方法
JPH09173859A (ja) * 1995-11-30 1997-07-08 Wacker Chemie Gmbh オルガノシランを製造するための方法および触媒、ならびに該触媒の製造法
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KR20060112237A (ko) * 2005-04-26 2006-10-31 와커 헤미 아게 유기수소실란의 제조 방법

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Publication number Priority date Publication date Assignee Title
JPH08337588A (ja) * 1995-06-07 1996-12-24 Huels Ag アルキルヒドロゲンクロルシランの製造方法
JPH09173859A (ja) * 1995-11-30 1997-07-08 Wacker Chemie Gmbh オルガノシランを製造するための方法および触媒、ならびに該触媒の製造法
KR20020034849A (ko) * 2000-11-01 2002-05-09 박호군 유기 실란의 제조방법
KR20060112237A (ko) * 2005-04-26 2006-10-31 와커 헤미 아게 유기수소실란의 제조 방법

Also Published As

Publication number Publication date
WO2011008009A9 (ko) 2011-08-04
CN102498117A (zh) 2012-06-13
US20120114544A1 (en) 2012-05-10
WO2011008009A2 (ko) 2011-01-20
KR101263789B1 (ko) 2013-05-13
KR20110006125A (ko) 2011-01-20
JP2012532927A (ja) 2012-12-20

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